Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** PUNKARUAIVITE 1, DN LiTi(2)[Si(4)O(11)(OH)](2).H(2)O Monoclinic C 2/c Z = 4 C2/c 19 .4 .12 Ref.Str.: Yakovenchuk V.N., Ivanyuk G.Y., Pakhomovsky Y.A., Selivanova E.A., Menshikov Y.P., Korchak J.A., Krivovichev S.V., Spiridonova D.V., Zalkind O.A. (2010) * Canad. Mineral., 48, 41-50 R: from Khibiny and Lovozero alkaline massifs, Kola Peninsula, Russia. N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 26.688 alpha = 90.0 b = 8.7568 beta = 91.19 c = 5.2188 gamma = 90.0 Unit cell volume (cub. angs.) = 1219.38 Molar volume ( cub.cm/mol.) = 183.62 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0 0.518 0.25 0.0 Li = 1.00 2 0.1662 0.1048 0.892 0.0 Ti = 1.00 3 0.0887 0.6008 0.5131 0.0 Si = 1.00 4 0.2685 0.0845 0.2283 0.0 Si = 1.00 5 0.2076 0.069 0.216 0.0 O = 1.00 6 0.1295 0.0614 0.5811 0.0 OH = 1.00 7 0.287 0.2594 0.2216 0.0 O = 1.00 8 0.2907 0.9939 0.9859 0.0 O = 1.00 9 0.1214 0.7493 0.5087 0.0 O = 1.00 10 0.0314 0.6339 0.507 0.0 O = 0.5 , H(2)O = 0.5 11 0.1012 0.5048 0.767 0.0 O = 1.00 12 0.0323 0.109 0.52 0.0 H(2)O = 0.5 , H(2)O = 0.0 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0 0.518 0.25 2 2 0.1662 0.1048 0.892 3 3 0.0887 0.6008 0.5131 4 4 0.2685 0.0845 0.2283 5 5 0.2076 0.069 0.216 6 6 0.1295 0.0614 0.5811 7 7 0.287 0.2594 0.2216 8 8 0.2907 0.9939 0.9859 9 9 0.1214 0.7493 0.5087 10 10 0.0314 0.6339 0.507 11 11 0.1012 0.5048 0.767 12 12 0.0323 0.109 0.52 13 1 0.0 0.482 0.75 14 2 0.8338 0.8952 0.108 15 3 0.9113 0.3992 0.4869 16 4 0.7315 0.9155 0.7717 17 5 0.7924 0.931 0.784 18 6 0.8705 0.9386 0.4189 19 7 0.713 0.7406 0.7784 20 8 0.7093 0.0061 0.0141 21 9 0.8786 0.2507 0.4913 22 10 0.9686 0.3661 0.493 23 11 0.8988 0.4952 0.233 24 12 0.9677 0.891 0.48 25 2 0.1662 0.8952 0.392 26 3 0.0887 0.3992 0.0131 27 4 0.2685 0.9155 0.7283 28 5 0.2076 0.931 0.716 29 6 0.1295 0.9386 0.0811 30 7 0.287 0.7406 0.7216 31 8 0.2907 0.0061 0.4859 32 9 0.1214 0.2507 0.0087 33 10 0.0314 0.3661 0.007 34 11 0.1012 0.4952 0.267 35 12 0.0323 0.891 0.02 36 2 0.8338 0.1048 0.608 37 3 0.9113 0.6008 0.9869 38 4 0.7315 0.0845 0.2717 39 5 0.7924 0.069 0.284 40 6 0.8705 0.0614 0.9189 41 7 0.713 0.2594 0.2784 42 8 0.7093 0.9939 0.5141 43 9 0.8786 0.7493 0.9913 44 10 0.9686 0.6339 0.993 45 11 0.8988 0.5048 0.733 46 12 0.9677 0.109 0.98 47 1 0.5 0.982 0.75 48 2 0.6662 0.3952 0.392 49 3 0.5887 0.8992 0.0131 50 4 0.7685 0.4155 0.7283 51 5 0.7076 0.431 0.716 52 6 0.6295 0.4386 0.0811 53 7 0.787 0.2406 0.7216 54 8 0.7907 0.5061 0.4859 55 9 0.6214 0.7507 0.0087 56 10 0.5314 0.8661 0.007 57 11 0.6012 0.9952 0.267 58 12 0.5323 0.391 0.02 59 1 0.5 0.018 0.25 60 2 0.3338 0.6048 0.608 61 3 0.4113 0.1008 0.9869 62 4 0.2315 0.5845 0.2717 63 5 0.2924 0.569 0.284 64 6 0.3705 0.5614 0.9189 65 7 0.213 0.7594 0.2784 66 8 0.2093 0.4939 0.5141 67 9 0.3786 0.2493 0.9913 68 10 0.4686 0.1339 0.993 69 11 0.3988 0.0048 0.733 70 12 0.4677 0.609 0.98 71 2 0.6662 0.6048 0.892 72 3 0.5887 0.1008 0.5131 73 4 0.7685 0.5845 0.2283 74 5 0.7076 0.569 0.216 75 6 0.6295 0.5614 0.5811 76 7 0.787 0.7594 0.2216 77 8 0.7907 0.4939 0.9859 78 9 0.6214 0.2493 0.5087 79 10 0.5314 0.1339 0.507 80 11 0.6012 0.0048 0.767 81 12 0.5323 0.609 0.52 82 2 0.3338 0.3952 0.108 83 3 0.4113 0.8992 0.4869 84 4 0.2315 0.4155 0.7717 85 5 0.2924 0.431 0.784 86 6 0.3705 0.4386 0.4189 87 7 0.213 0.2406 0.7784 88 8 0.2093 0.5061 0.0141 89 9 0.3786 0.7507 0.4913 90 10 0.4686 0.8661 0.493 91 11 0.3988 0.9952 0.233 92 12 0.4677 0.391 0.48 X-ray density (g/cm cub.) = 2.51 MU (1/cm) = 161.014 Mass attenuation coefficient (cm**2/g) = 64.124 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Li 2.616 4 1.8667 10 2.0307 10 2.0307 10 1.8667 10 2 Ti 2.736 6 2.0251 5 1.9157 6 2.1032 5 2.0226 6 1.8606 9 1.8326 7 3 Si 2.268 4 1.5668 9 1.5556 10 1.5987 11 1.623 11 4 Si 2.268 4 1.6319 5 1.6097 7 1.6159 8 1.6112 8 5 O 3.432 11 2.8538 6 2.696 7 2.6281 8 2.8756 5 2.8756 5 2.4664 6 2.6608 8 2.9816 9 2.7341 7 3.2979 7 2.7401 7 6 OH 3.48 9 2.8538 5 2.7668 9 2.6399 12 2.4664 5 2.8223 6 2.8223 6 2.7918 9 3.4193 9 2.8975 7 7 O 3.432 11 2.696 5 2.6331 8 2.6128 8 2.7341 5 3.3135 8 2.7481 9 3.2979 5 2.7401 5 2.8975 6 3.0142 7 3.1698 8 8 O 3.432 11 2.6281 5 2.6331 7 2.6608 5 2.6128 7 2.6116 8 2.6116 8 3.3135 7 3.2405 9 3.1983 11 3.1698 7 3.1351 11 9 O 3.432 9 2.7668 6 2.6057 10 2.5927 11 2.9816 5 3.4193 6 2.7918 6 2.6086 11 2.7481 7 3.2405 8 10 O ,H(2)O 3.6 11 2.6057 9 2.5464 11 2.8825 10 2.8229 12 3.5083 10 3.5083 10 2.5712 11 3.4977 12 3.3958 12 3.0689 10 3.1334 10 11 O 3.432 8 2.5927 9 2.5464 10 2.6086 9 2.5712 10 2.6108 11 2.6108 11 3.1983 8 3.1351 8 12 H(2)O,H(2)O 3.6 9 2.6399 6 2.8229 10 2.5778 12 3.3958 10 3.4977 10 3.2331 12 3.2331 12 2.9845 12 3.273 12 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 2 0 0 3.31 6.62 0.037 596.96 2 195.1 3055.7 2 1 1 0 5.312 10.624 0.06 230.37 4 55.4 190.5 3 4 0 0 6.631 13.262 0.075 147.03 2 54.7 59.2 4 3 1 0 7.091 14.182 0.08 128.29 4 136.0 638.8 5 5 1 0 9.732 19.463 0.11 67.08 4 93.1 156.5 6 6 0 0 9.975 19.949 0.112 63.75 2 27.9 6.7 7 1 1 -1 10.006 20.012 0.113 63.33 4 185.5 586.4 8 1 1 1 10.065 20.13 0.113 62.57 4 99.6 166.9 9 0 2 0 10.133 20.265 0.114 61.71 2 198.9 328.4 10 2 2 0 10.67 21.341 0.12 55.43 4 62.3 57.8 11 3 1 -1 11.014 22.029 0.124 51.89 4 13.1 2.4 12 3 1 1 11.175 22.351 0.126 50.35 4 178.5 431.6 13 4 2 0 12.148 24.296 0.137 42.29 4 5.0 0.3 14 7 1 0 12.732 25.465 0.143 38.31 4 213.8 471.1 15 5 1 -1 12.853 25.706 0.144 37.56 4 48.9 24.2 16 5 1 1 13.084 26.169 0.147 36.17 4 113.6 125.5 17 0 2 1 13.277 26.554 0.149 35.07 4 9.0 0.8 18 8 0 0 13.353 26.706 0.15 34.65 2 22.6 2.4 19 2 2 -1 13.654 27.308 0.153 33.05 4 26.7 6.4 20 2 2 1 13.742 27.484 0.154 32.6 4 103.7 94.4 21 6 2 0 14.293 28.587 0.16 29.98 4 34.0 9.3 22 4 2 -1 14.814 29.628 0.166 27.78 4 355.1 942.1 23 4 2 1 14.977 29.954 0.168 27.14 4 64.6 30.5 24 7 1 -1 15.244 30.488 0.171 26.13 4 13.2 1.2 25 1 3 0 15.395 30.789 0.172 25.58 4 18.9 2.5 26 7 1 1 15.521 31.042 0.174 25.13 4 31.5 6.7 27 9 1 0 15.921 31.841 0.178 23.79 4 216.8 300.9 28 3 3 0 16.125 32.251 0.18 23.15 4 96.5 58.0 29 6 2 -1 16.607 33.214 0.186 21.72 4 111.2 72.2 30 10 0 0 16.779 33.559 0.187 21.24 2 95.3 25.9 31 6 2 1 16.828 33.656 0.188 21.1 4 144.0 117.7 32 8 2 0 16.877 33.755 0.188 20.97 4 12.4 0.9 33 0 0 2 17.173 34.346 0.192 20.19 2 76.8 16.0 34 2 0 -2 17.438 34.876 0.195 19.53 2 115.1 34.8 35 5 3 0 17.505 35.01 0.195 19.36 4 45.2 10.6 36 2 0 2 17.579 35.158 0.196 19.19 2 234.0 141.3 37 1 3 -1 17.666 35.331 0.197 18.98 4 107.3 58.8 38 1 3 1 17.701 35.401 0.197 18.9 4 33.9 5.8 39 1 1 -2 17.991 35.981 0.2 18.24 4 46.4 10.6 40 9 1 -1 17.995 35.991 0.201 18.23 4 3.6 0.1 41 1 1 2 18.059 36.119 0.201 18.09 4 22.4 2.4 42 3 3 -1 18.282 36.564 0.204 17.61 4 41.1 8.0 43 9 1 1 18.304 36.607 0.204 17.56 4 25.6 3.1 44 4 0 -2 18.349 36.697 0.204 17.47 2 27.8 1.8 45 3 3 1 18.384 36.767 0.205 17.39 4 69.2 22.4 46 3 1 -2 18.564 37.128 0.207 17.02 4 15.2 1.1 47 4 0 2 18.618 37.236 0.207 16.91 2 257.5 150.9 48 3 1 2 18.764 37.529 0.209 16.63 4 12.8 0.7 49 8 2 -1 18.876 37.752 0.21 16.41 4 33.7 5.0 50 8 2 1 19.139 38.279 0.213 15.91 4 131.4 73.9 51 11 1 0 19.239 38.478 0.214 15.73 4 15.6 1.0 52 7 3 0 19.413 38.826 0.216 15.42 4 18.0 1.3 53 5 3 -1 19.496 38.992 0.217 15.28 4 11.0 0.5 54 5 3 1 19.657 39.313 0.218 15.0 4 12.5 0.6 55 5 1 -2 19.731 39.463 0.219 14.88 4 42.7 7.3 56 10 2 0 19.759 39.518 0.219 14.83 4 48.2 9.3 57 6 0 -2 19.828 39.656 0.22 14.72 2 31.2 1.9 58 5 1 2 20.048 40.096 0.223 14.36 4 99.4 38.2 59 0 2 2 20.102 40.205 0.223 14.27 4 25.3 2.5 60 6 0 2 20.206 40.413 0.224 14.11 2 88.8 15.0 61 12 0 0 20.269 40.537 0.225 14.01 2 26.3 1.3 62 2 2 -2 20.334 40.669 0.226 13.91 4 27.0 2.7 63 2 2 2 20.458 40.917 0.227 13.73 4 33.1 4.1 64 0 4 0 20.601 41.202 0.228 13.51 2 104.5 19.8 65 2 4 0 20.889 41.778 0.231 13.1 4 35.9 4.6 66 11 1 -1 21.0 42.0 0.233 12.95 4 49.8 8.7 67 4 2 -2 21.138 42.277 0.234 12.76 4 33.3 3.8 68 7 3 -1 21.222 42.444 0.235 12.65 4 159.4 86.4 69 11 1 1 21.331 42.662 0.236 12.5 4 34.2 3.9 70 4 2 2 21.378 42.756 0.237 12.44 4 35.9 4.3 71 7 1 -2 21.412 42.824 0.237 12.4 4 15.6 0.8 72 7 3 1 21.431 42.863 0.237 12.37 4 5.2 0.1 73 10 2 -1 21.499 42.999 0.238 12.28 4 150.2 74.5 74 4 4 0 21.735 43.471 0.24 11.98 4 11.1 0.4 75 9 3 0 21.736 43.472 0.24 11.98 4 8.2 0.2 76 8 0 -2 21.781 43.562 0.241 11.93 2 106.8 18.3 77 10 2 1 21.795 43.59 0.241 11.91 4 74.8 17.9 78 7 1 2 21.826 43.652 0.241 11.87 4 196.4 123.2 79 8 0 2 22.248 44.495 0.246 11.37 2 58.2 5.2 80 0 4 1 22.431 44.862 0.248 11.16 4 47.8 6.9 81 6 2 -2 22.464 44.929 0.248 11.13 4 44.7 6.0 82 2 4 -1 22.672 45.344 0.25 10.9 4 55.9 9.2 83 13 1 0 22.672 45.345 0.25 10.9 4 47.1 6.5 84 2 4 1 22.729 45.458 0.251 10.84 4 108.4 34.2 85 6 2 2 22.807 45.613 0.252 10.75 4 23.0 1.5 86 12 2 0 22.863 45.727 0.252 10.69 4 54.5 8.6 87 6 4 0 23.09 46.18 0.255 10.46 4 72.5 14.8 88 1 3 -2 23.366 46.732 0.257 10.18 4 122.3 40.9 89 9 3 -1 23.37 46.74 0.257 10.17 4 152.4 63.6 90 1 3 2 23.422 46.843 0.258 10.12 4 12.8 0.4 91 4 4 -1 23.439 46.878 0.258 10.11 4 194.8 103.2 92 9 1 -2 23.518 47.037 0.259 10.03 4 45.1 5.5 93 4 4 1 23.55 47.1 0.259 10.0 4 49.4 6.6 94 9 3 1 23.62 47.239 0.26 9.93 4 44.9 5.4 95 3 3 -2 23.831 47.663 0.262 9.73 4 62.4 10.2 96 14 0 0 23.839 47.677 0.262 9.73 2 19.3 0.5 97 3 3 2 23.996 47.991 0.264 9.58 4 21.0 1.1 98 9 1 2 24.013 48.026 0.264 9.57 4 18.7 0.9 99 10 0 -2 24.119 48.238 0.265 9.47 2 94.8 11.4 100 13 1 -1 24.203 48.406 0.266 9.4 4 142.1 51.0 101 8 2 -2 24.246 48.492 0.267 9.36 4 118.5 35.3 102 11 3 0 24.387 48.773 0.268 9.24 4 45.4 5.1 103 12 2 -1 24.398 48.796 0.268 9.23 4 21.0 1.1 104 13 1 1 24.553 49.107 0.27 9.1 4 9.5 0.2 105 10 0 2 24.658 49.316 0.271 9.01 2 127.4 19.7 106 8 2 2 24.676 49.352 0.271 8.99 4 51.0 6.3 107 6 4 -1 24.694 49.389 0.271 8.98 4 119.5 34.5 108 12 2 1 24.72 49.44 0.271 8.96 4 122.0 35.9 109 5 3 -2 24.796 49.591 0.272 8.89 4 132.8 42.2 110 6 4 1 24.854 49.708 0.273 8.85 4 29.9 2.1 111 8 4 0 24.89 49.78 0.273 8.82 4 73.1 12.7 112 5 3 2 25.061 50.122 0.275 8.68 4 38.4 3.4 113 11 3 -1 25.866 51.732 0.283 8.08 4 154.8 52.1 114 11 1 -2 25.978 51.956 0.284 8.0 4 36.2 2.8 115 11 3 1 26.149 52.298 0.286 7.88 4 90.9 17.5 116 1 5 0 26.153 52.305 0.286 7.88 4 42.0 3.7 117 14 2 0 26.154 52.309 0.286 7.88 4 2.6 0.0 118 7 3 -2 26.218 52.436 0.287 7.83 4 43.9 4.1 119 15 1 0 26.223 52.447 0.287 7.83 4 68.0 9.7 120 8 4 -1 26.387 52.774 0.288 7.72 4 48.9 5.0 121 10 2 -2 26.417 52.833 0.289 7.7 4 51.6 5.5 122 11 1 2 26.54 53.08 0.29 7.62 4 156.8 50.4 123 7 3 2 26.574 53.148 0.29 7.6 4 2.1 0.0 124 8 4 1 26.59 53.18 0.291 7.59 4 81.7 13.6 125 3 5 0 26.632 53.265 0.291 7.56 4 127.0 32.8 126 12 0 -2 26.775 53.55 0.292 7.47 2 22.1 0.5 127 1 1 -3 26.864 53.728 0.293 7.41 4 0.5 0.0 128 10 2 2 26.922 53.844 0.294 7.38 4 37.7 2.8 129 1 1 3 26.939 53.879 0.294 7.36 4 38.8 3.0 130 10 4 0 27.073 54.146 0.295 7.28 4 132.5 34.4 131 3 1 -3 27.26 54.521 0.297 7.17 4 60.5 7.1 132 13 3 0 27.309 54.617 0.298 7.14 4 20.3 0.8 133 0 4 2 27.344 54.687 0.298 7.12 4 85.1 13.9 134 12 0 2 27.375 54.751 0.298 7.1 2 17.5 0.3 135 3 1 3 27.484 54.967 0.3 7.04 4 147.3 41.1 136 16 0 0 27.51 55.019 0.3 7.02 2 205.6 39.9 137 2 4 -2 27.527 55.055 0.3 7.01 4 44.2 3.7 138 14 2 -1 27.528 55.056 0.3 7.01 4 55.1 5.7 139 5 5 0 27.574 55.149 0.3 6.98 4 87.2 14.3 140 15 1 -1 27.583 55.165 0.301 6.98 4 43.8 3.6 141 2 4 2 27.626 55.253 0.301 6.95 4 175.1 57.4 142 1 5 -1 27.687 55.374 0.302 6.92 4 3.6 0.0 143 1 5 1 27.712 55.423 0.302 6.91 4 12.3 0.3 144 14 2 1 27.873 55.746 0.303 6.82 4 49.1 4.4 145 15 1 1 27.951 55.903 0.304 6.77 4 87.9 14.1 146 9 3 -2 28.051 56.101 0.305 6.72 4 26.6 1.3 147 5 1 -3 28.115 56.23 0.306 6.68 4 12.2 0.3 148 3 5 -1 28.124 56.249 0.306 6.68 4 22.7 0.9 149 4 4 -2 28.172 56.344 0.306 6.65 4 61.1 6.7 150 3 5 1 28.197 56.395 0.307 6.64 4 9.3 0.2 151 4 4 2 28.366 56.733 0.308 6.55 4 122.3 26.4 152 0 2 3 28.46 56.921 0.309 6.5 4 208.5 76.1 153 10 4 -1 28.465 56.93 0.309 6.5 4 65.3 7.5 154 5 1 3 28.479 56.958 0.31 6.49 4 10.0 0.2 155 9 3 2 28.488 56.976 0.31 6.49 4 18.3 0.6 156 2 2 -3 28.615 57.231 0.311 6.42 4 211.9 77.5 157 13 3 -1 28.657 57.313 0.311 6.4 4 256.6 113.4 158 10 4 1 28.706 57.412 0.312 6.38 4 8.3 0.1 159 13 1 -2 28.737 57.474 0.312 6.36 4 53.8 4.9 160 2 2 3 28.76 57.52 0.312 6.35 4 21.6 0.8 161 12 2 -2 28.922 57.845 0.314 6.27 4 21.6 0.8 162 7 5 0 28.948 57.897 0.314 6.26 4 112.7 21.4 163 13 3 1 28.969 57.937 0.314 6.25 4 63.4 6.8 164 5 5 -1 29.01 58.02 0.315 6.23 4 13.1 0.3 165 5 5 1 29.129 58.258 0.316 6.17 4 18.9 0.6 166 4 2 -3 29.22 58.441 0.317 6.13 4 53.7 4.8 167 6 4 -2 29.257 58.515 0.317 6.11 4 3.0 0.0 168 13 1 2 29.358 58.716 0.318 6.06 4 137.7 30.9 169 7 1 -3 29.401 58.803 0.319 6.04 4 24.9 1.0 170 12 2 2 29.493 58.987 0.32 6.0 4 8.5 0.1 171 4 2 3 29.505 59.01 0.32 5.99 4 27.6 1.2 172 6 4 2 29.542 59.083 0.32 5.98 4 16.4 0.4 173 12 4 0 29.589 59.178 0.321 5.95 4 186.2 55.5 174 16 2 0 29.621 59.243 0.321 5.94 4 67.0 7.2 175 14 0 -2 29.706 59.412 0.322 5.9 2 194.2 29.9 176 7 1 3 29.896 59.793 0.324 5.82 4 135.8 28.9 177 17 1 0 29.907 59.813 0.324 5.81 4 54.8 4.7 178 11 3 -2 30.249 60.497 0.327 5.67 4 12.7 0.2 179 6 2 -3 30.259 60.517 0.327 5.66 4 18.8 0.5 180 7 5 -1 30.319 60.637 0.328 5.64 4 61.4 5.7 181 14 0 2 30.361 60.722 0.328 5.62 2 71.4 3.9 182 15 3 0 30.471 60.942 0.329 5.58 4 32.2 1.6 183 7 5 1 30.481 60.962 0.329 5.57 4 25.6 1.0 184 6 2 3 30.676 61.352 0.331 5.49 4 67.8 6.8 185 9 5 0 30.719 61.438 0.332 5.48 4 108.5 17.3 186 8 4 -2 30.754 61.509 0.332 5.46 4 132.0 25.6 187 11 3 2 30.758 61.517 0.332 5.46 4 63.9 6.0 188 16 2 -1 30.87 61.74 0.333 5.42 4 97.4 13.8 189 12 4 -1 30.884 61.769 0.333 5.41 4 45.9 3.1 190 1 3 -3 31.054 62.107 0.335 5.35 4 3.9 0.0 191 9 1 -3 31.088 62.175 0.335 5.33 4 98.2 13.8 192 8 4 2 31.122 62.244 0.336 5.32 4 34.1 1.7 193 1 3 3 31.122 62.245 0.336 5.32 4 113.4 18.4 194 17 1 -1 31.137 62.274 0.336 5.32 4 7.3 0.1 195 12 4 1 31.16 62.319 0.336 5.31 4 41.7 2.5 196 16 2 1 31.237 62.474 0.337 5.28 4 74.5 7.9 197 18 0 0 31.308 62.616 0.337 5.25 2 70.7 3.5 198 3 3 -3 31.416 62.832 0.338 5.21 4 51.1 3.7 199 17 1 1 31.525 63.05 0.339 5.17 4 91.0 11.5 200 3 3 3 31.62 63.241 0.34 5.14 4 183.1 46.3 201 9 1 3 31.703 63.406 0.341 5.11 4 95.5 12.5 202 8 2 -3 31.705 63.409 0.341 5.11 4 31.1 1.3 203 15 3 -1 31.711 63.422 0.341 5.11 4 40.4 2.2 204 14 2 -2 31.726 63.451 0.341 5.1 4 17.0 0.4 205 15 1 -2 31.764 63.528 0.342 5.09 4 97.4 13.0 206 0 6 0 31.856 63.711 0.343 5.06 2 221.6 33.4 207 1 5 -2 32.018 64.036 0.344 5.0 4 111.2 16.6 208 9 5 -1 32.021 64.042 0.344 5.0 4 23.6 0.8 209 15 3 1 32.05 64.1 0.344 4.99 4 220.8 65.4 210 1 5 2 32.063 64.126 0.345 4.98 4 0.0 0.0 211 2 6 0 32.068 64.137 0.345 4.98 4 108.4 15.8 212 5 3 -3 32.201 64.402 0.346 4.94 4 100.9 13.5 213 9 5 1 32.224 64.448 0.346 4.93 4 71.9 6.9 214 8 2 3 32.246 64.492 0.346 4.92 4 25.8 0.9 215 14 2 2 32.357 64.713 0.347 4.89 4 116.7 17.9 216 3 5 -2 32.397 64.793 0.348 4.87 4 81.9 8.8 217 14 4 0 32.402 64.805 0.348 4.87 4 94.4 11.7 218 15 1 2 32.44 64.879 0.348 4.86 4 67.3 5.9 219 3 5 2 32.531 65.062 0.349 4.83 4 12.2 0.2 220 5 3 3 32.537 65.074 0.349 4.83 4 14.6 0.3 221 10 4 -2 32.632 65.264 0.35 4.8 4 107.3 14.8 222 4 6 0 32.702 65.404 0.351 4.78 4 24.7 0.8 223 13 3 -2 32.776 65.551 0.351 4.75 4 23.2 0.7 224 11 5 0 32.852 65.705 0.352 4.73 4 44.7 2.5 225 16 0 -2 32.889 65.778 0.352 4.72 2 104.8 7.0 226 10 4 2 33.077 66.153 0.354 4.66 4 20.8 0.5 227 11 1 -3 33.142 66.283 0.355 4.64 4 83.8 8.8 228 5 5 -2 33.191 66.382 0.355 4.63 4 225.0 63.0 229 0 6 1 33.233 66.465 0.356 4.62 4 40.5 2.0 230 18 2 0 33.272 66.543 0.356 4.6 4 8.8 0.1 231 13 3 2 33.352 66.704 0.357 4.58 4 39.4 1.9 232 7 3 -3 33.393 66.785 0.357 4.57 4 35.8 1.6 233 5 5 2 33.412 66.824 0.357 4.56 4 44.8 2.5 234 2 6 -1 33.419 66.837 0.358 4.56 4 6.1 0.0 235 2 6 1 33.463 66.925 0.358 4.55 4 27.4 0.9 236 10 2 -3 33.531 67.062 0.359 4.53 4 1.1 0.0 237 16 0 2 33.597 67.193 0.359 4.51 2 140.8 12.0 238 14 4 -1 33.614 67.228 0.359 4.51 4 38.8 1.8 239 6 6 0 33.744 67.487 0.361 4.47 4 18.1 0.4 240 19 1 0 33.746 67.492 0.361 4.47 4 55.7 3.7 241 7 3 3 33.854 67.708 0.362 4.44 4 105.0 13.2 242 17 3 0 33.864 67.727 0.362 4.44 4 26.6 0.8 243 11 1 3 33.868 67.736 0.362 4.43 4 11.7 0.2 244 14 4 1 33.921 67.842 0.362 4.42 4 52.1 3.2 245 4 6 -1 34.017 68.034 0.363 4.39 4 101.6 12.2 246 11 5 -1 34.089 68.177 0.364 4.38 4 43.6 2.2 247 4 6 1 34.105 68.209 0.364 4.37 4 89.2 9.4 248 10 2 3 34.188 68.376 0.365 4.35 4 99.1 11.5 249 11 5 1 34.328 68.657 0.366 4.31 4 60.9 4.3 250 7 5 -2 34.387 68.774 0.367 4.3 4 72.6 6.1 251 18 2 -1 34.424 68.848 0.367 4.29 4 41.0 1.9 252 0 4 3 34.447 68.894 0.367 4.28 4 151.3 26.4 253 2 4 -3 34.586 69.173 0.368 4.25 4 134.8 20.8 254 7 5 2 34.691 69.382 0.369 4.22 4 77.8 6.9 255 2 4 3 34.716 69.433 0.37 4.21 4 34.9 1.4 256 16 2 -2 34.806 69.613 0.371 4.19 4 14.8 0.2 257 18 2 1 34.814 69.629 0.371 4.19 4 3.1 0.0 258 12 4 -2 34.863 69.726 0.371 4.18 4 94.6 10.1 259 19 1 -1 34.88 69.761 0.371 4.17 4 30.5 1.0 260 9 3 -3 34.971 69.942 0.372 4.15 4 153.5 26.3 261 17 3 -1 35.018 70.035 0.372 4.14 4 42.4 2.0 262 6 6 -1 35.018 70.036 0.372 4.14 4 4.8 0.0 263 17 1 -2 35.047 70.093 0.373 4.13 4 235.6 61.7 264 4 4 -3 35.132 70.265 0.374 4.11 4 1.6 0.0 265 6 6 1 35.148 70.295 0.374 4.11 4 104.0 12.0 266 8 6 0 35.177 70.353 0.374 4.1 4 15.7 0.3 267 20 0 0 35.266 70.532 0.375 4.08 2 91.8 4.6 268 19 1 1 35.29 70.579 0.375 4.08 4 17.3 0.3 269 13 5 0 35.322 70.644 0.375 4.07 4 61.4 4.1 270 12 4 2 35.38 70.76 0.376 4.06 4 53.0 3.1 271 17 3 1 35.383 70.767 0.376 4.06 4 225.7 55.6 272 4 4 3 35.39 70.781 0.376 4.05 4 20.3 0.5 273 16 2 2 35.495 70.99 0.377 4.03 4 95.4 9.9 274 16 4 0 35.496 70.992 0.377 4.03 4 111.2 13.4 275 13 1 -3 35.537 71.075 0.377 4.02 4 8.6 0.1 276 9 3 3 35.552 71.103 0.377 4.02 4 9.0 0.1 277 15 3 -2 35.609 71.219 0.378 4.0 4 49.3 2.6 278 12 2 -3 35.713 71.427 0.379 3.98 4 1.4 0.0 279 17 1 2 35.776 71.552 0.379 3.97 4 88.0 8.3 280 9 5 -2 35.967 71.933 0.381 3.93 4 17.5 0.3 281 6 4 -3 36.077 72.154 0.382 3.9 4 18.2 0.3 282 0 0 4 36.194 72.387 0.383 3.88 2 165.3 14.3 283 15 3 2 36.249 72.499 0.384 3.87 4 49.9 2.6 284 2 0 -4 36.309 72.618 0.384 3.86 2 47.4 1.2 285 18 0 -2 36.321 72.642 0.384 3.85 2 111.9 6.5 286 9 5 2 36.35 72.699 0.385 3.85 4 16.6 0.3 287 13 1 3 36.369 72.738 0.385 3.84 4 35.6 1.3 288 8 6 -1 36.407 72.815 0.385 3.84 4 25.8 0.7 289 6 4 3 36.459 72.919 0.386 3.82 4 10.3 0.1 290 2 0 4 36.479 72.957 0.386 3.82 2 25.8 0.3 291 12 2 3 36.48 72.959 0.386 3.82 4 133.1 18.2 292 13 5 -1 36.498 72.996 0.386 3.82 4 15.8 0.3 293 8 6 1 36.577 73.154 0.387 3.8 4 94.0 9.0 294 16 4 -1 36.638 73.276 0.387 3.79 4 22.2 0.5 295 1 1 -4 36.665 73.33 0.388 3.78 4 194.2 38.4 296 1 1 4 36.75 73.499 0.388 3.77 4 42.0 1.8 297 13 5 1 36.773 73.546 0.389 3.76 4 50.8 2.6 298 4 0 -4 36.823 73.646 0.389 3.75 2 124.3 7.8 299 11 3 -3 36.917 73.834 0.39 3.74 4 41.7 1.7 300 16 4 1 36.976 73.952 0.39 3.72 4 60.1 3.6 301 3 1 -4 36.979 73.957 0.39 3.72 4 125.4 15.8 302 10 6 0 36.983 73.966 0.39 3.72 4 33.4 1.1 303 18 0 2 37.082 74.165 0.391 3.7 2 113.7 6.4 304 20 2 0 37.127 74.254 0.392 3.7 4 30.6 0.9 305 4 0 4 37.16 74.321 0.392 3.69 2 41.9 0.9 306 0 6 2 37.211 74.423 0.393 3.68 4 2.8 0.0 307 3 1 4 37.231 74.463 0.393 3.68 4 62.0 3.8 308 2 6 -2 37.367 74.735 0.394 3.65 4 109.7 11.8 309 8 4 -3 37.408 74.816 0.394 3.65 4 27.6 0.7 310 14 4 -2 37.428 74.855 0.395 3.64 4 112.2 12.3 311 2 6 2 37.451 74.903 0.395 3.64 4 166.1 27.0 312 19 3 0 37.494 74.989 0.395 3.63 4 99.2 9.6 313 11 3 3 37.611 75.222 0.396 3.61 4 26.7 0.7 314 5 1 -4 37.687 75.374 0.397 3.6 4 23.2 0.5 315 6 0 -4 37.73 75.459 0.397 3.59 2 185.7 16.6 316 21 1 0 37.777 75.554 0.398 3.58 4 153.3 22.6 317 8 4 3 37.911 75.822 0.399 3.56 4 14.4 0.2 318 11 5 -2 37.913 75.826 0.399 3.56 4 47.2 2.1 319 4 6 -2 37.918 75.836 0.399 3.56 4 100.8 9.7 320 14 4 2 38.014 76.028 0.4 3.54 4 10.3 0.1 321 0 2 4 38.037 76.073 0.4 3.54 4 31.2 0.9 322 1 7 0 38.055 76.111 0.4 3.53 4 58.1 3.2 323 4 6 2 38.085 76.17 0.4 3.53 4 239.6 54.5 324 5 1 4 38.105 76.21 0.401 3.53 4 22.0 0.5 325 15 5 0 38.113 76.226 0.401 3.53 4 4.8 0.0 326 2 2 -4 38.15 76.3 0.401 3.52 4 3.0 0.0 327 18 2 -2 38.162 76.324 0.401 3.52 4 47.8 2.2 328 10 6 -1 38.17 76.34 0.401 3.52 4 51.0 2.5 329 20 2 -1 38.208 76.416 0.401 3.51 4 154.2 22.4 330 6 0 4 38.231 76.462 0.402 3.51 2 182.2 15.7 331 14 2 -3 38.235 76.469 0.402 3.51 4 95.3 8.6 332 15 1 -3 38.26 76.519 0.402 3.5 4 21.3 0.4 333 2 2 4 38.317 76.633 0.402 3.49 4 20.6 0.4 334 11 5 2 38.372 76.744 0.403 3.48 4 218.9 44.9 335 10 6 1 38.378 76.757 0.403 3.48 4 26.8 0.7 336 3 7 0 38.448 76.896 0.404 3.47 4 32.9 1.0 337 19 3 -1 38.583 77.165 0.405 3.45 4 97.0 8.7 338 19 1 -2 38.59 77.179 0.405 3.45 4 77.8 5.6 339 20 2 1 38.624 77.249 0.405 3.45 4 167.0 25.8 340 1 5 -3 38.639 77.278 0.405 3.44 4 15.3 0.2 341 4 2 -4 38.655 77.31 0.405 3.44 4 70.9 4.6 342 1 5 3 38.701 77.403 0.406 3.43 4 26.4 0.6 343 17 3 -2 38.743 77.485 0.406 3.43 4 37.4 1.3 344 7 1 -4 38.782 77.565 0.407 3.42 4 27.3 0.7 345 21 1 -1 38.842 77.684 0.407 3.41 4 66.2 4.0 346 6 6 -2 38.857 77.715 0.407 3.41 4 33.8 1.0 347 18 4 0 38.87 77.74 0.407 3.41 4 17.5 0.3 348 18 2 2 38.91 77.821 0.408 3.4 4 26.9 0.7 349 3 5 -3 38.968 77.936 0.408 3.39 4 41.6 1.6 350 19 3 1 38.977 77.954 0.408 3.39 4 47.5 2.1 351 4 2 4 38.987 77.974 0.408 3.39 4 20.1 0.4 352 8 0 -4 39.02 78.04 0.409 3.39 2 22.4 0.2 353 6 6 2 39.106 78.212 0.409 3.37 4 30.9 0.9 354 14 2 3 39.107 78.214 0.409 3.37 4 53.1 2.6 355 10 4 -3 39.114 78.227 0.41 3.37 4 33.4 1.0 356 12 6 0 39.147 78.295 0.41 3.37 4 48.4 2.1 357 3 5 3 39.154 78.309 0.41 3.37 4 33.8 1.0 358 15 1 3 39.194 78.388 0.41 3.36 4 4.3 0.0 359 13 3 -3 39.216 78.432 0.41 3.36 4 12.1 0.1 360 5 7 0 39.23 78.46 0.411 3.36 4 25.6 0.6 361 15 5 -1 39.237 78.474 0.411 3.36 4 26.1 0.6 362 21 1 1 39.277 78.554 0.411 3.35 4 0.2 0.0 363 1 7 -1 39.325 78.649 0.411 3.34 4 154.0 21.3 364 1 7 1 39.345 78.691 0.412 3.34 4 94.6 8.0 365 7 1 4 39.362 78.724 0.412 3.34 4 31.3 0.9 366 19 1 2 39.377 78.754 0.412 3.34 4 7.3 0.0 367 22 0 0 39.428 78.856 0.412 3.33 2 6.5 0.0 368 17 3 2 39.447 78.893 0.412 3.33 4 16.8 0.3 369 15 5 1 39.547 79.094 0.413 3.31 4 5.7 0.0 370 6 2 -4 39.548 79.096 0.413 3.31 4 87.8 6.9 371 8 0 4 39.681 79.363 0.414 3.3 2 131.4 7.7 372 5 5 -3 39.685 79.37 0.415 3.3 4 88.1 6.9 373 3 7 -1 39.693 79.386 0.415 3.29 4 11.5 0.1 374 10 4 3 39.733 79.467 0.415 3.29 4 73.7 4.8 375 3 7 1 39.755 79.51 0.415 3.29 4 146.6 19.0 376 18 4 -1 39.957 79.914 0.417 3.26 4 22.1 0.4 377 5 5 3 39.994 79.988 0.417 3.26 4 14.6 0.2 378 20 0 -2 40.017 80.033 0.417 3.25 2 128.5 7.2 379 13 3 3 40.021 80.041 0.417 3.25 4 74.3 4.8 380 6 2 4 40.042 80.085 0.418 3.25 4 37.4 1.2 381 8 6 -2 40.178 80.356 0.419 3.23 4 25.6 0.6 382 13 5 -2 40.214 80.429 0.419 3.23 4 69.6 4.2 383 9 1 -4 40.256 80.513 0.419 3.22 4 19.4 0.3 384 12 6 -1 40.294 80.588 0.42 3.22 4 3.7 0.0 385 1 3 -4 40.308 80.616 0.42 3.22 4 16.7 0.2 386 16 4 -2 40.319 80.639 0.42 3.22 4 38.3 1.3 387 18 4 1 40.327 80.654 0.42 3.21 4 5.4 0.0 388 1 3 4 40.39 80.78 0.421 3.21 4 13.3 0.2 389 7 7 0 40.395 80.791 0.421 3.21 4 17.2 0.3 390 5 7 -1 40.448 80.896 0.421 3.2 4 9.1 0.1 391 8 6 2 40.507 81.013 0.422 3.19 4 59.5 3.0 392 12 6 1 40.54 81.081 0.422 3.19 4 86.0 6.3 393 5 7 1 40.551 81.101 0.422 3.19 4 119.8 12.3 394 3 3 -4 40.613 81.225 0.423 3.18 4 11.2 0.1 395 10 0 -4 40.685 81.37 0.423 3.17 2 213.3 19.4 396 13 5 2 40.748 81.496 0.424 3.17 4 126.8 13.7 397 7 5 -3 40.786 81.571 0.424 3.16 4 0.6 0.0 398 8 2 -4 40.822 81.644 0.424 3.16 4 19.7 0.3 399 20 0 2 40.838 81.676 0.424 3.16 2 39.6 0.7 400 3 3 4 40.859 81.717 0.425 3.15 4 15.3 0.2 401 16 4 2 40.975 81.951 0.426 3.14 4 181.8 27.9 402 9 1 4 40.995 81.989 0.426 3.14 4 60.7 3.1 403 16 2 -3 41.089 82.179 0.427 3.13 4 80.9 5.5 404 12 4 -3 41.184 82.368 0.427 3.12 4 22.5 0.4 405 7 5 3 41.215 82.431 0.428 3.12 4 54.1 2.5 406 17 5 0 41.224 82.449 0.428 3.11 4 23.4 0.5 407 22 2 0 41.226 82.451 0.428 3.11 4 34.2 1.0 408 5 3 -4 41.302 82.605 0.428 3.11 4 13.9 0.2 409 17 1 -3 41.307 82.613 0.428 3.11 4 49.0 2.0 410 21 3 0 41.39 82.781 0.429 3.1 4 33.8 1.0 411 8 2 4 41.476 82.953 0.43 3.09 4 5.0 0.0 412 10 0 4 41.503 83.007 0.43 3.09 2 39.1 0.6 413 7 7 -1 41.585 83.17 0.431 3.08 4 32.4 0.9 414 14 6 0 41.664 83.327 0.432 3.07 4 11.2 0.1 415 5 3 4 41.711 83.422 0.432 3.07 4 24.7 0.5 416 7 7 1 41.728 83.455 0.432 3.06 4 13.5 0.2 417 20 2 -2 41.808 83.617 0.433 3.06 4 3.1 0.0 418 15 3 -3 41.862 83.724 0.433 3.05 4 86.5 6.1 419 10 6 -2 41.873 83.746 0.433 3.05 4 71.6 4.2 420 12 4 3 41.919 83.838 0.434 3.05 4 42.6 1.5 421 9 7 0 41.937 83.875 0.434 3.04 4 11.5 0.1 422 23 1 0 42.05 84.1 0.435 3.03 4 30.3 0.7 423 16 2 3 42.069 84.139 0.435 3.03 4 37.4 1.1 424 11 1 -4 42.102 84.204 0.435 3.03 4 20.0 0.3 425 19 3 -2 42.185 84.37 0.436 3.02 4 1.6 0.0 426 22 2 -1 42.258 84.516 0.437 3.02 4 48.3 1.9 427 9 5 -3 42.264 84.528 0.437 3.01 4 0.5 0.0 428 10 6 2 42.281 84.561 0.437 3.01 4 10.7 0.1 429 17 5 -1 42.308 84.615 0.437 3.01 4 27.7 0.6 430 17 1 3 42.347 84.694 0.437 3.01 4 29.9 0.7 431 7 3 -4 42.374 84.748 0.437 3.0 4 30.7 0.8 432 21 1 -2 42.419 84.838 0.438 3.0 4 20.1 0.3 433 21 3 -1 42.432 84.865 0.438 3.0 4 3.4 0.0 434 10 2 -4 42.471 84.943 0.438 3.0 4 64.8 3.4 435 20 4 0 42.542 85.085 0.439 2.99 4 77.7 4.9 436 20 2 2 42.623 85.246 0.44 2.98 4 14.6 0.2 437 17 5 1 42.654 85.307 0.44 2.98 4 26.8 0.6 438 22 2 1 42.706 85.411 0.44 2.98 4 47.7 1.8 439 12 0 -4 42.719 85.438 0.44 2.98 2 110.4 4.9 440 14 6 -1 42.776 85.551 0.441 2.97 4 27.8 0.6 441 15 3 3 42.778 85.556 0.441 2.97 4 37.4 1.1 442 9 5 3 42.813 85.626 0.441 2.97 4 14.5 0.2 443 21 3 1 42.859 85.719 0.442 2.96 4 35.9 1.0 444 15 5 -2 42.868 85.736 0.442 2.96 4 12.2 0.1 445 7 3 4 42.943 85.887 0.442 2.96 4 12.5 0.1 446 19 3 2 42.958 85.916 0.442 2.96 4 48.3 1.9 447 11 1 4 42.997 85.994 0.443 2.95 4 51.1 2.1 448 14 6 1 43.06 86.12 0.443 2.95 4 0.0 0.0 449 23 1 -1 43.069 86.139 0.443 2.95 4 37.3 1.1 450 1 7 -2 43.096 86.193 0.443 2.95 4 19.9 0.3 451 9 7 -1 43.099 86.199 0.444 2.95 4 47.9 1.8 452 1 7 2 43.137 86.274 0.444 2.94 4 26.4 0.6 453 21 1 2 43.273 86.545 0.445 2.93 4 57.5 2.6 454 9 7 1 43.282 86.564 0.445 2.93 4 25.1 0.5 455 10 2 4 43.284 86.569 0.445 2.93 4 32.4 0.8 456 0 4 4 43.424 86.848 0.446 2.92 4 45.2 1.6 457 3 7 -2 43.438 86.877 0.446 2.92 4 12.6 0.1 458 15 5 2 43.477 86.955 0.447 2.92 4 6.6 0.0 459 2 4 -4 43.534 87.069 0.447 2.92 4 42.5 1.4 460 23 1 1 43.536 87.073 0.447 2.91 4 74.7 4.4 461 18 4 -2 43.546 87.092 0.447 2.91 4 71.1 4.0 462 0 6 3 43.55 87.1 0.447 2.91 4 53.2 2.2 463 3 7 2 43.56 87.12 0.447 2.91 4 14.9 0.2 464 20 4 -1 43.591 87.182 0.448 2.91 4 81.4 5.2 465 14 4 -3 43.617 87.234 0.448 2.91 4 6.0 0.0 466 2 6 -3 43.68 87.361 0.448 2.91 4 77.9 4.7 467 12 0 4 43.694 87.387 0.448 2.9 2 74.4 2.2 468 2 4 4 43.697 87.393 0.448 2.9 4 103.0 8.3 469 2 6 3 43.802 87.604 0.449 2.9 4 39.2 1.2 470 9 3 -4 43.824 87.648 0.449 2.9 4 46.5 1.7 471 11 7 0 43.853 87.706 0.45 2.89 4 9.4 0.1 472 24 0 0 43.856 87.712 0.45 2.89 2 149.0 8.6 473 12 6 -2 43.94 87.879 0.45 2.89 4 102.8 8.2 474 20 4 1 43.997 87.993 0.451 2.88 4 78.1 4.7 475 22 0 -2 44.012 88.024 0.451 2.88 2 15.5 0.1 476 4 4 -4 44.027 88.053 0.451 2.88 4 113.5 10.0 477 11 5 -3 44.117 88.234 0.452 2.88 4 11.4 0.1 478 5 7 -2 44.163 88.325 0.452 2.87 4 62.1 3.0 479 4 6 -3 44.193 88.386 0.452 2.87 4 44.0 1.5 480 18 4 2 44.276 88.552 0.453 2.87 4 30.9 0.7 481 18 2 -3 44.288 88.575 0.453 2.87 4 136.8 14.4 482 13 1 -4 44.318 88.635 0.453 2.87 4 123.5 11.8 483 4 4 4 44.351 88.702 0.454 2.86 4 12.5 0.1 484 5 7 2 44.365 88.731 0.454 2.86 4 47.9 1.8 485 12 6 2 44.426 88.852 0.454 2.86 4 54.0 2.2 486 4 6 3 44.436 88.872 0.454 2.86 4 12.1 0.1 487 14 4 3 44.469 88.937 0.455 2.86 4 37.1 1.1 488 12 2 -4 44.495 88.989 0.455 2.86 4 16.9 0.2 489 16 6 0 44.536 89.072 0.455 2.85 4 51.7 2.0 490 9 3 4 44.554 89.108 0.455 2.85 4 78.5 4.7 491 19 5 0 44.673 89.346 0.456 2.85 4 146.6 16.4 492 19 1 -3 44.694 89.388 0.457 2.84 4 10.0 0.1 493 0 8 0 44.725 89.451 0.457 2.84 2 105.4 4.2 494 11 5 3 44.786 89.572 0.457 2.84 4 26.6 0.5 495 17 3 -3 44.864 89.727 0.458 2.84 4 5.5 0.0 496 6 4 -4 44.901 89.802 0.458 2.83 4 95.0 6.9 497 22 0 2 44.904 89.808 0.458 2.83 2 44.7 0.8 498 2 8 0 44.916 89.833 0.458 2.83 4 29.7 0.7 499 11 7 -1 44.99 89.981 0.459 2.83 4 52.1 2.1 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 2 0 0 3.31 6.62 13.34113 3055.7 100.0 100.0 5.5 2 1 1 0 5.312 10.624 8.32018 190.5 6.2 6.2 5.6 3 4 0 0 6.631 13.262 6.67056 59.2 1.9 1.9 5.6 4 3 1 0 7.091 14.182 6.23996 638.8 20.9 20.8 5.6 5 5 1 0 9.732 19.463 4.55695 156.5 5.1 5.1 5.6 6 1 1 -1 10.006 20.012 4.43331 586.4 19.2 19.0 5.6 7 1 1 1 10.065 20.13 4.40756 166.9 5.5 5.4 5.6 8 0 2 0 10.133 20.265 4.3784 328.4 10.7 10.7 5.6 9 2 2 0 10.67 21.341 4.16009 57.8 1.9 1.9 5.6 10 3 1 1 11.175 22.351 3.97437 431.6 14.1 14.0 5.6 11 7 1 0 12.732 25.465 3.49499 471.1 15.4 15.2 5.6 12 5 1 1 13.084 26.169 3.40249 125.5 4.1 4.1 5.6 13 2 2 1 13.742 27.484 3.24254 94.4 3.1 3.0 5.6 14 4 2 -1 14.814 29.628 3.01269 942.1 30.8 30.4 5.6 15 9 1 0 15.921 31.841 2.80812 300.9 9.8 9.7 5.6 16 3 3 0 16.125 32.251 2.77339 58.0 1.9 1.9 5.6 17 6 2 -1 16.607 33.214 2.6951 72.2 2.4 2.3 5.6 18 6 2 1 16.828 33.656 2.66076 117.7 3.9 3.8 5.7 19 2 0 -2 17.438 34.876 2.57041 34.8 1.1 1.1 5.7 20 2 0 2 17.579 35.158 2.5504 141.3 4.6 4.5 5.7 21 1 3 -1 17.666 35.331 2.53831 58.8 1.9 1.9 5.7 22 4 0 2 18.618 37.236 2.41271 150.9 4.9 4.8 5.7 23 8 2 1 19.139 38.279 2.34936 73.9 2.4 2.4 5.7 24 5 1 2 20.048 40.096 2.24696 38.2 1.2 1.2 5.7 25 7 3 -1 21.222 42.444 2.12795 86.4 2.8 2.8 5.7 26 10 2 -1 21.499 42.999 2.10177 74.5 2.4 2.4 5.7 27 8 0 -2 21.781 43.562 2.0759 36.2 1.2 1.2 5.7 28 7 1 2 21.826 43.652 2.07182 123.2 4.0 3.9 5.7 29 2 4 1 22.729 45.458 1.99362 34.2 1.1 1.1 5.7 30 9 3 -1 23.37 46.74 1.94187 104.5 3.4 3.3 5.7 31 4 4 -1 23.439 46.878 1.93648 103.2 3.4 3.3 5.7 32 13 1 -1 24.203 48.406 1.87886 51.0 1.7 1.6 5.7 33 8 2 -2 24.246 48.492 1.87575 35.3 1.2 1.1 5.7 34 12 2 1 24.72 49.44 1.84197 70.3 2.3 2.2 5.7 35 5 3 -2 24.796 49.591 1.8367 42.2 1.4 1.3 5.7 36 11 3 -1 25.866 51.732 1.76562 52.1 1.7 1.6 5.8 37 11 1 2 26.54 53.08 1.72392 50.4 1.6 1.6 5.8 38 3 5 0 26.632 53.265 1.71836 32.8 1.1 1.0 5.8 39 10 4 0 27.073 54.146 1.69245 34.4 1.1 1.1 5.8 40 3 1 3 27.484 54.967 1.66909 81.0 2.7 2.5 5.8 41 2 4 2 27.626 55.253 1.66115 57.4 1.9 1.8 5.8 42 0 2 3 28.46 56.921 1.61637 84.3 2.8 2.6 5.8 43 2 2 -3 28.615 57.231 1.60834 77.5 2.5 2.4 5.8 44 13 3 -1 28.657 57.313 1.60622 113.4 3.7 3.5 5.8 45 13 1 2 29.358 58.716 1.57116 30.9 1.0 1.0 5.8 46 12 4 0 29.589 59.178 1.55999 55.5 1.8 1.7 5.8 47 7 1 3 29.896 59.793 1.5454 33.6 1.1 1.0 5.8 48 8 4 -2 30.754 61.509 1.50634 31.6 1.0 1.0 5.8 49 3 3 3 31.62 63.241 1.46919 46.3 1.5 1.4 5.9 50 0 6 0 31.856 63.711 1.45947 33.4 1.1 1.0 5.9 51 15 3 1 32.05 64.1 1.45155 81.2 2.7 2.5 5.9 52 5 5 -2 33.191 66.382 1.40707 63.0 2.1 1.9 5.9 53 17 1 -2 35.047 70.093 1.34139 63.8 2.1 2.0 5.9 54 17 3 1 35.383 70.767 1.33026 59.1 1.9 1.8 5.9 55 1 1 -4 36.665 73.33 1.28996 38.4 1.3 1.2 6.0 56 2 6 2 37.451 74.903 1.26672 39.3 1.3 1.2 6.0 57 4 6 2 38.085 76.17 1.24877 57.7 1.9 1.7 6.0 58 20 2 -1 38.208 76.416 1.24536 46.7 1.5 1.4 6.0 59 11 5 2 38.372 76.744 1.24086 45.6 1.5 1.4 6.0 60 16 4 2 40.975 81.951 1.17468 31.0 1.0 0.9 6.1 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |