Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** KORNERUPINE 4, DN Mg(3.98)Fe(0.38)Al(5.47)Si(4.11)B(0.43)O(21.24)(OH)(0.76) Orthorhombic C mcm Z = 4 R =0.027 NR =1807 17 .11 .1998 Ref.Str.: Moore P.B., Gupta P.K., Schlomper E.O. (1989) * Amer. Mineral., 74, 642-655 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 16.041 alpha = 90.0 b = 13.746 beta = 90.0 c = 6.715 gamma = 90.0 Unit cell volume (cub. angs.) = 1480.65 Molar volume ( cub.cm/mol.) = 222.96 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.0 0.0 0.0 2.48 Mg = 0.37, Mg = 0.0 2 0.1218 0.1403 0.25 0.48 Mg = 1.00 3 0.5 0.1456 0.25 0.51 Mg = 1.00 4 0.2154 0.0 0.0 0.41 Al = 1.00 5 0.3137 0.1418 0.25 0.65 Al = 0.81, Fe = 0.19 6 0.4076 0.0 0.0 0.39 Al = 1.00 7 0.402 0.353 0.25 0.35 Si = 1.00 8 0.1784 0.3338 0.25 0.66 Si = 0.77, Al = 0.23 9 0.0 0.3425 0.25 0.36 Si = 0.57, B = 0.43 10 0.224 0.0448 0.25 0.49 O = 1.00 11 0.4037 0.046 0.25 0.44 O = 1.00 12 0.4028 0.2355 0.25 0.69 O = 1.00 13 0.1382 0.0996 0.9485 0.64 O = 1.00 14 0.2338 0.2358 0.25 1.2 O = 1.00 15 0.3167 0.0948 0.9529 0.6 O = 1.00 16 0.0824 0.2821 0.25 1.02 O = 1.00 17 0.5 0.0885 0.9459 0.54 O = 1.00 18 0.0 0.1128 0.75 1.06 O = 1.00 19 0.0 0.0882 0.25 1.03 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.0 0.0 0.0 2 2 0.1218 0.1403 0.25 3 3 0.5 0.1456 0.25 4 4 0.2154 0.0 0.0 5 5 0.3137 0.1418 0.25 6 6 0.4076 0.0 0.0 7 7 0.402 0.353 0.25 8 8 0.1784 0.3338 0.25 9 9 0.0 0.3425 0.25 10 10 0.224 0.0448 0.25 11 11 0.4037 0.046 0.25 12 12 0.4028 0.2355 0.25 13 13 0.1382 0.0996 0.9485 14 14 0.2338 0.2358 0.25 15 15 0.3167 0.0948 0.9529 16 16 0.0824 0.2821 0.25 17 17 0.5 0.0885 0.9459 18 18 0.0 0.1128 0.75 19 19 0.0 0.0882 0.25 20 1 0.0 0.0 0.5 21 2 0.8782 0.8597 0.75 22 3 0.5 0.8544 0.75 23 4 0.7846 0.0 0.5 24 5 0.6863 0.8582 0.75 25 6 0.5924 0.0 0.5 26 7 0.598 0.647 0.75 27 8 0.8216 0.6662 0.75 28 9 0.0 0.6575 0.75 29 10 0.776 0.9552 0.75 30 11 0.5963 0.954 0.75 31 12 0.5972 0.7645 0.75 32 13 0.8618 0.9004 0.4485 33 14 0.7662 0.7642 0.75 34 15 0.6833 0.9052 0.4529 35 16 0.9176 0.7179 0.75 36 17 0.5 0.9115 0.4459 37 18 0.0 0.8872 0.25 38 19 0.0 0.9118 0.75 39 2 0.8782 0.1403 0.25 40 4 0.7846 0.0 0.0 41 5 0.6863 0.1418 0.25 42 6 0.5924 0.0 0.0 43 7 0.598 0.353 0.25 44 8 0.8216 0.3338 0.25 45 10 0.776 0.0448 0.25 46 11 0.5963 0.046 0.25 47 12 0.5972 0.2355 0.25 48 13 0.8618 0.0996 0.9485 49 14 0.7662 0.2358 0.25 50 15 0.6833 0.0948 0.9529 51 16 0.9176 0.2821 0.25 52 2 0.1218 0.8597 0.75 53 4 0.2154 0.0 0.5 54 5 0.3137 0.8582 0.75 55 6 0.4076 0.0 0.5 56 7 0.402 0.647 0.75 57 8 0.1784 0.6662 0.75 58 10 0.224 0.9552 0.75 59 11 0.4037 0.954 0.75 60 12 0.4028 0.7645 0.75 61 13 0.1382 0.9004 0.4485 62 14 0.2338 0.7642 0.75 63 15 0.3167 0.9052 0.4529 64 16 0.0824 0.7179 0.75 65 13 0.1382 0.0996 0.5515 66 15 0.3167 0.0948 0.5471 67 17 0.5 0.0885 0.5541 68 13 0.8618 0.9004 0.0515 69 15 0.6833 0.9052 0.0471 70 17 0.5 0.9115 0.0541 71 13 0.8618 0.0996 0.5515 72 15 0.6833 0.0948 0.5471 73 13 0.1382 0.9004 0.0515 74 15 0.3167 0.9052 0.0471 75 1 0.5 0.5 0.5 76 2 0.3782 0.3597 0.75 77 3 0.0 0.3544 0.75 78 4 0.2846 0.5 0.5 79 5 0.1863 0.3582 0.75 80 6 0.0924 0.5 0.5 81 7 0.098 0.147 0.75 82 8 0.3216 0.1662 0.75 83 9 0.5 0.1575 0.75 84 10 0.276 0.4552 0.75 85 11 0.0963 0.454 0.75 86 12 0.0972 0.2645 0.75 87 13 0.3618 0.4004 0.4485 88 14 0.2662 0.2642 0.75 89 15 0.1833 0.4052 0.4529 90 16 0.4176 0.2179 0.75 91 17 0.0 0.4115 0.4459 92 18 0.5 0.3872 0.25 93 19 0.5 0.4118 0.75 94 1 0.5 0.5 0.0 95 2 0.6218 0.6403 0.25 96 3 0.0 0.6456 0.25 97 4 0.7154 0.5 0.0 98 5 0.8137 0.6418 0.25 99 6 0.9076 0.5 0.0 100 7 0.902 0.853 0.25 101 8 0.6784 0.8338 0.25 102 9 0.5 0.8425 0.25 103 10 0.724 0.5448 0.25 104 11 0.9037 0.546 0.25 105 12 0.9028 0.7355 0.25 106 13 0.6382 0.5996 0.9485 107 14 0.7338 0.7358 0.25 108 15 0.8167 0.5948 0.9529 109 16 0.5824 0.7821 0.25 110 17 0.0 0.5885 0.9459 111 18 0.5 0.6128 0.75 112 19 0.5 0.5882 0.25 113 2 0.6218 0.3597 0.75 114 4 0.7154 0.5 0.5 115 5 0.8137 0.3582 0.75 116 6 0.9076 0.5 0.5 117 7 0.902 0.147 0.75 118 8 0.6784 0.1662 0.75 119 10 0.724 0.4552 0.75 120 11 0.9037 0.454 0.75 121 12 0.9028 0.2645 0.75 122 13 0.6382 0.4004 0.4485 123 14 0.7338 0.2642 0.75 124 15 0.8167 0.4052 0.4529 125 16 0.5824 0.2179 0.75 126 2 0.3782 0.6403 0.25 127 4 0.2846 0.5 0.0 128 5 0.1863 0.6418 0.25 129 6 0.0924 0.5 0.0 130 7 0.098 0.853 0.25 131 8 0.3216 0.8338 0.25 132 10 0.276 0.5448 0.25 133 11 0.0963 0.546 0.25 134 12 0.0972 0.7355 0.25 135 13 0.3618 0.5996 0.9485 136 14 0.2662 0.7358 0.25 137 15 0.1833 0.5948 0.9529 138 16 0.4176 0.7821 0.25 139 13 0.3618 0.4004 0.0515 140 15 0.1833 0.4052 0.0471 141 17 0.0 0.4115 0.0541 142 13 0.6382 0.5996 0.5515 143 15 0.8167 0.5948 0.5471 144 17 0.0 0.5885 0.5541 145 13 0.6382 0.4004 0.0515 146 15 0.8167 0.4052 0.0471 147 13 0.3618 0.5996 0.5515 148 15 0.1833 0.5948 0.5471 X-ray density (g/cm cub.) = 3.32 MU (1/cm) = 128.834 Mass attenuation coefficient (cm**2/g) = 38.856 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Mg ,Mg 2.52 4 2.2853 18 2.0708 19 2.2853 18 2.0708 19 2 Mg 2.52 6 2.1002 10 2.1169 13 2.2251 14 2.0491 16 2.0809 19 2.1169 13 3 Mg 2.52 6 2.0641 11 1.9895 12 2.1877 17 2.0641 11 1.9895 12 2.1877 17 4 Al 2.316 6 1.7935 10 1.8782 13 2.1068 15 1.7935 10 1.8782 13 2.1068 15 5 Al ,Fe 2.592 6 1.9617 10 1.9541 11 1.924 12 1.82 14 2.0976 15 2.0976 15 6 Al 2.316 6 1.795 11 1.981 15 1.9516 17 1.795 11 1.9516 17 1.981 15 7 Si 2.1 4 1.6152 12 1.6177 13 1.6408 18 1.6177 13 8 Si ,Al 2.316 4 1.6138 14 1.696 16 1.681 15 1.681 15 9 Si ,B 2.1 4 1.5609 16 1.5609 16 1.6217 17 1.6217 17 10 O 3.264 10 2.8826 11 2.5614 13 2.6302 14 2.5814 15 2.7588 13 2.7839 15 2.5614 13 2.5814 15 2.7588 13 2.7839 15 11 O 3.264 11 2.8826 10 2.6049 12 2.5254 15 2.6263 17 2.745 17 3.0895 11 2.7477 15 2.5254 15 2.6263 17 2.745 17 2.7477 15 12 O 3.264 8 2.6049 11 2.7109 14 3.1029 15 3.1184 12 3.1029 15 2.7106 13 2.6037 18 2.7106 13 13 O 3.264 9 2.5614 10 3.1553 14 2.8642 15 2.5931 18 3.0063 19 2.7588 10 2.6659 13 2.8242 13 2.7106 12 14 O 3.264 9 2.6302 10 2.7109 12 3.1553 13 3.083 15 2.5106 16 3.1553 13 3.083 15 2.8169 15 2.8169 15 15 O 3.264 12 2.5814 10 2.5254 11 3.1029 12 2.8642 13 3.083 14 2.942 17 2.7839 10 2.7477 11 2.7249 15 2.6819 15 2.8169 14 2.7091 16 16 O 3.264 7 2.5106 14 2.9751 19 2.6436 16 2.7091 15 2.5771 17 2.7091 15 2.5771 17 17 O 3.264 10 2.6263 11 2.942 15 2.745 11 2.6263 11 2.942 15 2.745 11 2.6309 17 2.5392 17 2.5771 16 2.5771 16 18 O 3.264 7 2.5931 13 2.7629 19 2.5931 13 2.5931 13 2.5931 13 2.6037 12 2.6037 12 19 O 3.264 7 3.0063 13 2.9751 16 2.7629 18 3.0063 13 2.9751 16 3.0063 13 3.0063 13 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 4.232 8.464 0.048 364.26 4 85.7 487.7 2 2 0 0 5.511 11.022 0.062 213.86 2 80.1 125.3 3 0 2 0 6.435 12.87 0.073 156.26 2 118.9 201.6 4 1 1 1 7.839 15.679 0.089 104.55 8 20.8 16.6 5 2 2 0 8.488 16.975 0.096 88.87 4 32.2 16.8 6 3 1 0 8.892 17.784 0.1 80.77 4 16.3 3.9 7 0 2 1 9.228 18.457 0.104 74.84 4 7.1 0.7 8 1 3 0 10.069 20.138 0.113 62.52 4 25.7 7.5 9 2 2 1 10.774 21.547 0.121 54.33 8 66.6 87.9 10 4 0 0 11.074 22.148 0.125 51.31 2 113.6 60.4 11 3 1 1 11.098 22.196 0.125 51.08 8 25.9 12.5 12 1 3 1 12.07 24.14 0.136 42.86 8 41.6 27.1 13 3 3 0 12.791 25.581 0.144 37.94 4 66.5 30.6 14 4 2 0 12.849 25.698 0.144 37.58 4 53.7 19.8 15 0 4 0 12.953 25.905 0.145 36.95 2 211.4 150.6 16 0 0 2 13.263 26.526 0.149 35.15 2 339.2 368.8 17 1 1 2 13.945 27.891 0.156 31.6 8 47.8 26.4 18 2 4 0 14.114 28.228 0.158 30.8 4 53.1 15.8 19 5 1 0 14.273 28.547 0.16 30.07 4 58.7 18.9 20 2 0 2 14.401 28.803 0.161 29.51 4 51.5 14.3 21 3 3 1 14.439 28.877 0.162 29.34 8 26.3 7.4 22 4 2 1 14.491 28.982 0.162 29.12 8 38.0 15.4 23 0 4 1 14.584 29.167 0.163 28.72 4 104.0 56.7 24 0 2 2 14.793 29.586 0.166 27.86 4 404.3 831.1 25 2 4 1 15.634 31.268 0.175 24.75 8 16.3 2.4 26 5 1 1 15.779 31.558 0.177 24.26 8 85.9 65.4 27 2 2 2 15.831 31.661 0.177 24.09 8 39.8 13.9 28 3 1 2 16.059 32.119 0.18 23.35 8 80.3 54.9 29 1 5 0 16.515 33.03 0.185 21.98 4 139.3 77.8 30 6 0 0 16.745 33.49 0.187 21.33 2 66.1 8.5 31 1 3 2 16.765 33.53 0.187 21.28 8 55.4 23.8 32 5 3 0 17.044 34.087 0.19 20.53 4 496.9 924.8 33 4 4 0 17.169 34.338 0.192 20.2 4 95.8 33.8 34 4 0 2 17.41 34.821 0.194 19.6 4 27.3 2.7 35 1 5 1 17.851 35.702 0.199 18.55 8 13.4 1.2 36 6 2 0 18.008 36.016 0.201 18.2 4 6.5 0.1 37 5 3 1 18.346 36.691 0.204 17.47 8 33.0 6.9 38 3 5 0 18.364 36.727 0.205 17.43 4 0.7 0.0 39 4 4 1 18.463 36.926 0.206 17.23 8 16.0 1.6 40 3 3 2 18.592 37.183 0.207 16.97 8 32.9 6.7 41 4 2 2 18.633 37.267 0.207 16.88 8 46.0 13.1 42 0 4 2 18.708 37.416 0.208 16.74 4 211.9 137.1 43 6 2 1 19.253 38.506 0.214 15.71 8 8.5 0.4 44 2 4 2 19.561 39.122 0.217 15.17 8 44.6 11.0 45 3 5 1 19.59 39.179 0.218 15.12 8 23.9 3.2 46 0 6 0 19.647 39.293 0.218 15.02 2 108.1 16.0 47 5 1 2 19.681 39.362 0.219 14.96 8 123.4 83.2 48 7 1 0 19.924 39.848 0.221 14.56 4 39.4 4.1 49 2 6 0 20.467 40.934 0.227 13.71 4 28.3 2.0 50 1 1 3 20.607 41.214 0.228 13.51 8 27.0 3.6 51 0 6 1 20.809 41.617 0.231 13.21 4 38.7 3.6 52 7 1 1 21.073 42.147 0.233 12.85 8 10.8 0.5 53 0 2 3 21.218 42.436 0.235 12.65 4 209.5 101.3 54 6 4 0 21.41 42.82 0.237 12.4 4 385.4 336.0 55 1 5 2 21.426 42.852 0.237 12.38 8 89.3 36.0 56 2 6 1 21.592 43.185 0.239 12.16 8 1.9 0.0 57 6 0 2 21.611 43.222 0.239 12.14 4 49.3 5.4 58 5 5 0 21.653 43.306 0.24 12.09 4 309.0 210.6 59 5 3 2 21.852 43.704 0.242 11.84 8 124.9 67.4 60 4 4 2 21.954 43.907 0.243 11.72 8 3.4 0.1 61 2 2 3 21.99 43.98 0.243 11.67 8 71.4 21.7 62 7 3 0 22.076 44.151 0.244 11.57 4 55.7 6.6 63 3 1 3 22.164 44.327 0.245 11.47 8 46.0 8.9 64 6 4 1 22.497 44.994 0.248 11.09 8 71.6 20.7 65 8 0 0 22.591 45.183 0.249 10.99 2 74.0 5.5 66 6 2 2 22.642 45.284 0.25 10.93 8 47.2 8.9 67 1 3 3 22.706 45.411 0.251 10.86 8 54.5 11.8 68 5 5 1 22.731 45.462 0.251 10.83 8 125.1 61.9 69 4 6 0 22.782 45.563 0.251 10.78 4 34.5 2.3 70 3 5 2 22.938 45.875 0.253 10.61 8 9.8 0.4 71 7 3 1 23.138 46.276 0.255 10.41 8 42.0 6.7 72 1 7 0 23.278 46.555 0.257 10.27 4 49.7 4.6 73 8 2 0 23.589 47.178 0.26 9.96 4 25.7 1.2 74 4 6 1 23.819 47.638 0.262 9.75 8 23.6 2.0 75 0 6 2 24.019 48.037 0.264 9.56 4 120.8 25.5 76 3 3 3 24.154 48.308 0.266 9.44 8 18.7 1.2 77 4 2 3 24.188 48.376 0.266 9.41 8 14.0 0.7 78 0 4 3 24.248 48.497 0.267 9.36 4 211.3 76.2 79 7 1 2 24.255 48.511 0.267 9.35 8 6.3 0.1 80 1 7 1 24.299 48.598 0.267 9.31 8 19.4 1.3 81 8 2 1 24.6 49.201 0.27 9.06 8 41.5 5.7 82 3 7 0 24.7 49.401 0.271 8.97 4 16.2 0.4 83 2 6 2 24.722 49.443 0.271 8.96 8 13.9 0.6 84 2 4 3 24.946 49.893 0.274 8.77 8 1.4 0.0 85 5 1 3 25.045 50.091 0.275 8.69 8 12.4 0.5 86 6 4 2 25.54 51.081 0.28 8.32 8 49.0 7.3 87 3 7 1 25.679 51.358 0.281 8.21 8 50.6 7.7 88 5 5 2 25.753 51.506 0.282 8.16 8 185.6 102.6 89 9 1 0 25.836 51.672 0.283 8.1 4 158.0 36.9 90 7 5 0 25.951 51.901 0.284 8.02 4 90.3 11.9 91 7 3 2 26.124 52.249 0.286 7.9 8 17.9 0.9 92 6 6 0 26.281 52.563 0.287 7.79 4 45.0 2.9 93 8 4 0 26.408 52.817 0.289 7.71 4 37.5 2.0 94 1 5 3 26.51 53.02 0.29 7.64 8 4.9 0.1 95 8 0 2 26.58 53.16 0.29 7.59 4 40.2 2.2 96 0 8 0 26.634 53.268 0.291 7.56 2 265.6 48.6 97 4 6 2 26.749 53.498 0.292 7.48 8 90.8 22.5 98 9 1 1 26.785 53.569 0.293 7.46 8 24.8 1.7 99 5 3 3 26.874 53.748 0.293 7.4 8 101.2 27.7 100 7 5 1 26.897 53.793 0.294 7.39 8 96.4 25.1 101 4 4 3 26.961 53.923 0.294 7.35 8 29.7 2.4 102 1 7 2 27.191 54.381 0.297 7.21 8 58.9 9.1 103 6 6 1 27.219 54.439 0.297 7.19 8 106.7 29.9 104 2 8 0 27.288 54.576 0.298 7.15 4 20.7 0.6 105 0 0 4 27.312 54.625 0.298 7.14 2 680.5 301.5 106 8 4 1 27.343 54.687 0.298 7.12 8 39.8 4.1 107 5 7 0 27.381 54.762 0.299 7.1 4 146.6 27.8 108 8 2 2 27.469 54.938 0.299 7.05 8 22.4 1.3 109 6 2 3 27.555 55.11 0.3 7.0 8 117.6 35.3 110 0 8 1 27.564 55.128 0.3 6.99 4 62.6 5.0 111 9 3 0 27.627 55.255 0.301 6.95 4 89.8 10.2 112 1 1 4 27.693 55.387 0.302 6.92 8 39.5 3.9 113 3 5 3 27.811 55.623 0.303 6.85 8 16.7 0.7 114 2 0 4 27.955 55.911 0.304 6.77 4 39.9 2.0 115 0 2 4 28.186 56.371 0.307 6.65 4 33.9 1.4 116 2 8 1 28.203 56.406 0.307 6.64 8 16.5 0.7 117 5 7 1 28.294 56.588 0.308 6.59 8 65.3 10.2 118 3 7 2 28.471 56.941 0.309 6.5 8 4.0 0.0 119 9 3 1 28.535 57.07 0.31 6.46 8 19.8 0.9 120 10 0 0 28.698 57.396 0.312 6.38 2 386.6 87.0 121 0 6 3 28.758 57.516 0.312 6.35 4 52.1 3.1 122 2 2 4 28.816 57.632 0.313 6.32 8 21.7 1.1 123 3 1 4 28.959 57.917 0.314 6.25 8 7.0 0.1 124 7 1 3 28.967 57.934 0.314 6.25 8 44.5 4.5 125 4 8 0 29.19 58.38 0.317 6.14 4 51.4 3.0 126 2 6 3 29.38 58.761 0.318 6.05 8 20.8 1.0 127 1 3 4 29.408 58.816 0.319 6.04 8 18.0 0.7 128 9 1 2 29.505 59.009 0.32 5.99 8 64.1 9.0 129 10 2 0 29.545 59.089 0.32 5.97 4 64.6 4.5 130 7 5 2 29.61 59.219 0.321 5.95 8 24.2 1.3 131 4 0 4 29.83 59.659 0.323 5.85 4 58.3 3.6 132 6 6 2 29.913 59.826 0.324 5.81 8 256.5 139.5 133 8 4 2 30.03 60.06 0.325 5.76 8 1.4 0.0 134 4 8 1 30.067 60.135 0.325 5.74 8 8.6 0.2 135 6 4 3 30.111 60.222 0.326 5.73 8 25.4 1.3 136 0 8 2 30.238 60.475 0.327 5.67 4 30.6 1.0 137 5 5 3 30.302 60.604 0.328 5.65 8 72.7 10.9 138 10 2 1 30.415 60.831 0.329 5.6 8 0.7 0.0 139 1 9 0 30.438 60.877 0.329 5.59 4 7.2 0.1 140 3 3 4 30.628 61.256 0.331 5.51 8 50.4 5.1 141 7 3 3 30.636 61.272 0.331 5.51 8 73.3 10.8 142 4 2 4 30.657 61.313 0.331 5.5 8 37.0 2.7 143 8 6 0 30.698 61.395 0.331 5.49 4 70.0 4.9 144 0 4 4 30.708 61.416 0.331 5.48 4 67.0 4.5 145 2 8 2 30.841 61.683 0.333 5.43 8 45.9 4.2 146 5 7 2 30.927 61.855 0.334 5.4 8 464.9 425.4 147 9 5 0 31.001 62.002 0.334 5.37 4 1.0 0.0 148 7 7 0 31.103 62.206 0.335 5.33 4 53.5 2.8 149 9 3 2 31.156 62.312 0.336 5.31 8 142.3 39.2 150 4 6 3 31.201 62.402 0.336 5.29 8 47.3 4.3 151 1 9 1 31.294 62.589 0.337 5.26 8 95.6 17.5 152 2 4 4 31.306 62.613 0.337 5.25 8 42.6 3.5 153 5 1 4 31.392 62.783 0.338 5.22 8 14.6 0.4 154 8 6 1 31.55 63.099 0.34 5.16 8 52.0 5.1 155 1 7 3 31.602 63.205 0.34 5.14 8 21.6 0.9 156 3 9 0 31.635 63.269 0.34 5.13 4 40.1 1.5 157 9 5 1 31.848 63.696 0.343 5.06 8 42.0 3.3 158 8 2 3 31.856 63.712 0.343 5.06 8 57.5 6.1 159 7 7 1 31.949 63.898 0.343 5.02 8 21.7 0.9 160 10 4 0 32.001 64.002 0.344 5.01 4 44.8 1.8 161 11 1 0 32.085 64.17 0.345 4.98 4 317.7 91.7 162 10 0 2 32.153 64.306 0.345 4.95 4 148.0 19.8 163 6 8 0 32.201 64.403 0.346 4.94 4 67.0 4.0 164 3 9 1 32.473 64.946 0.349 4.85 8 0.7 0.0 165 4 8 2 32.614 65.228 0.35 4.8 8 20.7 0.8 166 1 5 4 32.667 65.335 0.35 4.79 8 98.8 17.1 167 3 7 3 32.775 65.549 0.351 4.75 8 19.5 0.7 168 6 0 4 32.806 65.612 0.352 4.74 4 25.3 0.6 169 10 4 1 32.834 65.668 0.352 4.74 8 52.8 4.8 170 11 1 1 32.917 65.834 0.353 4.71 8 85.3 12.5 171 10 2 2 32.947 65.893 0.353 4.7 8 138.4 32.9 172 5 3 4 32.988 65.976 0.353 4.69 8 352.8 212.9 173 6 8 1 33.032 66.063 0.354 4.68 8 31.7 1.7 174 4 4 4 33.065 66.13 0.354 4.67 8 50.8 4.4 175 6 2 4 33.592 67.183 0.359 4.51 8 46.7 3.6 176 11 3 0 33.664 67.328 0.36 4.49 4 52.6 2.3 177 9 1 3 33.73 67.461 0.36 4.47 8 20.2 0.7 178 1 9 2 33.789 67.578 0.361 4.46 8 50.4 4.1 179 3 5 4 33.82 67.64 0.361 4.45 8 19.5 0.6 180 7 5 3 33.828 67.656 0.361 4.45 8 91.5 13.6 181 5 9 0 33.957 67.913 0.363 4.41 4 197.3 31.3 182 8 6 2 34.034 68.069 0.363 4.39 8 31.7 1.6 183 0 10 0 34.081 68.162 0.364 4.38 2 43.4 0.8 184 6 6 3 34.11 68.22 0.364 4.37 8 132.5 28.0 185 8 4 3 34.219 68.438 0.365 4.34 8 19.4 0.6 186 9 5 2 34.322 68.643 0.366 4.31 8 46.0 3.3 187 0 8 3 34.413 68.825 0.367 4.29 4 90.6 6.4 188 7 7 2 34.418 68.837 0.367 4.29 8 15.5 0.4 189 11 3 1 34.476 68.953 0.367 4.27 8 37.0 2.1 190 2 10 0 34.648 69.297 0.369 4.23 4 4.0 0.0 191 0 6 4 34.669 69.339 0.369 4.23 4 213.5 35.1 192 5 9 1 34.766 69.532 0.37 4.2 8 35.5 1.9 193 7 1 4 34.858 69.716 0.371 4.18 8 1.7 0.0 194 0 10 1 34.889 69.778 0.371 4.17 4 136.0 14.1 195 3 9 2 34.923 69.847 0.372 4.16 8 16.2 0.4 196 2 8 3 34.977 69.954 0.372 4.15 8 0.3 0.0 197 5 7 3 35.058 70.116 0.373 4.13 8 136.6 28.1 198 12 0 0 35.186 70.372 0.374 4.1 2 148.6 8.3 199 2 6 4 35.232 70.464 0.374 4.09 8 28.6 1.2 200 10 4 2 35.272 70.544 0.375 4.08 8 209.4 65.3 201 9 3 3 35.272 70.544 0.375 4.08 8 19.6 0.6 202 1 1 5 35.33 70.659 0.375 4.07 8 9.9 0.1 203 11 1 2 35.352 70.705 0.376 4.06 8 54.9 4.5 204 2 10 1 35.45 70.9 0.376 4.04 8 76.8 8.7 205 6 8 2 35.463 70.927 0.377 4.04 8 49.1 3.5 206 9 7 0 35.707 71.415 0.379 3.98 4 116.2 9.8 207 0 2 5 35.761 71.521 0.379 3.97 4 75.5 4.1 208 10 6 0 35.888 71.776 0.381 3.94 4 154.8 17.2 209 6 4 4 35.897 71.795 0.381 3.94 8 213.1 65.3 210 12 2 0 35.947 71.893 0.381 3.93 4 49.0 1.7 211 5 5 4 36.072 72.144 0.382 3.9 8 157.0 35.1 212 8 8 0 36.184 72.367 0.383 3.88 4 45.7 1.5 213 2 2 5 36.316 72.632 0.384 3.85 8 22.3 0.7 214 4 10 0 36.326 72.651 0.385 3.85 4 34.6 0.8 215 7 3 4 36.378 72.757 0.385 3.84 8 23.2 0.8 216 3 1 5 36.442 72.885 0.386 3.83 8 9.8 0.1 217 9 7 1 36.499 72.998 0.386 3.82 8 29.3 1.2 218 4 8 3 36.648 73.296 0.387 3.79 8 22.1 0.7 219 10 6 1 36.678 73.356 0.388 3.78 8 15.4 0.3 220 11 5 0 36.721 73.443 0.388 3.77 4 38.7 1.0 221 12 2 1 36.736 73.473 0.388 3.77 8 96.8 12.9 222 8 0 4 36.757 73.514 0.388 3.77 4 24.4 0.4 223 1 3 5 36.842 73.683 0.389 3.75 8 13.6 0.3 224 11 3 2 36.864 73.728 0.389 3.75 8 166.6 38.0 225 4 6 4 36.898 73.796 0.39 3.74 8 39.3 2.1 226 10 2 3 36.964 73.928 0.39 3.73 8 6.8 0.1 227 8 8 1 36.971 73.943 0.39 3.73 8 6.3 0.1 228 4 10 1 37.112 74.224 0.392 3.7 8 13.7 0.3 229 5 9 2 37.146 74.292 0.392 3.69 8 55.4 4.1 230 0 10 2 37.266 74.531 0.393 3.67 4 459.8 141.6 231 1 7 4 37.269 74.539 0.393 3.67 8 13.9 0.3 232 7 9 0 37.307 74.614 0.393 3.66 4 87.1 5.1 233 11 5 1 37.505 75.01 0.395 3.63 8 32.3 1.4 234 8 2 4 37.505 75.01 0.395 3.63 8 9.9 0.1 235 1 9 3 37.766 75.532 0.398 3.58 8 60.5 4.8 236 2 10 2 37.813 75.625 0.398 3.58 8 69.6 6.3 237 3 3 5 37.937 75.874 0.399 3.55 8 24.1 0.8 238 4 2 5 37.963 75.926 0.399 3.55 8 37.8 1.8 239 8 6 3 38.0 76.001 0.4 3.54 8 34.3 1.5 240 0 4 5 38.01 76.019 0.4 3.54 4 7.9 0.0 241 7 9 1 38.086 76.172 0.4 3.53 8 42.3 2.3 242 1 11 0 38.19 76.38 0.401 3.51 4 24.4 0.4 243 12 4 0 38.192 76.383 0.401 3.51 4 20.2 0.3 244 9 5 3 38.275 76.55 0.402 3.5 8 32.0 1.3 245 12 0 2 38.333 76.665 0.403 3.49 4 111.6 7.9 246 3 7 4 38.361 76.721 0.403 3.49 8 24.2 0.7 247 7 7 3 38.368 76.736 0.403 3.48 8 18.2 0.4 248 2 4 5 38.553 77.106 0.405 3.46 8 11.6 0.2 249 5 1 5 38.631 77.261 0.405 3.44 8 74.0 6.9 250 13 1 0 38.812 77.623 0.407 3.42 4 45.5 1.3 251 9 7 2 38.838 77.675 0.407 3.41 8 49.5 3.0 252 3 9 3 38.853 77.705 0.407 3.41 8 18.8 0.4 253 1 11 1 38.963 77.927 0.408 3.39 8 8.0 0.1 254 12 4 1 38.965 77.93 0.408 3.39 8 71.6 6.4 255 10 6 2 39.013 78.026 0.409 3.39 8 13.2 0.2 256 6 10 0 39.057 78.115 0.409 3.38 4 22.5 0.3 257 12 2 2 39.07 78.14 0.409 3.38 8 62.8 4.9 258 10 4 3 39.188 78.376 0.41 3.36 8 61.1 4.6 259 9 1 4 39.258 78.516 0.411 3.35 8 116.9 16.7 260 11 1 3 39.265 78.53 0.411 3.35 8 141.2 24.4 261 3 11 0 39.273 78.546 0.411 3.35 4 23.0 0.3 262 8 8 2 39.3 78.601 0.411 3.35 8 50.5 3.1 263 7 5 4 39.35 78.7 0.412 3.34 8 43.8 2.3 264 6 8 3 39.372 78.744 0.412 3.34 8 55.8 3.8 265 4 10 2 39.438 78.877 0.412 3.33 8 76.3 7.1 266 13 1 1 39.581 79.163 0.414 3.31 8 31.6 1.2 267 6 6 4 39.616 79.233 0.414 3.3 8 17.1 0.4 268 8 4 4 39.719 79.438 0.415 3.29 8 17.1 0.4 269 1 5 5 39.802 79.603 0.416 3.28 8 18.3 0.4 270 11 5 2 39.824 79.647 0.416 3.28 8 66.6 5.3 271 6 10 1 39.826 79.651 0.416 3.28 8 57.3 3.9 272 0 8 4 39.903 79.805 0.416 3.27 4 197.1 23.1 273 3 11 1 40.04 80.08 0.418 3.25 8 8.6 0.1 274 5 3 5 40.098 80.197 0.418 3.24 8 60.0 4.3 275 4 4 5 40.17 80.34 0.419 3.23 8 4.6 0.0 276 13 3 0 40.278 80.555 0.42 3.22 4 24.3 0.3 277 7 9 2 40.395 80.79 0.421 3.21 8 51.1 3.1 278 2 8 4 40.439 80.877 0.421 3.2 8 9.0 0.1 279 5 7 4 40.515 81.031 0.422 3.19 8 138.4 22.3 280 6 2 5 40.659 81.319 0.423 3.18 8 39.5 1.8 281 9 3 4 40.72 81.439 0.423 3.17 8 69.0 5.5 282 11 3 3 40.727 81.454 0.424 3.17 8 146.5 24.8 283 3 5 5 40.873 81.746 0.425 3.15 8 14.8 0.3 284 5 9 3 41.0 82.001 0.426 3.14 8 33.8 1.3 285 13 3 1 41.04 82.081 0.426 3.13 8 22.4 0.6 286 10 8 0 41.066 82.132 0.426 3.13 4 122.1 8.5 287 0 10 3 41.117 82.234 0.427 3.13 4 88.5 4.5 288 11 7 0 41.142 82.285 0.427 3.12 4 71.3 2.9 289 1 11 2 41.259 82.518 0.428 3.11 8 51.7 3.0 290 12 4 2 41.261 82.521 0.428 3.11 8 16.4 0.3 291 5 11 0 41.415 82.831 0.429 3.09 4 89.0 4.5 292 10 0 4 41.619 83.237 0.431 3.07 4 287.5 46.4 293 9 9 0 41.619 83.238 0.431 3.07 4 4.6 0.0 294 2 10 3 41.65 83.3 0.431 3.07 8 72.1 5.8 295 0 6 5 41.67 83.339 0.432 3.07 4 40.2 0.9 296 10 8 1 41.826 83.651 0.433 3.05 8 6.4 0.0 297 12 6 0 41.847 83.695 0.433 3.05 4 14.7 0.1 298 7 1 5 41.847 83.695 0.433 3.05 8 9.3 0.1 299 13 1 2 41.869 83.738 0.433 3.05 8 1.7 0.0 300 11 7 1 41.902 83.804 0.434 3.05 8 11.6 0.1 301 4 8 4 42.038 84.076 0.435 3.03 8 29.4 1.0 302 6 10 2 42.111 84.221 0.435 3.03 8 8.5 0.1 303 5 11 1 42.174 84.348 0.436 3.02 8 78.9 6.9 304 2 6 5 42.201 84.402 0.436 3.02 8 0.3 0.0 305 14 0 0 42.243 84.485 0.436 3.02 2 25.0 0.2 306 0 12 0 42.256 84.511 0.436 3.02 2 162.1 7.2 307 3 11 2 42.323 84.645 0.437 3.01 8 71.4 5.6 308 10 2 4 42.342 84.685 0.437 3.01 8 43.5 2.1 309 9 9 1 42.377 84.754 0.438 3.0 8 6.3 0.0 310 12 6 1 42.605 85.21 0.439 2.99 8 38.5 1.6 311 9 7 3 42.652 85.304 0.44 2.98 8 33.5 1.2 312 2 12 0 42.786 85.572 0.441 2.97 4 22.6 0.3 313 8 10 0 42.797 85.594 0.441 2.97 4 17.8 0.2 314 10 6 3 42.824 85.648 0.441 2.97 8 19.9 0.4 315 6 4 5 42.833 85.666 0.441 2.97 8 69.5 5.2 316 12 2 3 42.88 85.76 0.442 2.96 8 77.0 6.4 317 14 2 0 42.965 85.93 0.442 2.96 4 91.3 4.5 318 5 5 5 42.999 85.999 0.443 2.95 8 66.1 4.7 319 0 12 1 43.012 86.024 0.443 2.95 4 103.0 5.7 320 8 8 3 43.106 86.212 0.444 2.95 8 9.1 0.1 321 1 9 4 43.119 86.238 0.444 2.95 8 0.3 0.0 322 13 5 0 43.176 86.353 0.444 2.94 4 26.0 0.4 323 4 10 3 43.242 86.483 0.445 2.94 8 24.8 0.7 324 7 3 5 43.292 86.584 0.445 2.93 8 9.1 0.1 325 13 3 2 43.314 86.628 0.445 2.93 8 25.2 0.7 326 8 6 4 43.346 86.693 0.446 2.93 8 39.2 1.6 327 0 0 6 43.493 86.985 0.447 2.92 2 273.6 19.9 328 2 12 1 43.542 87.083 0.447 2.91 8 58.0 3.6 329 8 10 1 43.552 87.105 0.447 2.91 8 15.9 0.3 330 9 5 4 43.614 87.227 0.448 2.91 8 4.4 0.0 331 11 5 3 43.621 87.242 0.448 2.91 8 15.6 0.3 332 7 7 4 43.704 87.408 0.448 2.9 8 42.8 1.9 333 14 2 1 43.72 87.44 0.449 2.9 8 16.2 0.3 334 4 6 5 43.791 87.581 0.449 2.9 8 3.5 0.0 335 1 1 6 43.805 87.61 0.449 2.9 8 18.2 0.3 336 13 5 1 43.931 87.863 0.45 2.89 8 52.2 2.9 337 2 0 6 44.022 88.043 0.451 2.88 4 15.9 0.1 338 10 8 2 44.094 88.188 0.452 2.88 8 10.9 0.1 339 1 7 5 44.148 88.296 0.452 2.88 8 11.8 0.1 340 11 7 2 44.17 88.339 0.452 2.87 8 3.2 0.0 341 3 9 4 44.177 88.354 0.452 2.87 8 24.8 0.6 342 7 9 3 44.184 88.368 0.452 2.87 8 28.9 0.9 343 0 2 6 44.213 88.426 0.453 2.87 4 170.3 15.2 344 4 12 0 44.374 88.747 0.454 2.86 4 31.1 0.5 345 8 2 5 44.375 88.751 0.454 2.86 8 19.3 0.4 346 5 11 2 44.44 88.881 0.454 2.86 8 12.3 0.2 347 10 4 4 44.505 89.01 0.455 2.85 8 35.6 1.3 348 11 1 4 44.581 89.162 0.456 2.85 8 186.5 36.2 349 7 11 0 44.596 89.191 0.456 2.85 4 6.5 0.0 350 9 9 2 44.642 89.285 0.456 2.85 8 64.1 4.3 351 6 8 4 44.686 89.371 0.456 2.84 8 58.4 3.5 352 2 2 6 44.742 89.483 0.457 2.84 8 22.0 0.5 353 3 1 6 44.862 89.725 0.458 2.84 8 19.6 0.4 354 12 6 2 44.87 89.739 0.458 2.83 8 35.6 1.3 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 4.232 8.464 10.43784 487.7 52.7 53.7 5.6 2 2 0 0 5.511 11.022 8.0205 125.3 13.5 13.8 5.6 3 0 2 0 6.435 12.87 6.873 201.6 21.8 22.1 5.6 4 1 1 1 7.839 15.679 5.64729 16.6 1.8 1.8 5.6 5 2 2 0 8.488 16.975 5.21892 16.8 1.8 1.8 5.6 6 2 2 1 10.774 21.547 4.12071 87.9 9.5 9.6 5.6 7 4 0 0 11.074 22.148 4.01025 73.0 7.9 8.0 5.6 8 1 3 1 12.07 24.14 3.68368 27.1 2.9 3.0 5.6 9 3 3 0 12.791 25.581 3.47928 30.6 3.3 3.3 5.6 10 4 2 0 12.849 25.698 3.46375 19.8 2.1 2.2 5.6 11 0 4 0 12.953 25.905 3.4365 150.6 16.3 16.4 5.6 12 0 0 2 13.263 26.526 3.3575 368.8 39.9 40.1 5.6 13 1 1 2 13.945 27.891 3.19621 26.4 2.9 2.9 5.6 14 2 4 0 14.114 28.228 3.15876 15.8 1.7 1.7 5.6 15 5 1 0 14.273 28.547 3.12424 18.9 2.0 2.1 5.6 16 2 0 2 14.401 28.803 3.09708 14.3 1.5 1.6 5.6 17 4 2 1 14.491 28.982 3.07834 15.4 1.7 1.7 5.6 18 0 4 1 14.584 29.167 3.05917 56.7 6.1 6.2 5.6 19 0 2 2 14.793 29.586 3.01678 831.1 89.9 90.2 5.6 20 5 1 1 15.779 31.558 2.83265 65.4 7.1 7.1 5.6 21 2 2 2 15.831 31.661 2.82365 13.9 1.5 1.5 5.6 22 3 1 2 16.059 32.119 2.78447 54.9 5.9 5.9 5.6 23 1 5 0 16.515 33.03 2.70969 77.8 8.4 8.4 5.6 24 1 3 2 16.765 33.53 2.67045 32.3 3.5 3.5 5.7 25 5 3 0 17.044 34.087 2.62804 924.8 100.0 100.0 5.7 26 4 4 0 17.169 34.338 2.60946 33.8 3.7 3.7 5.7 27 4 2 2 18.633 37.267 2.4108 13.1 1.4 1.4 5.7 28 0 4 2 18.708 37.416 2.40155 137.1 14.8 14.8 5.7 29 2 4 2 19.561 39.122 2.30063 11.0 1.2 1.2 5.7 30 0 6 0 19.647 39.293 2.291 16.0 1.7 1.7 5.7 31 5 1 2 19.681 39.362 2.28719 83.2 9.0 8.9 5.7 32 0 2 3 21.218 42.436 2.12831 101.3 10.9 10.9 5.7 33 6 4 0 21.41 42.82 2.11013 372.0 40.2 39.9 5.7 34 5 5 0 21.653 43.306 2.08757 210.6 22.8 22.6 5.7 35 5 3 2 21.852 43.704 2.06947 67.4 7.3 7.2 5.7 36 2 2 3 21.99 43.98 2.05712 21.7 2.3 2.3 5.7 37 6 4 1 22.497 44.994 2.01308 20.7 2.2 2.2 5.7 38 5 5 1 22.731 45.462 1.99346 73.7 8.0 7.9 5.7 39 0 6 2 24.019 48.037 1.89242 25.5 2.8 2.7 5.7 40 0 4 3 24.248 48.497 1.87557 76.4 8.3 8.1 5.7 41 5 5 2 25.753 51.506 1.77283 102.6 11.1 10.9 5.8 42 9 1 0 25.836 51.672 1.76754 36.9 4.0 3.9 5.8 43 7 5 0 25.951 51.901 1.76025 11.9 1.3 1.3 5.8 44 0 8 0 26.634 53.268 1.71825 48.6 5.3 5.2 5.8 45 4 6 2 26.749 53.498 1.71143 22.5 2.4 2.4 5.8 46 5 3 3 26.874 53.748 1.70403 52.8 5.7 5.6 5.8 47 6 6 1 27.219 54.439 1.68404 39.0 4.2 4.1 5.8 48 0 0 4 27.312 54.625 1.67875 301.5 32.6 31.9 5.8 49 5 7 0 27.381 54.762 1.67487 27.8 3.0 2.9 5.8 50 6 2 3 27.555 55.11 1.66511 40.3 4.4 4.3 5.8 51 9 3 0 27.627 55.255 1.66109 10.2 1.1 1.1 5.8 52 5 7 1 28.294 56.588 1.62508 10.2 1.1 1.1 5.8 53 10 0 0 28.698 57.396 1.6041 87.0 9.4 9.2 5.8 54 6 6 2 29.913 59.826 1.54462 139.5 15.1 14.6 5.8 55 5 5 3 30.302 60.604 1.52665 10.9 1.2 1.1 5.8 56 7 3 3 30.636 61.272 1.51159 18.7 2.0 2.0 5.8 57 8 6 0 30.698 61.395 1.50885 9.4 1.0 1.0 5.8 58 5 7 2 30.927 61.855 1.49874 425.4 46.0 44.5 5.8 59 9 3 2 31.156 62.312 1.48884 39.2 4.2 4.1 5.8 60 1 9 1 31.294 62.589 1.48292 21.0 2.3 2.2 5.8 61 8 2 3 31.856 63.712 1.45944 9.4 1.0 1.0 5.9 62 11 1 0 32.085 64.17 1.45014 91.7 9.9 9.6 5.9 63 10 0 2 32.153 64.306 1.44739 19.8 2.1 2.1 5.9 64 1 5 4 32.667 65.335 1.42707 17.1 1.8 1.8 5.9 65 11 1 1 32.917 65.834 1.41746 12.5 1.4 1.3 5.9 66 10 2 2 32.947 65.893 1.41633 32.9 3.6 3.4 5.9 67 5 3 4 32.988 65.976 1.41474 212.9 23.0 22.1 5.9 68 7 5 3 33.828 67.656 1.38365 13.6 1.5 1.4 5.9 69 5 9 0 33.957 67.913 1.37903 31.3 3.4 3.2 5.9 70 6 6 3 34.11 68.22 1.37357 28.0 3.0 2.9 5.9 71 0 6 4 34.669 69.339 1.35412 35.1 3.8 3.6 5.9 72 0 10 1 34.889 69.778 1.34667 14.1 1.5 1.5 5.9 73 5 7 3 35.058 70.116 1.34101 28.1 3.0 2.9 5.9 74 10 4 2 35.272 70.544 1.33391 65.8 7.1 6.8 5.9 75 2 10 1 35.45 70.9 1.32808 12.2 1.3 1.3 5.9 76 9 7 0 35.707 71.415 1.31978 9.8 1.1 1.0 5.9 77 6 4 4 35.897 71.795 1.31372 82.5 8.9 8.5 5.9 78 5 5 4 36.072 72.144 1.30822 35.1 3.8 3.6 5.9 79 12 2 1 36.736 73.473 1.28781 13.9 1.5 1.4 6.0 80 11 3 2 36.864 73.728 1.28397 38.0 4.1 3.9 6.0 81 0 10 2 37.266 74.531 1.27211 141.9 15.3 14.5 6.0 82 11 1 3 39.265 78.53 1.21704 41.4 4.5 4.2 6.0 83 0 8 4 39.903 79.805 1.20078 23.1 2.5 2.3 6.0 84 5 7 4 40.515 81.031 1.18568 22.3 2.4 2.3 6.1 85 11 3 3 40.727 81.454 1.18059 30.3 3.3 3.1 6.1 86 10 0 4 41.619 83.237 1.15976 46.4 5.0 4.7 6.1 87 0 12 1 43.012 86.024 1.12919 10.4 1.1 1.0 6.1 88 0 0 6 43.493 86.985 1.11917 19.9 2.2 2.0 6.1 89 0 2 6 44.213 88.426 1.10462 15.2 1.6 1.5 6.2 90 11 1 4 44.581 89.162 1.0974 36.2 3.9 3.6 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |