Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** THOMSONITE-CA 1, at 295'K, f-zeolites, sf-thomsonite, ZL, DN (Na,Ca)(3)Al(5)Si(5)O(20).5.7H(2)O Orthorhombic P bmn Z = 2 Pbmn 3 .3 .11 Ref.Str.: Gatta G.D., Kahlenberg V., Kaindl R., Rotiroti N., Cappelletti P., de Gennaro M. (2010) * Amer. Mineral., 95, 495-502 R: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 13.0809 alpha = 90.0 b = 13.0597 beta = 90.0 c = 6.6051 gamma = 90.0 Unit cell volume (cub. angs.) = 1128.37 Molar volume ( cub.cm/mol.) = 339.83 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0575 0.0 0.2774 0.0 Na = 0.7 , Ca = 0.3 2 0.5 0.0242 0.0 0.0 Ca = 0.47, Ca = 0.0 3 0.3089 0.1193 0.2413 0.0 Al = 0.5 , Si = 0.5 4 0.1161 0.1952 0.0026 0.0 Al = 0.5 , Si = 0.5 5 0.25 0.25 0.6209 0.0 Al = 0.5 , Si = 0.5 6 0.356 0.0 0.232 0.0 O = 1.00 7 0.1872 0.1225 0.1583 0.0 O = 1.00 8 0.0 0.1383 0.0 0.0 O = 1.00 9 0.3888 0.1839 0.0867 0.0 O = 1.00 10 0.3117 0.1626 0.4801 0.0 O = 1.00 11 0.1632 0.191 0.7673 0.0 O = 1.00 12 0.1265 0.0 0.6214 0.0 H(2)O = 0.95, H(2)O = 0.0 13 0.3928 0.0 0.7218 0.0 H(2)O = 0.97, H(2)O = 0.0 14 0.0 0.153 0.5 0.0 H(2)O = 0.91, H(2)O = 0.0 15 0.1557 0.0552 0.678 0.0 H = 0.95, H = 0.0 16 0.3776 0.06 0.652 0.0 H = 0.97, H = 0.0 17 0.0426 0.1975 0.557 0.0 H = 0.91, H = 0.0 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0575 0.0 0.2774 2 2 0.5 0.0242 0.0 3 3 0.3089 0.1193 0.2413 4 4 0.1161 0.1952 0.0026 5 5 0.25 0.25 0.6209 6 6 0.356 0.0 0.232 7 7 0.1872 0.1225 0.1583 8 8 0.0 0.1383 0.0 9 9 0.3888 0.1839 0.0867 10 10 0.3117 0.1626 0.4801 11 11 0.1632 0.191 0.7673 12 12 0.1265 0.0 0.6214 13 13 0.3928 0.0 0.7218 14 14 0.0 0.153 0.5 15 15 0.1557 0.0552 0.678 16 16 0.3776 0.06 0.652 17 17 0.0426 0.1975 0.557 18 2 0.5 0.9758 0.0 19 3 0.3089 0.8807 0.2413 20 4 0.1161 0.8048 0.0026 21 5 0.25 0.75 0.6209 22 7 0.1872 0.8775 0.1583 23 8 0.0 0.8617 0.0 24 9 0.3888 0.8161 0.0867 25 10 0.3117 0.8374 0.4801 26 11 0.1632 0.809 0.7673 27 14 0.0 0.847 0.5 28 15 0.1557 0.9448 0.678 29 16 0.3776 0.94 0.652 30 17 0.0426 0.8025 0.557 31 1 0.4424 0.5 0.2774 32 2 0.0 0.5242 0.0 33 3 0.1911 0.6193 0.2413 34 4 0.3839 0.6952 0.0026 35 6 0.144 0.5 0.232 36 7 0.3128 0.6225 0.1583 37 8 0.5 0.6383 0.0 38 9 0.1112 0.6839 0.0867 39 10 0.1883 0.6626 0.4801 40 11 0.3368 0.691 0.7673 41 12 0.3735 0.5 0.6214 42 13 0.1072 0.5 0.7218 43 14 0.5 0.653 0.5 44 15 0.3443 0.5552 0.678 45 16 0.1224 0.56 0.652 46 17 0.4574 0.6975 0.557 47 2 0.0 0.4758 0.0 48 3 0.1911 0.3807 0.2413 49 4 0.3839 0.3048 0.0026 50 7 0.3128 0.3775 0.1583 51 8 0.5 0.3617 0.0 52 9 0.1112 0.3161 0.0867 53 10 0.1883 0.3374 0.4801 54 11 0.3368 0.3089 0.7673 55 14 0.5 0.347 0.5 56 15 0.3443 0.4448 0.678 57 16 0.1224 0.44 0.652 58 17 0.4574 0.3025 0.557 59 1 0.5576 0.5 0.7226 60 3 0.8089 0.6193 0.7587 61 4 0.6161 0.6952 0.9974 62 5 0.75 0.75 0.3791 63 6 0.856 0.5 0.768 64 7 0.6872 0.6225 0.8417 65 9 0.8888 0.6839 0.9133 66 10 0.8117 0.6626 0.5199 67 11 0.6632 0.691 0.2327 68 12 0.6265 0.5 0.3786 69 13 0.8928 0.5 0.2782 70 15 0.6557 0.5552 0.322 71 16 0.8776 0.56 0.348 72 17 0.5426 0.6975 0.443 73 3 0.8089 0.3807 0.7587 74 4 0.6161 0.3048 0.9974 75 5 0.75 0.25 0.3791 76 7 0.6872 0.3775 0.8417 77 9 0.8888 0.3161 0.9133 78 10 0.8117 0.3374 0.5199 79 11 0.6632 0.3089 0.2327 80 15 0.6557 0.4448 0.322 81 16 0.8776 0.44 0.348 82 17 0.5426 0.3025 0.443 83 1 0.9424 0.0 0.7226 84 3 0.6911 0.1193 0.7587 85 4 0.8839 0.1952 0.9974 86 6 0.644 0.0 0.768 87 7 0.8128 0.1225 0.8417 88 9 0.6112 0.1839 0.9133 89 10 0.6883 0.1626 0.5199 90 11 0.8368 0.1911 0.2327 91 12 0.8735 0.0 0.3786 92 13 0.6072 0.0 0.2782 93 15 0.8443 0.0552 0.322 94 16 0.6224 0.06 0.348 95 17 0.9574 0.1975 0.443 96 3 0.6911 0.8807 0.7587 97 4 0.8839 0.8048 0.9974 98 7 0.8128 0.8775 0.8417 99 9 0.6112 0.8161 0.9133 100 10 0.6883 0.8374 0.5199 101 11 0.8368 0.8089 0.2327 102 15 0.8443 0.9448 0.322 103 16 0.6224 0.94 0.348 104 17 0.9574 0.8025 0.443 X-ray density (g/cm cub.) = 2.36 MU (1/cm) = 90.893 Mass attenuation coefficient (cm**2/g) = 38.49 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Na ,Ca 3.048 8 2.4604 7 2.6806 8 2.4449 12 2.5925 14 2.4604 7 2.6806 8 2.5925 14 2.4988 12 2 Ca ,Ca 3.048 6 2.4489 6 2.6064 9 2.333 13 2.4489 6 2.6064 9 2.333 13 3 Al ,Si 2.484 4 1.6762 6 1.6844 7 1.6886 9 1.676 10 4 Al ,Si 2.484 4 1.6797 7 1.6904 8 1.6731 11 1.6749 9 5 Al ,Si 2.484 4 1.6788 10 1.6782 11 1.6788 10 1.6782 11 6 O 3.432 9 2.7705 7 2.6223 9 2.7441 10 3.2708 13 3.4042 13 2.7705 7 2.6223 9 2.7441 10 3.3001 13 7 O 3.432 8 2.7705 6 2.67 8 2.7975 9 2.7285 10 2.7514 11 3.3533 14 3.2007 7 2.7566 9 8 O 3.432 8 2.67 7 2.7196 11 3.3081 14 3.3081 14 2.7985 9 2.7985 9 2.67 7 2.7196 11 9 O 3.432 8 2.6223 6 2.7975 7 2.8017 10 3.4031 13 2.7566 7 2.7985 8 2.7531 11 3.1258 9 10 O 3.432 8 2.7441 6 2.7285 7 2.8017 9 2.7398 11 3.3536 12 2.8607 13 2.7958 10 2.7126 11 11 O 3.432 8 2.7514 7 2.7196 8 2.7398 10 2.7173 12 2.8145 14 2.7531 9 2.7126 10 2.7432 11 12 H(2)O,H(2)O 3.6 11 3.5421 7 3.5007 8 3.3536 10 2.7173 11 3.546 13 2.7154 14 3.5421 7 3.5007 8 3.3536 10 2.7173 11 2.7154 14 13 H(2)O,H(2)O 3.6 8 3.4042 6 3.2708 6 3.4031 9 2.8607 10 3.546 12 3.4031 9 2.8607 10 3.3001 6 14 H(2)O,H(2)O 3.6 10 3.3533 7 3.3081 8 3.3081 8 2.8145 11 2.7154 12 3.4477 10 3.4477 10 3.3533 7 2.8145 11 2.7154 12 15 H ,H 1.8 1 0.8974 12 16 H ,H 1.8 1 0.9307 13 17 H ,H 1.8 1 0.8889 14 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 4.781 9.562 0.054 284.94 4 25.2 56.7 2 0 0 1 6.697 13.394 0.076 144.1 2 93.8 199.0 3 2 0 0 6.764 13.527 0.076 141.23 2 83.5 154.8 4 0 2 0 6.775 13.549 0.077 140.77 2 68.4 103.6 5 1 0 1 7.507 15.013 0.085 114.23 4 80.8 234.3 6 1 1 1 8.241 16.482 0.093 94.4 8 21.8 28.1 7 2 0 1 9.54 19.081 0.108 69.88 4 88.7 172.7 8 0 2 1 9.548 19.096 0.108 69.76 4 43.3 41.1 9 2 2 0 9.595 19.191 0.108 69.06 4 110.7 265.8 10 2 1 1 10.132 20.265 0.114 61.71 8 42.1 68.8 11 1 2 1 10.138 20.276 0.114 61.64 8 61.3 145.6 12 3 1 0 10.734 21.467 0.121 54.76 4 63.0 68.3 13 1 3 0 10.748 21.496 0.121 54.61 4 74.3 94.7 14 2 2 1 11.738 23.476 0.132 45.44 8 30.9 27.3 15 3 0 1 12.221 24.441 0.137 41.76 4 3.3 0.1 16 3 1 1 12.694 25.388 0.143 38.55 8 68.8 114.7 17 1 3 1 12.706 25.412 0.143 38.48 8 92.4 206.5 18 0 0 2 13.488 26.976 0.151 33.92 2 6.1 0.2 19 4 0 0 13.624 27.247 0.153 33.2 2 102.1 54.3 20 0 4 0 13.646 27.292 0.153 33.09 2 2.1 0.0 21 1 0 2 13.919 27.839 0.156 31.72 4 133.6 177.8 22 3 2 1 14.024 28.048 0.157 31.22 8 31.2 19.0 23 2 3 1 14.031 28.062 0.157 31.19 8 94.8 176.3 24 1 1 2 14.34 28.681 0.161 29.77 8 7.0 0.9 25 3 3 0 14.48 28.959 0.162 29.17 4 36.6 12.3 26 2 0 2 15.146 30.293 0.17 26.49 4 124.0 128.0 27 0 2 2 15.151 30.303 0.17 26.47 4 150.3 187.8 28 4 0 1 15.238 30.476 0.171 26.15 4 101.8 85.1 29 0 4 1 15.259 30.517 0.171 26.07 4 29.6 7.2 30 4 2 0 15.274 30.547 0.171 26.02 4 19.1 3.0 31 2 4 0 15.289 30.578 0.171 25.96 4 88.8 64.3 32 2 1 2 15.537 31.074 0.174 25.08 8 3.0 0.1 33 1 2 2 15.541 31.081 0.174 25.07 8 22.0 7.6 34 4 1 1 15.627 31.253 0.175 24.77 8 110.4 189.7 35 1 4 1 15.645 31.291 0.175 24.71 8 141.1 309.2 36 3 3 1 16.015 32.031 0.179 23.49 8 69.6 71.4 37 2 2 2 16.659 33.319 0.186 21.57 8 18.6 4.7 38 4 2 1 16.744 33.487 0.187 21.33 8 168.1 378.7 39 2 4 1 16.758 33.515 0.187 21.3 8 41.1 22.6 40 3 0 2 17.013 34.026 0.19 20.61 4 0.7 0.0 41 3 1 2 17.366 34.732 0.194 19.7 8 58.6 42.5 42 1 3 2 17.375 34.75 0.194 19.68 8 83.4 86.1 43 5 1 0 17.474 34.949 0.195 19.44 4 40.7 10.1 44 1 5 0 17.501 35.003 0.195 19.37 4 53.5 17.4 45 3 2 2 18.389 36.779 0.205 17.38 8 23.7 6.1 46 2 3 2 18.395 36.789 0.205 17.37 8 17.4 3.3 47 5 0 1 18.462 36.925 0.206 17.23 4 5.7 0.2 48 4 3 1 18.472 36.944 0.206 17.21 8 9.1 0.9 49 3 4 1 18.48 36.959 0.206 17.2 8 88.6 84.8 50 5 1 1 18.792 37.584 0.209 16.57 8 9.1 0.9 51 1 5 1 18.817 37.634 0.209 16.52 8 15.5 2.5 52 4 0 2 19.359 38.718 0.215 15.52 4 31.8 4.9 53 0 4 2 19.375 38.751 0.215 15.49 4 13.2 0.9 54 4 4 0 19.474 38.948 0.216 15.32 4 49.3 11.7 55 4 1 2 19.675 39.351 0.219 14.97 8 46.7 20.5 56 1 4 2 19.691 39.381 0.219 14.94 8 15.8 2.3 57 5 2 1 19.751 39.503 0.219 14.84 8 39.1 14.3 58 2 5 1 19.773 39.546 0.22 14.81 8 23.5 5.1 59 3 3 2 19.995 39.989 0.222 14.44 8 123.2 137.8 60 5 3 0 20.091 40.182 0.223 14.29 4 2.2 0.0 61 3 5 0 20.107 40.214 0.223 14.27 4 65.0 19.0 62 0 0 3 20.479 40.957 0.227 13.69 2 59.1 7.5 63 4 2 2 20.6 41.201 0.228 13.51 8 93.3 74.0 64 2 4 2 20.612 41.224 0.229 13.5 8 86.6 63.5 65 4 4 1 20.682 41.365 0.229 13.4 8 6.6 0.4 66 6 0 0 20.69 41.38 0.229 13.38 2 110.9 25.8 67 0 6 0 20.725 41.451 0.23 13.33 2 216.9 98.5 68 1 0 3 20.78 41.56 0.23 13.26 4 41.2 7.1 69 1 1 3 21.079 42.157 0.233 12.84 8 15.4 1.9 70 5 3 1 21.27 42.54 0.235 12.58 8 41.6 13.7 71 3 5 1 21.285 42.571 0.236 12.56 8 54.3 23.3 72 2 0 3 21.663 43.326 0.24 12.07 4 95.9 34.9 73 0 2 3 21.667 43.334 0.24 12.07 4 15.3 0.9 74 6 0 1 21.843 43.686 0.242 11.85 4 13.2 0.6 75 6 2 0 21.869 43.738 0.242 11.82 4 27.8 2.9 76 0 6 1 21.877 43.753 0.242 11.81 4 37.0 5.1 77 2 6 0 21.899 43.798 0.242 11.78 4 90.7 30.5 78 2 1 3 21.952 43.904 0.243 11.72 8 2.7 0.1 79 1 2 3 21.955 43.91 0.243 11.72 8 52.0 19.9 80 5 0 2 22.062 44.125 0.244 11.59 4 17.4 1.1 81 4 3 2 22.071 44.142 0.244 11.58 8 16.9 2.1 82 3 4 2 22.077 44.155 0.244 11.57 8 13.5 1.3 83 6 1 1 22.13 44.26 0.245 11.51 8 23.8 4.1 84 1 6 1 22.162 44.325 0.245 11.47 8 12.6 1.2 85 5 1 2 22.347 44.695 0.247 11.26 8 14.9 1.6 86 1 5 2 22.369 44.739 0.247 11.23 8 29.1 6.0 87 2 2 3 22.801 45.603 0.252 10.76 8 47.0 14.9 88 6 2 1 22.974 45.948 0.253 10.58 8 44.9 13.4 89 2 6 1 23.003 46.006 0.254 10.55 8 12.5 1.0 90 3 0 3 23.075 46.149 0.254 10.47 4 54.6 9.8 91 5 2 2 23.185 46.37 0.256 10.36 8 70.5 32.3 92 2 5 2 23.204 46.408 0.256 10.34 8 44.9 13.1 93 5 4 1 23.26 46.52 0.256 10.28 8 42.8 11.8 94 4 5 1 23.268 46.536 0.256 10.28 8 44.7 12.9 95 3 1 3 23.35 46.699 0.257 10.2 8 34.5 7.6 96 1 3 3 23.357 46.714 0.257 10.19 8 45.9 13.5 97 4 4 2 24.008 48.016 0.264 9.57 8 14.1 1.2 98 3 2 3 24.161 48.321 0.266 9.44 8 76.8 34.9 99 2 3 3 24.165 48.33 0.266 9.43 8 49.3 14.4 100 6 3 1 24.33 48.661 0.267 9.29 8 46.7 12.7 101 3 6 1 24.354 48.707 0.268 9.27 8 10.6 0.7 102 5 3 2 24.532 49.065 0.27 9.11 8 15.8 1.4 103 3 5 2 24.546 49.092 0.27 9.1 8 6.2 0.2 104 7 1 0 24.607 49.215 0.27 9.05 4 2.3 0.0 105 5 5 0 24.628 49.256 0.271 9.03 4 21.8 1.4 106 1 7 0 24.648 49.297 0.271 9.02 4 9.7 0.3 107 4 0 3 24.946 49.891 0.274 8.77 4 29.0 2.3 108 0 4 3 24.959 49.918 0.274 8.76 4 148.3 60.5 109 6 0 2 25.047 50.093 0.275 8.69 4 21.0 1.2 110 0 6 2 25.077 50.154 0.275 8.67 4 46.2 5.8 111 6 4 0 25.141 50.282 0.276 8.62 4 142.4 54.9 112 4 6 0 25.158 50.315 0.276 8.61 4 109.2 32.2 113 4 1 3 25.205 50.411 0.276 8.57 8 106.9 61.5 114 1 4 3 25.218 50.436 0.277 8.56 8 0.8 0.0 115 6 1 2 25.306 50.611 0.277 8.49 8 9.1 0.4 116 1 6 2 25.335 50.67 0.278 8.47 8 20.9 2.3 117 7 0 1 25.365 50.73 0.278 8.45 4 111.9 33.2 118 3 3 3 25.469 50.938 0.279 8.37 8 17.3 1.6 119 7 1 1 25.621 51.243 0.281 8.26 8 30.8 4.9 120 5 5 1 25.641 51.282 0.281 8.24 8 48.6 12.2 121 1 7 1 25.661 51.322 0.281 8.23 8 37.4 7.2 122 4 2 3 25.973 51.946 0.284 8.0 8 33.8 5.7 123 2 4 3 25.983 51.965 0.284 8.0 8 35.3 6.3 124 6 2 2 26.071 52.142 0.285 7.93 8 65.8 21.6 125 2 6 2 26.097 52.194 0.286 7.92 8 5.8 0.2 126 6 4 1 26.14 52.279 0.286 7.89 8 40.6 8.1 127 4 6 1 26.156 52.312 0.286 7.88 8 12.0 0.7 128 5 4 2 26.332 52.663 0.288 7.76 8 18.8 1.7 129 4 5 2 26.339 52.678 0.288 7.75 8 0.5 0.0 130 7 2 1 26.38 52.76 0.288 7.72 8 57.6 16.1 131 2 7 1 26.417 52.833 0.289 7.7 8 17.9 1.6 132 7 3 0 26.652 53.305 0.291 7.55 4 146.0 50.6 133 3 7 0 26.684 53.369 0.292 7.53 4 116.3 32.0 134 5 0 3 27.211 54.421 0.297 7.2 4 65.8 9.8 135 4 3 3 27.218 54.435 0.297 7.19 8 24.7 2.7 136 3 4 3 27.223 54.447 0.297 7.19 8 29.8 4.0 137 6 3 2 27.313 54.625 0.298 7.14 8 59.0 15.6 138 3 6 2 27.334 54.668 0.298 7.12 8 65.4 19.2 139 5 1 3 27.455 54.91 0.299 7.05 8 43.4 8.3 140 1 5 3 27.474 54.948 0.299 7.04 8 51.3 11.6 141 7 3 1 27.612 55.225 0.301 6.96 8 28.5 3.6 142 3 7 1 27.644 55.287 0.301 6.94 8 5.3 0.1 143 0 0 4 27.806 55.612 0.303 6.85 2 204.8 45.1 144 1 0 4 28.046 56.092 0.305 6.72 4 20.7 0.9 145 8 0 0 28.105 56.21 0.306 6.69 2 33.1 1.1 146 0 8 0 28.155 56.309 0.306 6.66 2 90.4 8.6 147 5 2 3 28.179 56.359 0.307 6.65 8 51.2 11.0 148 2 5 3 28.196 56.391 0.307 6.64 8 71.1 21.1 149 7 0 2 28.269 56.538 0.307 6.6 4 63.4 8.3 150 1 1 4 28.285 56.571 0.308 6.59 8 7.7 0.2 151 6 5 1 28.344 56.688 0.308 6.56 8 80.9 27.0 152 5 6 1 28.353 56.705 0.308 6.56 8 64.5 17.2 153 7 1 2 28.507 57.015 0.31 6.48 8 23.3 2.2 154 5 5 2 28.526 57.052 0.31 6.47 8 140.0 79.7 155 1 7 2 28.544 57.089 0.31 6.46 8 11.1 0.5 156 2 0 4 28.758 57.516 0.312 6.35 4 43.1 3.7 157 0 2 4 28.761 57.522 0.312 6.35 4 12.5 0.3 158 4 4 3 28.899 57.797 0.314 6.28 8 13.9 0.8 159 6 4 2 28.99 57.98 0.315 6.24 8 36.0 5.1 160 2 1 4 28.994 57.988 0.315 6.23 8 27.3 2.9 161 1 2 4 28.996 57.992 0.315 6.23 8 26.3 2.7 162 4 6 2 29.005 58.01 0.315 6.23 8 24.8 2.4 163 8 0 1 29.033 58.065 0.315 6.21 4 82.4 13.3 164 8 2 0 29.054 58.108 0.315 6.2 4 59.6 6.9 165 0 8 1 29.081 58.162 0.316 6.19 4 79.1 12.2 166 2 8 0 29.099 58.199 0.316 6.18 4 45.6 4.0 167 7 2 2 29.215 58.429 0.317 6.13 8 37.8 5.5 168 2 7 2 29.249 58.497 0.317 6.11 8 21.1 1.7 169 8 1 1 29.267 58.534 0.317 6.1 8 17.0 1.1 170 7 4 1 29.278 58.556 0.317 6.1 8 18.8 1.3 171 4 7 1 29.303 58.606 0.318 6.09 8 52.1 10.4 172 1 8 1 29.315 58.629 0.318 6.08 8 83.8 26.8 173 5 3 3 29.361 58.721 0.318 6.06 8 17.5 1.2 174 3 5 3 29.373 58.745 0.318 6.05 8 77.1 22.6 175 2 2 4 29.694 59.387 0.322 5.91 8 11.7 0.5 176 6 0 3 29.816 59.633 0.323 5.85 4 90.3 15.0 177 0 6 3 29.843 59.687 0.323 5.84 4 12.7 0.3 178 3 0 4 29.921 59.842 0.324 5.81 4 51.1 4.8 179 8 2 1 29.963 59.926 0.324 5.79 8 33.3 4.0 180 6 6 0 30.005 60.009 0.325 5.77 4 54.0 5.3 181 2 8 1 30.008 60.015 0.325 5.77 8 6.2 0.1 182 6 1 3 30.047 60.094 0.325 5.75 8 28.8 3.0 183 1 6 3 30.073 60.146 0.325 5.74 8 57.2 11.8 184 3 1 4 30.151 60.302 0.326 5.71 8 76.8 21.2 185 1 3 4 30.157 60.314 0.326 5.71 8 86.6 26.9 186 7 3 2 30.37 60.741 0.328 5.62 8 2.0 0.0 187 3 7 2 30.4 60.8 0.328 5.61 8 15.2 0.8 188 7 5 0 30.453 60.906 0.329 5.58 4 27.5 1.3 189 5 7 0 30.471 60.942 0.329 5.58 4 6.8 0.1 190 6 2 3 30.732 61.464 0.332 5.47 8 58.4 11.7 191 2 6 3 30.756 61.511 0.332 5.46 8 65.4 14.7 192 3 2 4 30.835 61.67 0.333 5.43 8 10.6 0.4 193 2 3 4 30.839 61.677 0.333 5.43 8 33.2 3.8 194 6 6 1 30.896 61.793 0.333 5.41 8 48.7 8.1 195 5 4 3 30.967 61.933 0.334 5.38 8 47.1 7.5 196 4 5 3 30.973 61.946 0.334 5.38 8 11.8 0.5 197 6 5 2 31.061 62.122 0.335 5.34 8 4.7 0.1 198 5 6 2 31.069 62.138 0.335 5.34 8 54.9 10.1 199 8 3 1 31.102 62.203 0.335 5.33 8 8.4 0.2 200 3 8 1 31.142 62.284 0.336 5.31 8 9.5 0.3 201 7 5 1 31.337 62.675 0.338 5.24 8 6.0 0.1 202 5 7 1 31.355 62.71 0.338 5.23 8 55.0 9.9 203 4 0 4 31.505 63.01 0.339 5.18 4 39.0 2.5 204 0 4 4 31.516 63.033 0.339 5.18 4 44.1 3.2 205 8 0 2 31.713 63.426 0.341 5.11 4 183.4 53.9 206 4 1 4 31.728 63.456 0.341 5.1 8 14.4 0.7 207 1 4 4 31.739 63.478 0.341 5.1 8 40.3 5.2 208 0 8 2 31.759 63.518 0.342 5.09 4 156.8 39.3 209 8 4 0 31.794 63.587 0.342 5.08 4 140.0 31.3 210 4 8 0 31.828 63.657 0.342 5.07 4 124.0 24.5 211 6 3 3 31.855 63.71 0.343 5.06 8 55.3 9.7 212 3 6 3 31.874 63.749 0.343 5.05 8 37.8 4.5 213 8 1 2 31.935 63.871 0.343 5.03 8 6.9 0.1 214 7 4 2 31.946 63.892 0.343 5.02 8 75.6 18.0 215 3 3 4 31.956 63.911 0.344 5.02 8 13.9 0.6 216 4 7 2 31.97 63.94 0.344 5.02 8 30.1 2.9 217 1 8 2 31.981 63.961 0.344 5.01 8 60.1 11.4 218 9 1 0 32.225 64.45 0.346 4.93 4 34.9 1.9 219 1 9 0 32.282 64.564 0.347 4.91 4 17.0 0.4 220 4 2 4 32.393 64.785 0.348 4.88 8 88.2 23.8 221 2 4 4 32.401 64.803 0.348 4.87 8 84.0 21.6 222 8 2 2 32.598 65.195 0.35 4.81 8 15.6 0.7 223 2 8 2 32.64 65.281 0.35 4.8 8 32.6 3.2 224 8 4 1 32.657 65.315 0.35 4.79 8 2.9 0.0 225 4 8 1 32.691 65.383 0.351 4.78 8 82.9 20.7 226 7 0 3 32.728 65.457 0.351 4.77 4 46.5 3.2 227 9 0 1 32.864 65.729 0.352 4.73 4 108.3 17.4 228 7 1 3 32.947 65.894 0.353 4.7 8 15.3 0.7 229 5 5 3 32.964 65.928 0.353 4.7 8 62.8 11.6 230 1 7 3 32.981 65.962 0.353 4.69 8 15.9 0.7 231 9 1 1 33.083 66.165 0.354 4.66 8 14.5 0.6 232 1 9 1 33.139 66.278 0.355 4.64 8 0.6 0.0 233 6 4 3 33.391 66.783 0.357 4.57 8 9.6 0.3 234 4 6 3 33.406 66.811 0.357 4.56 8 43.5 5.4 235 5 0 4 33.478 66.957 0.358 4.54 4 29.1 1.2 236 4 3 4 33.485 66.97 0.358 4.54 8 42.1 5.1 237 3 4 4 33.49 66.979 0.358 4.54 8 13.2 0.5 238 6 6 2 33.49 66.979 0.358 4.54 8 43.0 5.3 239 7 2 3 33.599 67.198 0.359 4.51 8 44.8 5.7 240 2 7 3 33.63 67.261 0.36 4.5 8 15.6 0.7 241 8 3 2 33.686 67.373 0.36 4.48 8 10.3 0.3 242 5 1 4 33.695 67.389 0.36 4.48 8 75.8 16.2 243 1 5 4 33.711 67.423 0.36 4.48 8 66.1 12.3 244 3 8 2 33.725 67.45 0.36 4.47 8 62.2 10.9 245 9 2 1 33.733 67.466 0.36 4.47 8 25.8 1.9 246 7 6 1 33.755 67.511 0.361 4.47 8 19.4 1.1 247 6 7 1 33.765 67.529 0.361 4.46 8 14.5 0.6 248 2 9 1 33.787 67.574 0.361 4.46 8 1.1 0.0 249 7 5 2 33.912 67.825 0.362 4.42 8 50.6 7.1 250 5 7 2 33.929 67.858 0.362 4.42 8 52.4 7.6 251 9 3 0 33.968 67.936 0.363 4.41 4 82.0 9.3 252 3 9 0 34.018 68.036 0.363 4.39 4 11.5 0.2 253 5 2 4 34.339 68.679 0.366 4.31 8 35.2 3.4 254 2 5 4 34.354 68.708 0.366 4.31 8 29.9 2.4 255 8 5 1 34.603 69.206 0.369 4.24 8 40.4 4.4 256 5 8 1 34.63 69.26 0.369 4.24 8 41.0 4.5 257 7 3 3 34.672 69.344 0.369 4.22 8 27.1 2.0 258 3 7 3 34.699 69.399 0.37 4.22 8 7.7 0.2 259 9 3 1 34.804 69.608 0.37 4.19 8 29.2 2.2 260 3 9 1 34.854 69.707 0.371 4.18 8 17.8 0.8 261 4 4 4 34.985 69.97 0.372 4.15 8 58.6 8.9 262 8 4 2 35.182 70.365 0.374 4.1 8 35.1 3.2 263 4 8 2 35.215 70.43 0.374 4.09 8 82.7 17.6 264 6 5 3 35.317 70.634 0.375 4.07 8 43.1 4.7 265 5 6 3 35.325 70.649 0.375 4.07 8 14.2 0.5 266 9 0 2 35.382 70.764 0.376 4.06 4 22.0 0.6 267 5 3 4 35.402 70.804 0.376 4.05 8 90.6 20.9 268 3 5 4 35.413 70.826 0.376 4.05 8 93.7 22.3 269 9 1 2 35.593 71.186 0.378 4.01 8 55.1 7.7 270 1 9 2 35.647 71.295 0.378 4.0 8 15.0 0.6 271 0 0 5 35.669 71.337 0.378 3.99 2 79.0 3.9 272 7 7 0 35.691 71.382 0.379 3.99 4 19.1 0.5 273 6 0 4 35.815 71.631 0.38 3.96 4 111.4 15.4 274 0 6 4 35.84 71.68 0.38 3.95 4 132.7 21.9 275 1 0 5 35.878 71.756 0.38 3.95 4 70.8 6.2 276 8 0 3 35.93 71.859 0.381 3.93 4 151.7 28.4 277 0 8 3 35.973 71.946 0.381 3.93 4 16.0 0.3 278 6 1 4 36.025 72.05 0.382 3.91 8 11.8 0.3 279 1 6 4 36.049 72.098 0.382 3.91 8 6.5 0.1 280 10 0 0 36.076 72.152 0.382 3.9 2 105.3 6.8 281 1 1 5 36.088 72.175 0.382 3.9 8 2.2 0.0 282 8 6 0 36.1 72.201 0.382 3.9 4 22.1 0.6 283 6 8 0 36.119 72.239 0.383 3.89 4 25.8 0.8 284 8 1 3 36.139 72.278 0.383 3.89 8 18.2 0.8 285 0 10 0 36.144 72.288 0.383 3.89 2 114.0 7.9 286 7 4 3 36.149 72.298 0.383 3.89 8 46.6 5.3 287 4 7 3 36.172 72.343 0.383 3.88 8 47.6 5.5 288 1 8 3 36.182 72.363 0.383 3.88 8 130.1 41.3 289 9 2 2 36.222 72.445 0.384 3.87 8 20.2 1.0 290 7 6 2 36.244 72.488 0.384 3.87 8 17.5 0.7 291 6 7 2 36.253 72.506 0.384 3.87 8 9.4 0.2 292 2 9 2 36.274 72.549 0.384 3.86 8 17.8 0.8 293 9 4 1 36.279 72.558 0.384 3.86 8 63.0 9.6 294 4 9 1 36.323 72.646 0.384 3.85 8 69.3 11.6 295 2 0 5 36.503 73.007 0.386 3.82 4 27.4 0.9 296 0 2 5 36.506 73.012 0.386 3.82 4 47.7 2.7 297 7 7 1 36.509 73.019 0.386 3.81 8 35.9 3.1 298 6 2 4 36.652 73.303 0.387 3.79 8 40.0 3.8 299 2 6 4 36.673 73.346 0.388 3.78 8 1.8 0.0 300 2 1 5 36.712 73.423 0.388 3.77 8 39.1 3.6 301 1 2 5 36.714 73.427 0.388 3.77 8 2.9 0.0 302 8 2 3 36.765 73.529 0.389 3.76 8 53.6 6.8 303 2 8 3 36.805 73.61 0.389 3.76 8 18.8 0.8 304 5 4 4 36.867 73.734 0.389 3.75 8 13.7 0.4 305 4 5 4 36.873 73.746 0.389 3.74 8 2.4 0.0 306 10 0 1 36.891 73.782 0.39 3.74 4 84.5 8.4 307 10 2 0 36.91 73.82 0.39 3.74 4 14.3 0.2 308 8 6 1 36.915 73.83 0.39 3.74 8 89.8 18.9 309 6 8 1 36.934 73.868 0.39 3.73 8 83.6 16.4 310 0 10 1 36.958 73.917 0.39 3.73 4 100.3 11.8 311 2 10 0 36.974 73.949 0.39 3.72 4 25.4 0.8 312 8 5 2 37.066 74.132 0.391 3.71 8 5.5 0.1 313 5 8 2 37.092 74.185 0.391 3.7 8 0.8 0.0 314 10 1 1 37.098 74.197 0.392 3.7 8 2.5 0.0 315 1 10 1 37.165 74.33 0.392 3.69 8 35.2 2.9 316 9 3 2 37.262 74.524 0.393 3.67 8 66.2 10.1 317 3 9 2 37.31 74.62 0.393 3.66 8 110.5 28.1 318 2 2 5 37.333 74.667 0.394 3.66 8 18.0 0.7 319 9 5 0 37.337 74.674 0.394 3.66 4 34.2 1.3 320 5 9 0 37.374 74.749 0.394 3.65 4 39.7 1.8 321 3 0 5 37.537 75.073 0.395 3.62 4 9.2 0.1 322 6 6 3 37.611 75.223 0.396 3.61 8 13.7 0.4 323 6 3 4 37.687 75.373 0.397 3.6 8 16.4 0.6 324 3 6 4 37.705 75.409 0.397 3.59 8 29.8 2.0 325 10 2 1 37.718 75.436 0.397 3.59 8 24.4 1.3 326 3 1 5 37.743 75.485 0.397 3.59 8 54.8 6.8 327 1 3 5 37.748 75.496 0.397 3.59 8 92.5 19.3 328 2 10 1 37.782 75.564 0.398 3.58 8 31.2 2.2 329 8 3 3 37.799 75.597 0.398 3.58 8 15.6 0.5 330 3 8 3 37.835 75.671 0.398 3.57 8 0.5 0.0 331 7 5 3 38.014 76.028 0.4 3.54 8 9.2 0.2 332 5 7 3 38.03 76.06 0.4 3.54 8 28.6 1.8 333 9 5 1 38.142 76.284 0.401 3.52 8 17.7 0.7 334 5 9 1 38.179 76.358 0.401 3.51 8 17.9 0.7 335 3 2 5 38.359 76.717 0.403 3.49 8 30.9 2.1 336 2 3 5 38.362 76.724 0.403 3.49 8 83.1 15.1 337 7 0 4 38.499 76.998 0.404 3.46 4 38.0 1.6 338 9 4 2 38.7 77.4 0.406 3.43 8 63.3 8.6 339 7 1 4 38.704 77.407 0.406 3.43 8 2.8 0.0 340 5 5 4 38.719 77.439 0.406 3.43 8 7.6 0.1 341 1 7 4 38.735 77.471 0.406 3.43 8 45.9 4.5 342 10 3 1 38.743 77.486 0.406 3.43 8 38.8 3.2 343 4 9 2 38.743 77.486 0.406 3.43 8 12.1 0.3 344 3 10 1 38.803 77.607 0.407 3.42 8 10.2 0.2 345 7 7 2 38.925 77.851 0.408 3.4 8 33.0 2.3 346 4 0 5 38.967 77.934 0.408 3.39 4 6.9 0.1 347 0 4 5 38.978 77.955 0.408 3.39 4 24.5 0.6 348 6 4 4 39.12 78.24 0.41 3.37 8 19.4 0.8 349 4 6 4 39.133 78.266 0.41 3.37 8 26.2 1.5 350 4 1 5 39.171 78.341 0.41 3.37 8 93.0 18.3 351 1 4 5 39.181 78.361 0.41 3.36 8 6.4 0.1 352 8 4 3 39.231 78.461 0.411 3.36 8 8.5 0.2 353 4 8 3 39.262 78.524 0.411 3.35 8 72.6 11.1 354 10 0 2 39.299 78.598 0.411 3.35 4 80.0 6.7 355 7 2 4 39.315 78.63 0.411 3.35 8 31.6 2.1 356 8 6 2 39.323 78.645 0.411 3.34 8 37.4 2.9 357 6 8 2 39.341 78.682 0.411 3.34 8 31.0 2.0 358 2 7 4 39.344 78.689 0.412 3.34 8 23.3 1.1 359 0 10 2 39.365 78.73 0.412 3.34 4 62.3 4.1 360 10 4 0 39.373 78.745 0.412 3.34 4 130.7 17.9 361 3 3 5 39.379 78.757 0.412 3.34 8 32.1 2.2 362 9 0 3 39.423 78.845 0.412 3.33 4 9.6 0.1 363 4 10 0 39.428 78.856 0.412 3.33 4 147.7 22.8 364 10 1 2 39.502 79.004 0.413 3.32 8 3.1 0.0 365 1 10 2 39.567 79.135 0.413 3.31 8 6.7 0.1 366 8 7 1 39.581 79.162 0.414 3.31 8 4.4 0.0 367 7 8 1 39.591 79.182 0.414 3.31 8 145.9 44.3 368 9 1 3 39.626 79.251 0.414 3.3 8 10.6 0.2 369 1 9 3 39.678 79.356 0.414 3.3 8 9.6 0.2 370 4 2 5 39.78 79.56 0.415 3.28 8 22.7 1.1 371 2 4 5 39.788 79.576 0.415 3.28 8 20.5 0.9 372 10 2 2 40.11 80.22 0.418 3.24 8 13.2 0.4 373 10 4 1 40.165 80.33 0.419 3.23 8 37.6 2.9 374 2 10 2 40.173 80.346 0.419 3.23 8 8.1 0.1 375 4 10 1 40.22 80.44 0.419 3.23 8 33.5 2.3 376 9 2 3 40.233 80.466 0.419 3.23 8 9.2 0.2 377 7 6 3 40.254 80.508 0.419 3.22 8 31.5 2.0 378 6 7 3 40.263 80.525 0.42 3.22 8 8.2 0.1 379 2 9 3 40.284 80.567 0.42 3.22 8 27.3 1.5 380 7 3 4 40.328 80.656 0.42 3.21 8 134.7 36.7 381 3 7 4 40.354 80.708 0.42 3.21 8 123.2 30.6 382 9 6 1 40.38 80.759 0.421 3.21 8 32.8 2.2 383 6 9 1 40.409 80.818 0.421 3.2 8 3.8 0.0 384 9 5 2 40.527 81.053 0.422 3.19 8 88.5 15.7 385 5 9 2 40.563 81.126 0.422 3.19 8 38.5 3.0 386 11 1 0 40.574 81.147 0.422 3.19 4 56.3 3.2 387 1 11 0 40.652 81.304 0.423 3.18 4 21.2 0.4 388 5 0 5 40.784 81.569 0.424 3.16 4 19.8 0.4 389 4 3 5 40.79 81.58 0.424 3.16 8 49.2 4.8 390 3 4 5 40.795 81.59 0.424 3.16 8 18.9 0.7 391 6 5 4 40.941 81.883 0.425 3.14 8 18.6 0.7 392 5 6 4 40.949 81.897 0.425 3.14 8 10.0 0.2 393 5 1 5 40.986 81.971 0.426 3.14 8 45.1 4.0 394 1 5 5 41.001 82.003 0.426 3.14 8 38.5 2.9 395 8 5 3 41.051 82.102 0.426 3.13 8 48.4 4.6 396 5 8 3 41.076 82.153 0.427 3.13 8 14.3 0.4 397 10 3 2 41.119 82.237 0.427 3.13 8 30.9 1.9 398 11 0 1 41.16 82.319 0.427 3.12 4 55.5 3.0 399 3 10 2 41.178 82.356 0.427 3.12 8 38.2 2.9 400 9 3 3 41.241 82.482 0.428 3.11 8 83.3 13.6 401 3 9 3 41.288 82.576 0.428 3.11 8 30.2 1.8 402 11 1 1 41.361 82.721 0.429 3.1 8 7.5 0.1 403 1 11 1 41.439 82.877 0.43 3.09 8 3.5 0.0 404 8 0 4 41.526 83.053 0.43 3.08 4 33.1 1.1 405 0 8 4 41.568 83.136 0.431 3.08 4 9.9 0.1 406 5 2 5 41.589 83.178 0.431 3.08 8 21.2 0.9 407 2 5 5 41.602 83.205 0.431 3.08 8 32.9 2.1 408 8 1 4 41.727 83.454 0.432 3.06 8 7.2 0.1 409 7 4 4 41.737 83.474 0.432 3.06 8 45.8 4.0 410 4 7 4 41.758 83.517 0.432 3.06 8 18.2 0.6 411 1 8 4 41.768 83.536 0.432 3.06 8 42.3 3.4 412 8 8 0 41.817 83.635 0.433 3.06 4 80.4 6.2 413 8 7 2 41.945 83.89 0.434 3.04 8 1.2 0.0 414 7 8 2 41.955 83.91 0.434 3.04 8 6.4 0.1 415 11 2 1 41.963 83.925 0.434 3.04 8 79.5 12.1 416 10 5 1 41.976 83.953 0.434 3.04 8 21.9 0.9 417 5 10 1 42.025 84.05 0.435 3.04 8 47.7 4.3 418 2 11 1 42.039 84.077 0.435 3.03 8 11.4 0.2 419 11 3 0 42.181 84.362 0.436 3.02 4 15.5 0.2 420 4 4 5 42.196 84.392 0.436 3.02 8 11.7 0.3 421 9 7 0 42.207 84.414 0.436 3.02 4 26.7 0.7 422 7 9 0 42.228 84.456 0.436 3.02 4 24.4 0.6 423 3 11 0 42.254 84.508 0.436 3.02 4 21.2 0.4 424 8 2 4 42.328 84.657 0.437 3.01 8 1.5 0.0 425 2 8 4 42.367 84.734 0.437 3.01 8 40.6 3.1 426 10 4 2 42.523 85.045 0.439 2.99 8 66.1 8.2 427 4 10 2 42.577 85.154 0.439 2.99 8 51.4 5.0 428 5 3 5 42.591 85.181 0.439 2.99 8 19.7 0.7 429 8 8 1 42.6 85.201 0.439 2.99 8 90.8 15.5 430 3 5 5 42.601 85.202 0.439 2.99 8 94.9 16.9 431 9 4 3 42.644 85.289 0.44 2.98 8 80.6 12.2 432 4 9 3 42.686 85.373 0.44 2.98 8 81.6 12.5 433 9 6 2 42.735 85.47 0.44 2.97 8 9.4 0.2 434 6 9 2 42.764 85.528 0.441 2.97 8 19.9 0.7 435 7 7 3 42.865 85.73 0.442 2.96 8 23.1 1.0 436 11 3 1 42.963 85.927 0.442 2.96 8 21.1 0.8 437 6 0 5 42.983 85.967 0.443 2.96 4 20.6 0.4 438 9 7 1 42.989 85.978 0.443 2.95 8 43.1 3.5 439 0 6 5 43.007 86.013 0.443 2.95 4 31.5 0.9 440 7 9 1 43.01 86.02 0.443 2.95 8 9.8 0.2 441 3 11 1 43.036 86.071 0.443 2.95 8 12.7 0.3 442 6 6 4 43.146 86.293 0.444 2.94 8 2.9 0.0 443 6 1 5 43.183 86.366 0.444 2.94 8 33.9 2.1 444 1 6 5 43.206 86.411 0.444 2.94 8 4.6 0.0 445 10 0 3 43.232 86.463 0.445 2.94 4 8.0 0.1 446 8 6 3 43.255 86.51 0.445 2.93 8 25.0 1.2 447 6 8 3 43.273 86.546 0.445 2.93 8 11.1 0.2 448 0 10 3 43.296 86.592 0.445 2.93 4 56.4 2.9 449 8 3 4 43.328 86.656 0.445 2.93 8 13.9 0.4 450 3 8 4 43.363 86.727 0.446 2.93 8 4.7 0.0 451 10 6 0 43.394 86.789 0.446 2.92 4 50.1 2.3 452 10 1 3 43.431 86.862 0.446 2.92 8 27.8 1.4 453 6 10 0 43.436 86.872 0.446 2.92 4 4.9 0.0 454 1 10 3 43.495 86.99 0.447 2.92 8 6.3 0.1 455 11 0 2 43.508 87.016 0.447 2.92 4 21.4 0.4 456 7 5 4 43.537 87.074 0.447 2.91 8 38.9 2.8 457 5 7 4 43.553 87.105 0.447 2.91 8 7.9 0.1 458 11 1 2 43.708 87.415 0.449 2.9 8 15.4 0.4 459 6 2 5 43.782 87.564 0.449 2.9 8 64.1 7.5 460 1 11 2 43.785 87.57 0.449 2.9 8 19.4 0.7 461 2 6 5 43.803 87.605 0.449 2.9 8 23.0 1.0 462 5 4 5 43.988 87.977 0.451 2.89 8 29.7 1.6 463 4 5 5 43.994 87.989 0.451 2.88 8 18.2 0.6 464 10 2 3 44.03 88.06 0.451 2.88 8 12.2 0.3 465 2 10 3 44.092 88.184 0.452 2.88 8 33.8 2.1 466 10 6 1 44.174 88.349 0.452 2.87 8 3.3 0.0 467 6 10 1 44.216 88.431 0.453 2.87 8 20.3 0.7 468 11 2 2 44.306 88.612 0.453 2.87 8 25.6 1.2 469 10 5 2 44.32 88.639 0.454 2.87 8 12.9 0.3 470 11 4 1 44.36 88.72 0.454 2.86 8 56.3 5.7 471 5 10 2 44.368 88.736 0.454 2.86 8 47.3 4.0 472 2 11 2 44.382 88.763 0.454 2.86 8 27.3 1.3 473 0 0 6 44.404 88.808 0.454 2.86 2 7.7 0.0 474 4 11 1 44.428 88.856 0.454 2.86 8 34.2 2.1 475 9 5 3 44.441 88.882 0.454 2.86 8 20.0 0.7 476 5 9 3 44.477 88.954 0.455 2.86 8 26.6 1.3 477 1 0 6 44.603 89.206 0.456 2.85 4 42.6 1.6 478 8 4 4 44.724 89.448 0.457 2.84 8 8.8 0.1 479 4 8 4 44.755 89.51 0.457 2.84 8 37.5 2.5 480 6 3 5 44.779 89.558 0.457 2.84 8 48.3 4.2 481 3 6 5 44.796 89.593 0.457 2.84 8 38.0 2.6 482 1 1 6 44.802 89.604 0.457 2.84 8 23.5 1.0 483 9 0 4 44.912 89.825 0.458 2.83 4 36.2 1.2 484 8 8 2 44.941 89.882 0.459 2.83 8 34.9 2.2 485 12 0 0 44.961 89.923 0.459 2.83 2 7.0 0.0 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 4.781 9.562 9.24209 56.7 11.4 11.5 5.6 2 0 0 1 6.697 13.394 6.6051 199.0 39.9 40.4 5.6 3 2 0 0 6.764 13.527 6.54045 258.3 51.8 52.4 5.6 4 1 0 1 7.507 15.013 5.89608 234.3 47.0 47.5 5.6 5 1 1 1 8.241 16.482 5.3738 28.1 5.6 5.7 5.6 6 2 0 1 9.54 19.081 4.64749 213.8 42.9 43.3 5.6 7 2 2 0 9.595 19.191 4.62104 265.8 53.3 53.8 5.6 8 1 2 1 10.138 20.276 4.37611 214.4 43.0 43.3 5.6 9 1 3 0 10.748 21.496 4.13051 163.0 32.7 32.9 5.6 10 2 2 1 11.738 23.476 3.78639 27.3 5.5 5.5 5.6 11 1 3 1 12.706 25.412 3.50211 321.2 64.4 64.7 5.6 12 4 0 0 13.624 27.247 3.27023 54.3 10.9 10.9 5.6 13 1 0 2 13.919 27.839 3.20207 177.8 35.6 35.7 5.6 14 2 3 1 14.031 28.062 3.17714 195.4 39.2 39.3 5.6 15 3 3 0 14.48 28.959 3.0807 12.3 2.5 2.5 5.6 16 0 2 2 15.151 30.303 2.94707 315.8 63.3 63.4 5.6 17 4 0 1 15.238 30.476 2.93069 92.3 18.5 18.5 5.6 18 2 4 0 15.289 30.578 2.92118 67.3 13.5 13.5 5.6 19 1 2 2 15.541 31.081 2.87501 7.6 1.5 1.5 5.6 20 1 4 1 15.645 31.291 2.85625 498.9 100.0 100.0 5.6 21 3 3 1 16.015 32.031 2.79195 71.4 14.3 14.3 5.6 22 4 2 1 16.744 33.487 2.67375 401.3 80.4 80.3 5.7 23 1 3 2 17.375 34.75 2.57942 128.6 25.8 25.7 5.7 24 1 5 0 17.501 35.003 2.56138 27.5 5.5 5.5 5.7 25 3 2 2 18.389 36.779 2.44167 9.4 1.9 1.9 5.7 26 3 4 1 18.48 36.959 2.43015 84.8 17.0 16.9 5.7 27 4 0 2 19.359 38.718 2.32374 5.8 1.2 1.1 5.7 28 4 4 0 19.474 38.948 2.31052 11.7 2.3 2.3 5.7 29 4 1 2 19.675 39.351 2.28781 22.8 4.6 4.5 5.7 30 5 2 1 19.751 39.503 2.27934 19.4 3.9 3.9 5.7 31 3 3 2 19.995 39.989 2.25273 137.8 27.6 27.4 5.7 32 3 5 0 20.107 40.214 2.24068 19.0 3.8 3.8 5.7 33 0 0 3 20.479 40.957 2.2017 7.5 1.5 1.5 5.7 34 4 2 2 20.6 41.201 2.18925 137.5 27.6 27.3 5.7 35 6 0 0 20.69 41.38 2.18015 25.8 5.2 5.1 5.7 36 0 6 0 20.725 41.451 2.17662 98.5 19.8 19.6 5.7 37 1 0 3 20.78 41.56 2.17116 7.1 1.4 1.4 5.7 38 3 5 1 21.285 42.571 2.12191 37.0 7.4 7.3 5.7 39 2 0 3 21.663 43.326 2.08664 35.8 7.2 7.1 5.7 40 2 6 0 21.899 43.798 2.06525 38.4 7.7 7.6 5.7 41 1 2 3 21.955 43.91 2.06026 19.9 4.0 3.9 5.7 42 1 5 2 22.369 44.739 2.02399 7.5 1.5 1.5 5.7 43 2 2 3 22.801 45.603 1.98763 14.9 3.0 3.0 5.7 44 6 2 1 22.974 45.948 1.97348 13.4 2.7 2.6 5.7 45 3 0 3 23.075 46.149 1.96536 9.8 2.0 1.9 5.7 46 5 2 2 23.185 46.37 1.95649 45.4 9.1 9.0 5.7 47 4 5 1 23.268 46.536 1.94991 24.7 5.0 4.9 5.7 48 1 3 3 23.357 46.714 1.94292 21.1 4.2 4.2 5.7 49 3 2 3 24.161 48.321 1.88196 49.3 9.9 9.7 5.7 50 6 3 1 24.33 48.661 1.86963 13.4 2.7 2.6 5.7 51 0 4 3 24.959 49.918 1.82543 62.8 12.6 12.4 5.7 52 0 6 2 25.077 50.154 1.8174 5.8 1.2 1.1 5.7 53 6 4 0 25.141 50.282 1.81309 87.2 17.5 17.1 5.8 54 4 1 3 25.205 50.411 1.80875 61.5 12.3 12.1 5.8 55 7 0 1 25.365 50.73 1.79812 33.2 6.7 6.5 5.8 56 5 5 1 25.641 51.282 1.78003 24.4 4.9 4.8 5.8 57 2 4 3 25.983 51.965 1.75823 12.0 2.4 2.4 5.8 58 6 2 2 26.071 52.142 1.75269 21.8 4.4 4.3 5.8 59 6 4 1 26.14 52.279 1.74841 8.9 1.8 1.7 5.8 60 7 2 1 26.38 52.76 1.7336 16.1 3.2 3.2 5.8 61 7 3 0 26.652 53.305 1.71717 50.6 10.1 9.9 5.8 62 3 7 0 26.684 53.369 1.71525 32.0 6.4 6.3 5.8 63 5 0 3 27.211 54.421 1.68455 16.6 3.3 3.2 5.8 64 3 6 2 27.334 54.668 1.67752 34.8 7.0 6.8 5.8 65 1 5 3 27.474 54.948 1.66965 20.0 4.0 3.9 5.8 66 0 0 4 27.806 55.612 1.65128 45.1 9.0 8.8 5.8 67 2 5 3 28.196 56.391 1.63028 40.6 8.1 7.9 5.8 68 7 0 2 28.269 56.538 1.62639 8.6 1.7 1.7 5.8 69 6 5 1 28.344 56.688 1.62244 44.1 8.8 8.6 5.8 70 5 5 2 28.526 57.052 1.61297 81.9 16.4 16.0 5.8 71 6 4 2 28.99 57.98 1.58933 13.1 2.6 2.6 5.8 72 8 0 1 29.033 58.065 1.5872 20.2 4.0 3.9 5.8 73 0 8 1 29.081 58.162 1.58478 16.2 3.2 3.2 5.8 74 7 2 2 29.215 58.429 1.57817 5.5 1.1 1.1 5.8 75 1 8 1 29.315 58.629 1.57327 38.6 7.7 7.5 5.8 76 3 5 3 29.373 58.745 1.57044 23.8 4.8 4.6 5.8 77 6 0 3 29.816 59.633 1.54916 15.3 3.1 3.0 5.8 78 6 6 0 30.005 60.009 1.54035 5.4 1.1 1.1 5.8 79 1 6 3 30.073 60.146 1.53717 14.8 3.0 2.9 5.8 80 1 3 4 30.157 60.314 1.53329 48.1 9.6 9.3 5.8 81 2 6 3 30.756 61.511 1.50628 26.4 5.3 5.1 5.8 82 6 6 1 30.896 61.793 1.5001 8.1 1.6 1.6 5.8 83 5 4 3 30.967 61.933 1.49703 8.0 1.6 1.5 5.8 84 5 6 2 31.069 62.138 1.4926 10.1 2.0 2.0 5.8 85 5 7 1 31.355 62.71 1.48035 9.9 2.0 1.9 5.8 86 0 4 4 31.516 63.033 1.47353 5.6 1.1 1.1 5.9 87 8 0 2 31.713 63.426 1.46535 59.8 12.0 11.5 5.9 88 0 8 2 31.759 63.518 1.46344 39.3 7.9 7.6 5.9 89 8 4 0 31.794 63.587 1.46201 31.3 6.3 6.0 5.9 90 4 8 0 31.828 63.657 1.46059 34.2 6.8 6.6 5.9 91 7 4 2 31.946 63.892 1.45577 21.5 4.3 4.1 5.9 92 1 8 2 31.981 63.961 1.45437 11.4 2.3 2.2 5.9 93 4 2 4 32.393 64.785 1.43784 45.4 9.1 8.8 5.9 94 4 8 1 32.691 65.383 1.42614 20.7 4.1 4.0 5.9 95 9 0 1 32.864 65.729 1.41947 17.4 3.5 3.3 5.9 96 5 5 3 32.964 65.928 1.41566 12.4 2.5 2.4 5.9 97 4 6 3 33.406 66.811 1.39908 5.4 1.1 1.0 5.9 98 6 6 2 33.49 66.979 1.39597 12.0 2.4 2.3 5.9 99 7 2 3 33.599 67.198 1.39197 5.7 1.1 1.1 5.9 100 5 1 4 33.695 67.389 1.38847 28.5 5.7 5.5 5.9 101 3 8 2 33.725 67.45 1.38738 12.8 2.6 2.4 5.9 102 5 7 2 33.929 67.858 1.38002 14.8 3.0 2.8 5.9 103 9 3 0 33.968 67.936 1.37862 9.3 1.9 1.8 5.9 104 5 2 4 34.339 68.679 1.36551 5.8 1.2 1.1 5.9 105 5 8 1 34.63 69.26 1.35548 8.8 1.8 1.7 5.9 106 4 4 4 34.985 69.97 1.34345 8.9 1.8 1.7 5.9 107 4 8 2 35.215 70.43 1.33579 17.6 3.5 3.4 5.9 108 6 5 3 35.317 70.634 1.33243 5.3 1.1 1.0 5.9 109 3 5 4 35.413 70.826 1.3293 43.2 8.7 8.2 5.9 110 9 1 2 35.593 71.186 1.32345 7.7 1.5 1.5 5.9 111 0 6 4 35.84 71.68 1.31554 37.3 7.5 7.1 5.9 112 1 0 5 35.878 71.756 1.31433 6.2 1.2 1.2 5.9 113 8 0 3 35.93 71.859 1.3127 28.4 5.7 5.4 5.9 114 10 0 0 36.076 72.152 1.30809 7.4 1.5 1.4 5.9 115 0 10 0 36.144 72.288 1.30597 18.8 3.8 3.6 5.9 116 1 8 3 36.182 72.363 1.30479 41.3 8.3 7.8 5.9 117 9 4 1 36.279 72.558 1.30177 9.6 1.9 1.8 6.0 118 4 9 1 36.323 72.646 1.30041 11.6 2.3 2.2 6.0 119 7 7 1 36.509 73.019 1.29469 5.8 1.2 1.1 6.0 120 8 2 3 36.765 73.529 1.28695 6.8 1.4 1.3 6.0 121 6 8 1 36.934 73.868 1.28189 55.8 11.2 10.6 6.0 122 9 3 2 37.262 74.524 1.27223 10.1 2.0 1.9 6.0 123 3 9 2 37.31 74.62 1.27082 30.2 6.1 5.7 6.0 124 1 3 5 37.748 75.496 1.25824 26.0 5.2 4.9 6.0 125 2 3 5 38.362 76.724 1.24113 17.2 3.4 3.2 6.0 126 9 4 2 38.7 77.4 1.23196 8.8 1.8 1.7 6.0 127 1 7 4 38.735 77.471 1.23102 8.1 1.6 1.5 6.0 128 4 1 5 39.171 78.341 1.21951 18.4 3.7 3.4 6.0 129 4 8 3 39.262 78.524 1.21712 11.1 2.2 2.1 6.0 130 10 0 2 39.299 78.598 1.21617 11.8 2.4 2.2 6.0 131 10 4 0 39.373 78.745 1.21426 27.3 5.5 5.1 6.0 132 4 10 0 39.428 78.856 1.21283 22.8 4.6 4.3 6.0 133 7 8 1 39.591 79.182 1.20866 44.3 8.9 8.3 6.0 134 7 3 4 40.328 80.656 1.19024 67.3 13.5 12.6 6.1 135 9 5 2 40.527 81.053 1.18541 15.7 3.2 2.9 6.1 136 11 1 0 40.574 81.147 1.18427 6.1 1.2 1.1 6.1 137 4 3 5 40.79 81.58 1.17908 5.5 1.1 1.0 6.1 138 5 1 5 40.986 81.971 1.17444 6.9 1.4 1.3 6.1 139 8 5 3 41.051 82.102 1.1729 5.0 1.0 0.9 6.1 140 11 0 1 41.16 82.319 1.17036 5.9 1.2 1.1 6.1 141 9 3 3 41.241 82.482 1.16846 13.6 2.7 2.5 6.1 142 8 8 0 41.817 83.635 1.15526 6.2 1.2 1.1 6.1 143 11 2 1 41.963 83.925 1.152 13.0 2.6 2.4 6.1 144 10 4 2 42.523 85.045 1.13967 8.2 1.6 1.5 6.1 145 3 5 5 42.601 85.202 1.13797 38.1 7.6 7.0 6.1 146 9 4 3 42.644 85.289 1.13704 12.2 2.4 2.2 6.1 147 4 9 3 42.686 85.373 1.13613 12.5 2.5 2.3 6.1 148 6 2 5 43.782 87.564 1.11326 9.1 1.8 1.7 6.2 149 11 4 1 44.36 88.72 1.10171 11.1 2.2 2.0 6.2 150 6 3 5 44.779 89.558 1.09357 10.2 2.1 1.9 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |