Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** JASKOLSKIITE 1, f-meneghinite, DN Cu(0.2)Pb(2.2)Sb(1.2)Bi(0.6)S(5) Orthorhombic P bnm Z = 4 R =0.072 NR =472 1 .2 .1989 Ref.Str.: E. Makovsky, R. Norrestam (1985) * Z. Kristallogr., 171, 179-194 Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 11.312 alpha = 90.0 b = 19.829 beta = 90.0 c = 4.088 gamma = 90.0 Unit cell volume (cub. angs.) = 916.96 Molar volume ( cub.cm/mol.) = 138.08 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.3014 0.9763 0.25 0.0 Sb = 0.71, Pb = 0.29 2 0.3753 0.1281 0.75 0.0 Sb = 0.6 , Bi = 0.4 3 0.4991 0.4043 0.75 0.0 Bi = 0.2 , Pb = 0.8 4 0.1688 0.2923 0.75 0.0 Pb = 1.00 5 0.3915 0.2587 0.25 0.0 Cu = 0.16, Cu = 0.0 6 0.6285 0.4764 0.25 0.0 S = 1.00 7 0.5632 0.0793 0.25 0.0 S = 1.00 8 0.2467 0.1711 0.25 0.0 S = 1.00 9 0.4948 0.2335 0.75 0.0 S = 1.00 10 0.3184 0.368 0.25 0.0 S = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.3014 0.9763 0.25 2 2 0.3753 0.1281 0.75 3 3 0.4991 0.4043 0.75 4 4 0.1688 0.2923 0.75 5 5 0.3915 0.2587 0.25 6 6 0.6285 0.4764 0.25 7 7 0.5632 0.0793 0.25 8 8 0.2467 0.1711 0.25 9 9 0.4948 0.2335 0.75 10 10 0.3184 0.368 0.25 11 1 0.6986 0.0237 0.75 12 2 0.6247 0.8719 0.25 13 3 0.5009 0.5957 0.25 14 4 0.8312 0.7077 0.25 15 5 0.6085 0.7413 0.75 16 6 0.3715 0.5236 0.75 17 7 0.4368 0.9207 0.75 18 8 0.7533 0.8289 0.75 19 9 0.5052 0.7665 0.25 20 10 0.6816 0.632 0.75 21 1 0.1986 0.4763 0.25 22 2 0.1247 0.6281 0.75 23 3 0.0009 0.9043 0.75 24 4 0.3312 0.7923 0.75 25 5 0.1085 0.7587 0.25 26 6 0.8715 0.9764 0.25 27 7 0.9368 0.5793 0.25 28 8 0.2533 0.6711 0.25 29 9 0.0052 0.7335 0.75 30 10 0.1816 0.868 0.25 31 1 0.8014 0.5237 0.75 32 2 0.8753 0.3719 0.25 33 3 0.9991 0.0957 0.25 34 4 0.6688 0.2077 0.25 35 5 0.8915 0.2413 0.75 36 6 0.1285 0.0236 0.75 37 7 0.0632 0.4207 0.75 38 8 0.7467 0.3289 0.75 39 9 0.9948 0.2665 0.25 40 10 0.8184 0.132 0.75 X-ray density (g/cm cub.) = 6.43 MU (1/cm) = 1364.58 Mass attenuation coefficient (cm**2/g) = 212.117 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Sb ,Pb 3.696 6 3.5975 7 2.782 7 2.782 7 2.5393 10 2.9804 6 2.9804 6 2 Sb ,Bi 3.624 6 3.1036 7 3.1036 7 2.6497 8 2.6497 8 2.489 9 3.4768 6 3 Bi ,Pb 3.696 7 2.8921 6 2.8921 6 3.3871 9 2.979 10 2.979 10 2.7712 6 3.1749 8 4 Pb 3.696 7 3.2757 8 3.2757 8 3.0488 10 3.0488 10 2.8123 7 2.8834 9 2.8834 9 5 Cu ,Cu 3.36 4 2.3875 8 2.4069 9 2.4069 9 2.3197 10 6 S 4.368 10 4.088 6 4.088 6 4.114 10 3.675 6 3.675 6 3.7495 10 3.7495 10 4.0405 7 3.8105 8 3.8105 8 7 S 4.368 10 4.088 7 4.088 7 4.0164 8 3.7584 9 3.7584 9 4.0141 7 4.0141 7 4.0405 6 3.6883 10 3.6883 10 8 S 4.368 9 4.0164 7 4.088 8 4.088 8 3.6858 9 3.6858 9 3.9877 10 3.8105 6 3.8105 6 3.4202 9 9 S 4.368 10 3.7584 7 3.7584 7 3.6858 8 3.6858 8 4.088 9 4.088 9 3.908 10 3.908 10 3.4202 8 4.1774 10 10 S 4.368 11 4.114 6 3.9877 8 3.908 9 3.908 9 4.088 10 4.088 10 3.7495 6 3.7495 6 3.6883 7 3.6883 7 4.1774 9 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 2 0 4.456 8.912 0.05 328.36 2 33.2 86.2 2 1 1 0 4.496 8.993 0.051 322.44 4 25.9 103.1 3 1 2 0 5.93 11.86 0.067 184.42 4 40.8 145.9 4 1 3 0 7.757 15.514 0.088 106.83 4 123.6 776.1 5 2 0 0 7.827 15.655 0.088 104.88 2 30.7 23.5 6 2 1 0 8.142 16.283 0.092 96.78 4 69.6 223.0 7 0 4 0 8.939 17.878 0.101 79.9 2 111.3 235.2 8 2 2 0 9.021 18.041 0.102 78.42 4 64.8 156.5 9 1 4 0 9.767 19.535 0.11 66.57 4 53.2 89.5 10 2 3 0 10.326 20.651 0.116 59.34 4 211.6 1264.2 11 1 0 1 11.558 23.115 0.13 46.94 4 154.0 529.7 12 0 2 1 11.76 23.52 0.132 45.26 4 130.8 368.6 13 1 1 1 11.776 23.552 0.132 45.14 8 146.4 920.5 14 1 5 0 11.878 23.755 0.134 44.33 4 329.1 2284.7 15 2 4 0 11.924 23.849 0.134 43.97 4 327.9 2248.4 16 3 1 0 12.002 24.004 0.135 43.37 4 483.5 4824.3 17 1 2 1 12.409 24.818 0.139 40.44 8 314.0 3795.0 18 3 2 0 12.624 25.249 0.142 39.0 4 130.3 315.1 19 1 3 1 13.402 26.804 0.15 34.38 8 379.3 4705.0 20 0 6 0 13.478 26.957 0.151 33.97 2 97.6 76.9 21 3 3 0 13.603 27.205 0.153 33.31 4 199.1 628.1 22 2 1 1 13.634 27.267 0.153 33.15 8 97.2 297.9 23 2 5 0 13.722 27.445 0.154 32.7 4 375.0 2188.1 24 1 6 0 14.053 28.106 0.158 31.09 4 460.9 3142.2 25 0 4 1 14.136 28.273 0.159 30.7 4 147.3 316.8 26 2 2 1 14.189 28.379 0.159 30.45 8 239.3 1659.0 27 1 4 1 14.687 29.375 0.165 28.29 8 114.5 352.8 28 3 4 0 14.872 29.744 0.167 27.55 4 59.4 46.2 29 2 3 1 15.074 30.147 0.169 26.76 8 506.5 6531.3 30 2 6 0 15.661 31.322 0.175 24.65 4 474.7 2642.8 31 4 0 0 15.806 31.611 0.177 24.17 2 17.7 1.8 32 4 1 0 15.97 31.94 0.179 23.64 4 219.7 542.8 33 3 0 1 16.136 32.271 0.18 23.11 4 381.3 1598.8 34 1 5 1 16.203 32.406 0.181 22.91 8 69.6 105.7 35 2 4 1 16.238 32.477 0.182 22.8 8 477.3 4941.6 36 1 7 0 16.279 32.559 0.182 22.68 4 48.9 25.8 37 3 1 1 16.297 32.594 0.182 22.62 8 358.7 2769.2 38 3 5 0 16.372 32.745 0.183 22.4 4 4.8 0.2 39 4 2 0 16.454 32.907 0.184 22.16 4 154.3 251.1 40 3 2 1 16.772 33.544 0.187 21.26 8 145.6 428.7 41 4 3 0 17.233 34.466 0.192 20.04 4 160.8 246.6 42 0 6 1 17.44 34.881 0.195 19.52 4 187.6 326.9 43 3 3 1 17.539 35.078 0.196 19.28 8 116.9 250.7 44 2 5 1 17.635 35.269 0.197 19.05 8 68.3 84.5 45 2 7 0 17.705 35.411 0.197 18.89 4 350.4 1103.2 46 1 6 1 17.9 35.799 0.2 18.44 8 137.8 333.1 47 3 6 0 18.055 36.11 0.201 18.1 4 50.9 22.3 48 0 8 0 18.106 36.211 0.202 17.99 2 202.2 174.9 49 4 4 0 18.275 36.55 0.204 17.62 4 24.7 5.1 50 1 8 0 18.551 37.101 0.207 17.05 4 112.4 102.5 51 3 4 1 18.566 37.133 0.207 17.02 8 93.7 142.0 52 2 6 1 19.221 38.441 0.214 15.77 8 186.4 521.1 53 4 1 1 19.479 38.959 0.216 15.31 8 126.5 233.1 54 4 5 0 19.544 39.089 0.217 15.19 4 195.7 276.7 55 1 7 1 19.741 39.481 0.219 14.86 8 316.1 1412.4 56 3 5 1 19.82 39.639 0.22 14.73 8 121.2 205.9 57 2 8 0 19.834 39.668 0.22 14.71 4 54.2 20.6 58 3 7 0 19.883 39.767 0.221 14.62 4 184.4 236.4 59 4 2 1 19.888 39.777 0.221 14.62 8 407.1 2305.2 60 5 1 0 20.04 40.08 0.222 14.37 4 95.6 62.5 61 5 2 0 20.44 40.879 0.227 13.75 4 17.3 2.0 62 4 3 1 20.555 41.11 0.228 13.58 8 360.2 1676.4 63 1 9 0 20.866 41.732 0.231 13.13 4 21.6 2.9 64 2 7 1 20.963 41.926 0.232 13.0 8 130.7 211.3 65 4 6 0 21.007 42.015 0.233 12.94 4 223.7 308.1 66 5 3 0 21.092 42.184 0.234 12.82 4 266.1 432.0 67 3 6 1 21.267 42.534 0.235 12.59 8 108.7 141.4 68 0 8 1 21.311 42.622 0.236 12.53 4 672.7 2697.0 69 4 4 1 21.459 42.918 0.237 12.33 8 218.1 558.4 70 1 8 1 21.7 43.401 0.24 12.03 8 56.8 36.9 71 3 8 0 21.833 43.666 0.241 11.86 4 142.0 113.8 72 5 4 0 21.978 43.956 0.243 11.69 4 266.3 394.4 73 2 9 0 22.037 44.074 0.244 11.62 4 234.0 302.7 74 0 0 2 22.139 44.277 0.245 11.5 2 1082.1 3202.7 75 4 5 1 22.579 45.157 0.249 11.0 8 86.2 77.7 76 0 2 2 22.63 45.259 0.25 10.94 4 22.3 2.6 77 4 7 0 22.636 45.272 0.25 10.94 4 233.8 284.3 78 1 1 2 22.639 45.277 0.25 10.93 8 24.0 6.0 79 2 8 1 22.837 45.674 0.252 10.72 8 11.7 1.4 80 0 10 0 22.859 45.718 0.252 10.7 2 380.9 369.2 81 3 7 1 22.881 45.762 0.252 10.67 8 215.0 469.5 82 5 0 1 22.901 45.801 0.253 10.65 4 321.1 522.6 83 1 2 2 23.001 46.003 0.254 10.55 8 32.9 10.8 84 5 1 1 23.021 46.042 0.254 10.53 8 19.7 3.9 85 5 5 0 23.078 46.155 0.254 10.47 4 657.1 2150.5 86 1 10 0 23.228 46.455 0.256 10.32 4 166.3 135.8 87 5 2 1 23.379 46.758 0.258 10.17 8 187.2 339.0 88 1 3 2 23.596 47.193 0.26 9.96 8 95.6 86.6 89 2 0 2 23.622 47.244 0.26 9.93 4 21.5 2.2 90 2 1 2 23.74 47.479 0.261 9.82 8 59.1 32.6 91 1 9 1 23.763 47.526 0.262 9.8 8 72.0 48.3 92 3 9 0 23.886 47.773 0.263 9.68 4 374.0 644.4 93 4 6 1 23.891 47.781 0.263 9.68 8 425.5 1667.4 94 5 3 1 23.967 47.934 0.264 9.61 8 268.3 658.1 95 0 4 2 24.056 48.112 0.265 9.53 4 90.2 36.9 96 2 2 2 24.09 48.179 0.265 9.5 8 56.1 28.5 97 6 0 0 24.115 48.229 0.265 9.48 2 538.4 653.4 98 6 1 0 24.23 48.461 0.266 9.37 4 171.0 130.4 99 2 10 0 24.308 48.616 0.267 9.31 4 113.5 57.0 100 5 6 0 24.369 48.737 0.268 9.25 4 295.8 385.3 101 4 8 0 24.408 48.817 0.268 9.22 4 116.5 59.5 102 1 4 2 24.411 48.822 0.268 9.22 8 51.0 22.8 103 6 2 0 24.575 49.15 0.27 9.08 4 80.6 28.1 104 3 8 1 24.64 49.279 0.271 9.02 8 131.5 148.4 105 2 3 2 24.665 49.329 0.271 9.0 8 178.3 272.3 106 5 4 1 24.772 49.544 0.272 8.91 8 2.1 0.0 107 2 9 1 24.826 49.651 0.273 8.87 8 219.6 406.9 108 6 3 0 25.142 50.284 0.276 8.62 4 163.1 109.1 109 4 7 1 25.374 50.748 0.278 8.44 8 211.4 359.0 110 1 5 2 25.429 50.858 0.279 8.4 8 278.0 617.7 111 2 4 2 25.453 50.907 0.279 8.38 8 281.1 629.9 112 3 1 2 25.494 50.988 0.279 8.35 8 410.8 1340.5 113 0 10 1 25.579 51.157 0.28 8.29 4 491.8 953.7 114 1 11 0 25.639 51.278 0.281 8.24 4 346.0 469.5 115 5 5 1 25.78 51.56 0.282 8.14 8 311.5 751.4 116 3 2 2 25.826 51.652 0.283 8.11 8 113.2 98.9 117 5 7 0 25.832 51.664 0.283 8.1 4 62.3 15.0 118 1 10 1 25.918 51.836 0.284 8.04 8 180.7 249.8 119 6 4 0 25.92 51.84 0.284 8.04 4 18.3 1.3 120 3 10 0 26.034 52.067 0.285 7.96 4 330.9 414.6 121 0 6 2 26.302 52.604 0.288 7.78 4 84.9 26.7 122 4 9 0 26.308 52.616 0.288 7.77 4 16.7 1.0 123 3 3 2 26.373 52.746 0.288 7.73 8 170.8 214.5 124 2 5 2 26.442 52.885 0.289 7.68 8 305.0 680.2 125 3 9 1 26.527 53.054 0.29 7.63 8 480.5 1675.7 126 1 6 2 26.635 53.27 0.291 7.56 8 393.7 1114.6 127 2 11 0 26.647 53.293 0.291 7.55 4 216.1 167.7 128 6 1 1 26.846 53.692 0.293 7.42 8 204.1 294.2 129 6 5 0 26.897 53.793 0.294 7.39 4 20.5 1.5 130 2 10 1 26.918 53.836 0.294 7.38 8 16.6 1.9 131 5 6 1 26.975 53.949 0.294 7.34 8 113.4 89.8 132 4 8 1 27.012 54.023 0.295 7.32 8 68.3 32.4 133 3 4 2 27.126 54.252 0.296 7.25 8 48.3 16.1 134 6 2 1 27.167 54.333 0.296 7.22 8 219.9 332.4 135 5 8 0 27.45 54.9 0.299 7.06 4 140.1 65.8 136 2 6 2 27.617 55.234 0.301 6.96 8 393.2 1023.6 137 6 3 1 27.695 55.39 0.302 6.92 8 4.4 0.1 138 4 0 2 27.709 55.418 0.302 6.91 4 12.8 0.5 139 0 12 0 27.785 55.57 0.303 6.86 2 244.8 97.9 140 4 1 2 27.814 55.627 0.303 6.85 8 191.2 238.3 141 1 7 2 28.013 56.026 0.305 6.74 8 48.9 15.3 142 6 6 0 28.058 56.117 0.305 6.71 4 181.2 104.9 143 3 5 2 28.074 56.148 0.305 6.71 8 4.3 0.1 144 1 12 0 28.106 56.212 0.306 6.69 4 128.1 52.2 145 4 2 2 28.127 56.254 0.306 6.68 8 140.6 125.6 146 1 11 1 28.161 56.321 0.306 6.66 8 72.2 33.0 147 3 11 0 28.27 56.54 0.307 6.6 4 114.0 40.8 148 4 10 0 28.323 56.645 0.308 6.57 4 146.8 67.3 149 5 7 1 28.342 56.683 0.308 6.56 8 23.0 3.3 150 6 4 1 28.424 56.849 0.309 6.52 8 53.0 17.4 151 3 10 1 28.531 57.062 0.31 6.46 8 14.6 1.3 152 7 1 0 28.57 57.141 0.31 6.44 4 252.1 194.8 153 4 3 2 28.644 57.287 0.311 6.41 8 133.8 109.1 154 4 9 1 28.789 57.578 0.313 6.33 8 115.0 79.7 155 7 2 0 28.878 57.756 0.313 6.29 4 347.3 361.0 156 2 7 2 28.964 57.928 0.314 6.25 8 297.1 524.6 157 2 12 0 29.054 58.109 0.315 6.2 4 302.4 270.0 158 2 11 1 29.108 58.216 0.316 6.18 8 197.3 228.8 159 3 6 2 29.204 58.409 0.317 6.13 8 43.9 11.2 160 5 9 0 29.21 58.419 0.317 6.13 4 57.3 9.6 161 0 8 2 29.239 58.479 0.317 6.12 4 170.8 84.9 162 6 5 1 29.344 58.688 0.318 6.07 8 23.0 3.0 163 4 4 2 29.357 58.715 0.318 6.06 8 23.0 3.1 164 7 3 0 29.386 58.773 0.319 6.05 4 266.6 204.5 165 6 7 0 29.392 58.784 0.319 6.04 4 7.0 0.1 166 1 8 2 29.55 59.1 0.32 5.97 8 95.2 51.5 167 5 8 1 29.868 59.735 0.323 5.83 8 1.1 0.0 168 7 4 0 30.089 60.178 0.325 5.74 4 130.9 46.8 169 0 12 1 30.185 60.37 0.326 5.69 4 96.9 25.5 170 4 5 2 30.259 60.519 0.327 5.66 8 168.2 152.5 171 6 6 1 30.445 60.89 0.329 5.59 8 71.0 26.8 172 4 11 0 30.447 60.893 0.329 5.59 4 356.9 338.6 173 2 8 2 30.47 60.94 0.329 5.58 8 47.2 11.8 174 1 12 1 30.49 60.98 0.329 5.57 8 278.9 412.1 175 3 7 2 30.506 61.012 0.33 5.56 8 161.3 137.7 176 3 12 0 30.594 61.188 0.33 5.53 4 77.6 15.8 177 5 1 2 30.621 61.242 0.331 5.52 8 83.9 37.0 178 1 13 0 30.635 61.27 0.331 5.51 4 47.7 6.0 179 3 11 1 30.646 61.292 0.331 5.51 8 118.0 73.0 180 4 10 1 30.696 61.392 0.331 5.49 8 0.0 0.0 181 7 0 1 30.834 61.668 0.333 5.43 4 2.7 0.0 182 6 8 0 30.886 61.771 0.333 5.41 4 14.1 0.5 183 5 2 2 30.916 61.832 0.334 5.4 8 15.1 1.2 184 7 1 1 30.932 61.864 0.334 5.39 8 147.4 111.4 185 7 5 0 30.978 61.956 0.334 5.38 4 163.0 67.9 186 5 10 0 31.101 62.202 0.335 5.33 4 29.5 2.2 187 7 2 1 31.225 62.451 0.337 5.28 8 308.8 479.3 188 1 9 2 31.234 62.469 0.337 5.28 8 17.6 1.6 189 4 6 2 31.341 62.681 0.338 5.24 8 194.9 189.4 190 2 12 1 31.394 62.787 0.338 5.22 8 298.5 442.5 191 5 3 2 31.404 62.808 0.338 5.22 8 229.0 260.3 192 2 13 0 31.536 63.073 0.34 5.17 4 110.7 30.2 193 5 9 1 31.542 63.084 0.34 5.17 8 12.1 0.7 194 7 3 1 31.711 63.422 0.341 5.11 8 291.0 411.4 195 6 7 1 31.716 63.432 0.341 5.1 8 208.1 210.2 196 3 8 2 31.969 63.937 0.344 5.02 8 122.8 72.0 197 7 6 0 32.045 64.091 0.344 4.99 4 132.2 41.5 198 5 4 2 32.081 64.161 0.345 4.98 8 230.4 251.6 199 2 9 2 32.126 64.252 0.345 4.96 8 204.8 198.2 200 7 4 1 32.384 64.767 0.348 4.88 8 142.6 94.4 201 6 9 0 32.529 65.059 0.349 4.83 4 199.5 91.5 202 4 7 2 32.592 65.184 0.35 4.81 8 203.4 189.3 203 4 12 0 32.677 65.353 0.35 4.78 4 421.9 405.2 204 4 11 1 32.727 65.454 0.351 4.77 8 73.4 24.4 205 0 10 2 32.767 65.533 0.351 4.76 4 336.4 256.1 206 3 12 1 32.868 65.737 0.352 4.72 8 79.4 28.3 207 1 13 1 32.908 65.816 0.353 4.71 8 244.1 267.2 208 5 5 2 32.939 65.878 0.353 4.7 8 575.7 1483.3 209 0 14 0 32.946 65.892 0.353 4.7 2 21.7 0.5 210 8 0 0 33.008 66.016 0.354 4.68 2 163.9 29.9 211 3 13 0 33.008 66.016 0.354 4.68 4 196.1 85.6 212 1 10 2 33.058 66.116 0.354 4.67 8 145.3 93.7 213 8 1 0 33.102 66.205 0.355 4.65 4 137.9 42.1 214 5 11 0 33.118 66.236 0.355 4.65 4 162.5 58.4 215 6 8 1 33.149 66.297 0.355 4.64 8 441.6 860.9 216 1 14 0 33.236 66.472 0.356 4.61 4 82.5 15.0 217 7 5 1 33.238 66.476 0.356 4.61 8 132.1 76.6 218 7 7 0 33.282 66.565 0.356 4.6 4 49.1 5.3 219 5 10 1 33.356 66.712 0.357 4.58 8 126.5 69.7 220 8 2 0 33.385 66.77 0.357 4.57 4 10.0 0.2 221 3 9 2 33.584 67.167 0.359 4.51 8 331.0 470.5 222 6 0 2 33.767 67.535 0.361 4.46 4 475.5 479.9 223 2 13 1 33.776 67.552 0.361 4.46 8 64.5 17.7 224 8 3 0 33.854 67.708 0.362 4.44 4 166.2 58.3 225 6 1 2 33.861 67.722 0.362 4.44 8 150.7 95.9 226 2 10 2 33.924 67.848 0.362 4.42 8 100.4 42.4 227 5 6 2 33.973 67.946 0.363 4.41 8 262.0 287.7 228 4 8 2 34.005 68.01 0.363 4.4 8 101.9 43.5 229 2 14 0 34.1 68.2 0.364 4.37 4 117.0 28.5 230 6 2 2 34.141 68.281 0.364 4.36 8 71.2 21.0 231 7 6 1 34.267 68.535 0.365 4.33 8 95.1 37.2 232 6 10 0 34.316 68.633 0.366 4.32 4 370.6 281.9 233 8 4 0 34.505 69.01 0.368 4.27 4 383.7 298.9 234 6 3 2 34.605 69.209 0.369 4.24 8 143.6 83.2 235 7 8 0 34.682 69.363 0.369 4.22 4 5.2 0.1 236 1 0 3 34.706 69.411 0.37 4.22 4 119.8 28.8 237 6 9 1 34.736 69.471 0.37 4.21 8 111.7 49.9 238 0 2 3 34.791 69.582 0.37 4.2 4 100.0 20.0 239 1 1 3 34.798 69.596 0.37 4.19 8 105.4 44.3 240 4 12 1 34.878 69.756 0.371 4.17 8 152.1 91.9 241 4 13 0 35.014 70.027 0.372 4.14 4 0.8 0.0 242 1 11 2 35.015 70.031 0.372 4.14 8 307.1 371.6 243 1 2 3 35.074 70.148 0.373 4.13 8 238.0 222.5 244 0 14 1 35.139 70.278 0.374 4.11 4 84.1 13.8 245 5 7 2 35.176 70.352 0.374 4.1 8 55.1 11.9 246 3 13 1 35.199 70.398 0.374 4.1 8 8.6 0.3 247 6 4 2 35.249 70.499 0.375 4.09 8 15.4 0.9 248 5 12 0 35.257 70.515 0.375 4.08 4 13.9 0.4 249 8 1 1 35.291 70.582 0.375 4.08 8 110.5 47.4 250 5 11 1 35.306 70.612 0.375 4.07 8 19.6 1.5 251 8 5 0 35.334 70.668 0.375 4.07 4 0.2 0.0 252 3 10 2 35.344 70.689 0.376 4.06 8 291.8 329.3 253 1 14 1 35.421 70.842 0.376 4.05 8 263.0 266.4 254 7 7 1 35.466 70.931 0.377 4.04 8 437.7 735.6 255 3 14 0 35.517 71.034 0.377 4.02 4 76.0 11.1 256 1 3 3 35.533 71.065 0.377 4.02 8 294.9 332.8 257 8 2 1 35.565 71.131 0.378 4.01 8 23.4 2.1 258 4 9 2 35.574 71.148 0.378 4.01 8 13.7 0.7 259 2 1 3 35.644 71.288 0.378 4.0 8 72.4 19.9 260 2 11 2 35.859 71.718 0.38 3.95 8 192.2 138.8 261 0 4 3 35.891 71.781 0.381 3.94 4 109.2 22.3 262 2 2 3 35.917 71.834 0.381 3.94 8 178.8 119.8 263 1 15 0 35.92 71.84 0.381 3.94 4 320.0 191.8 264 8 3 1 36.021 72.042 0.382 3.91 8 52.5 10.3 265 6 5 2 36.071 72.141 0.382 3.9 8 18.4 1.3 266 1 4 3 36.17 72.34 0.383 3.88 8 90.0 29.9 267 7 9 0 36.237 72.474 0.384 3.87 4 13.2 0.3 268 6 11 0 36.242 72.484 0.384 3.87 4 174.2 55.8 269 2 14 1 36.26 72.521 0.384 3.87 8 278.7 285.6 270 8 6 0 36.336 72.672 0.385 3.85 4 202.1 74.8 271 2 3 3 36.371 72.742 0.385 3.84 8 374.7 513.4 272 6 10 1 36.471 72.942 0.386 3.82 8 10.1 0.4 273 5 8 2 36.542 73.084 0.386 3.81 8 125.3 56.8 274 8 4 1 36.655 73.31 0.388 3.79 8 254.7 233.7 275 2 15 0 36.755 73.51 0.388 3.77 4 317.4 180.5 276 7 8 1 36.827 73.654 0.389 3.75 8 295.1 310.8 277 0 12 2 36.829 73.658 0.389 3.75 4 218.2 85.0 278 3 0 3 36.945 73.891 0.39 3.73 4 277.8 136.9 279 1 5 3 36.983 73.966 0.39 3.72 8 53.5 10.1 280 2 4 3 37.003 74.005 0.391 3.72 8 357.6 452.6 281 3 1 3 37.035 74.071 0.391 3.71 8 270.9 259.3 282 6 6 2 37.065 74.129 0.391 3.71 8 162.4 93.1 283 1 12 2 37.105 74.211 0.392 3.7 8 113.8 45.6 284 4 13 1 37.151 74.302 0.392 3.69 8 50.0 8.8 285 3 11 2 37.247 74.495 0.393 3.67 8 102.4 36.7 286 4 10 2 37.293 74.586 0.393 3.67 8 131.4 60.2 287 3 2 3 37.305 74.61 0.393 3.66 8 109.0 41.4 288 5 12 1 37.389 74.778 0.394 3.65 8 267.6 248.5 289 4 14 0 37.462 74.925 0.395 3.64 4 255.9 113.3 290 8 5 1 37.464 74.928 0.395 3.64 8 215.6 160.7 291 8 7 0 37.506 75.013 0.395 3.63 4 10.6 0.2 292 7 1 2 37.508 75.016 0.395 3.63 8 225.5 175.5 293 5 13 0 37.521 75.042 0.395 3.63 4 13.5 0.3 294 3 14 1 37.643 75.286 0.396 3.6 8 19.9 1.4 295 0 6 3 37.694 75.387 0.397 3.6 4 145.1 36.0 296 3 3 3 37.752 75.504 0.397 3.59 8 87.1 25.9 297 7 2 2 37.776 75.553 0.398 3.58 8 310.8 329.1 298 2 5 3 37.809 75.618 0.398 3.58 8 45.6 7.1 299 9 1 0 37.885 75.77 0.399 3.56 4 137.3 31.9 300 2 12 2 37.93 75.861 0.399 3.56 8 271.3 248.9 301 7 10 0 37.945 75.89 0.399 3.55 4 277.2 129.8 302 1 6 3 37.968 75.936 0.399 3.55 8 102.0 35.1 303 1 15 1 38.037 76.075 0.4 3.54 8 40.4 5.5 304 5 9 2 38.067 76.133 0.4 3.53 8 51.5 8.9 305 3 15 0 38.131 76.262 0.401 3.52 4 5.1 0.0 306 9 2 0 38.152 76.304 0.401 3.52 4 224.4 84.3 307 7 3 2 38.222 76.444 0.402 3.51 8 238.4 189.7 308 6 7 2 38.227 76.453 0.402 3.51 8 6.0 0.1 309 6 12 0 38.306 76.612 0.402 3.49 4 162.2 43.8 310 7 9 1 38.348 76.696 0.403 3.49 8 144.5 69.2 311 6 11 1 38.353 76.705 0.403 3.49 8 128.4 54.7 312 3 4 3 38.376 76.751 0.403 3.48 8 71.8 17.1 313 0 16 0 38.429 76.857 0.403 3.48 2 243.3 48.9 314 8 6 1 38.445 76.889 0.404 3.47 8 35.0 4.0 315 9 3 0 38.596 77.193 0.405 3.45 4 97.7 15.7 316 1 16 0 38.701 77.402 0.406 3.43 4 259.2 109.7 317 2 6 3 38.787 77.574 0.407 3.42 8 144.7 68.1 318 8 8 0 38.841 77.682 0.407 3.41 4 198.5 64.0 319 7 4 2 38.843 77.686 0.407 3.41 8 118.2 45.4 320 2 15 1 38.856 77.711 0.407 3.41 8 358.0 416.0 321 4 1 3 38.952 77.905 0.408 3.4 8 96.0 29.8 322 1 7 3 39.121 78.242 0.41 3.37 8 246.1 194.3 323 4 11 2 39.161 78.322 0.41 3.37 8 320.7 329.4 324 3 5 3 39.173 78.345 0.41 3.36 8 94.8 28.8 325 9 4 0 39.215 78.431 0.41 3.36 4 32.0 1.6 326 4 2 3 39.217 78.435 0.41 3.36 8 315.9 318.9 327 3 12 2 39.293 78.585 0.411 3.35 8 69.5 15.4 328 1 13 2 39.33 78.659 0.411 3.34 8 42.3 5.7 329 2 16 0 39.515 79.031 0.413 3.32 4 81.7 10.5 330 4 14 1 39.551 79.101 0.413 3.31 8 54.3 9.3 331 6 8 2 39.554 79.108 0.413 3.31 8 13.0 0.5 332 8 7 1 39.594 79.187 0.414 3.31 8 109.5 37.7 333 5 13 1 39.608 79.216 0.414 3.31 8 594.4 1111.0 334 7 5 2 39.637 79.274 0.414 3.3 8 148.0 68.8 335 4 3 3 39.658 79.316 0.414 3.3 8 279.9 245.9 336 5 10 2 39.747 79.495 0.415 3.29 8 26.3 2.2 337 7 11 0 39.803 79.606 0.416 3.28 4 333.8 173.8 338 9 0 1 39.878 79.757 0.416 3.27 4 246.3 94.4 339 5 14 0 39.913 79.827 0.416 3.27 4 14.7 0.3 340 2 7 3 39.933 79.866 0.417 3.26 8 103.0 32.9 341 9 1 1 39.966 79.932 0.417 3.26 8 434.1 584.3 342 9 5 0 40.008 80.015 0.417 3.25 4 31.9 1.6 343 7 10 1 40.025 80.05 0.417 3.25 8 172.6 92.2 344 4 15 0 40.032 80.063 0.418 3.25 4 196.4 59.7 345 2 13 2 40.14 80.28 0.418 3.24 8 99.4 30.4 346 3 6 3 40.14 80.281 0.418 3.24 8 84.3 21.9 347 0 8 3 40.171 80.341 0.419 3.23 4 529.0 430.5 348 3 15 1 40.209 80.417 0.419 3.23 8 166.6 85.2 349 9 2 1 40.229 80.459 0.419 3.23 8 173.7 92.6 350 4 4 3 40.273 80.545 0.42 3.22 8 173.2 92.0 351 8 9 0 40.338 80.675 0.42 3.21 4 177.8 48.3 352 6 12 1 40.381 80.762 0.421 3.21 8 148.5 67.4 353 1 8 3 40.44 80.88 0.421 3.2 8 45.1 6.2 354 0 16 1 40.502 81.004 0.422 3.19 4 8.9 0.1 355 6 13 0 40.51 81.019 0.422 3.19 4 27.7 1.2 356 7 6 2 40.602 81.204 0.422 3.18 8 119.5 43.2 357 9 3 1 40.667 81.334 0.423 3.17 8 156.2 73.7 358 1 16 1 40.771 81.541 0.424 3.16 8 78.4 18.5 359 3 16 0 40.863 81.725 0.425 3.15 4 122.2 22.4 360 8 8 1 40.909 81.817 0.425 3.15 8 45.2 6.1 361 9 6 0 40.971 81.941 0.426 3.14 4 41.4 2.6 362 6 9 2 41.044 82.088 0.426 3.13 8 178.7 95.2 363 4 5 3 41.06 82.12 0.426 3.13 8 70.0 14.6 364 4 12 2 41.179 82.357 0.427 3.12 8 382.2 433.5 365 2 8 3 41.246 82.491 0.428 3.11 8 10.9 0.4 366 3 7 3 41.277 82.554 0.428 3.11 8 170.4 85.9 367 9 4 1 41.278 82.557 0.428 3.11 8 17.0 0.9 368 5 0 3 41.291 82.583 0.428 3.11 4 255.1 96.2 369 5 1 3 41.379 82.757 0.429 3.1 8 15.8 0.7 370 0 14 2 41.426 82.852 0.429 3.09 4 20.0 0.6 371 8 0 2 41.483 82.966 0.43 3.09 4 148.9 32.6 372 3 13 2 41.483 82.966 0.43 3.09 8 177.5 92.5 373 8 1 2 41.57 83.14 0.431 3.08 8 124.8 45.6 374 2 16 1 41.575 83.15 0.431 3.08 8 49.7 7.2 375 5 11 2 41.584 83.169 0.431 3.08 8 147.7 63.9 376 1 17 0 41.597 83.194 0.431 3.08 4 76.8 8.6 377 5 2 3 41.64 83.28 0.431 3.07 8 149.6 65.4 378 1 14 2 41.694 83.387 0.432 3.07 8 73.1 15.6 379 7 7 2 41.736 83.473 0.432 3.06 8 44.5 5.8 380 7 12 0 41.814 83.627 0.433 3.06 4 99.0 14.3 381 8 2 2 41.831 83.662 0.433 3.05 8 9.6 0.3 382 7 11 1 41.86 83.719 0.433 3.05 8 121.1 42.6 383 1 9 3 41.923 83.846 0.434 3.05 8 55.9 9.1 384 5 14 1 41.969 83.937 0.434 3.04 8 100.8 29.4 385 8 10 0 41.995 83.991 0.434 3.04 4 24.6 0.9 386 4 6 3 42.018 84.036 0.434 3.04 8 339.6 333.3 387 9 5 1 42.062 84.124 0.435 3.03 8 10.1 0.3 388 5 3 3 42.075 84.15 0.435 3.03 8 215.7 134.3 389 4 15 1 42.086 84.171 0.435 3.03 8 230.5 153.2 390 9 7 0 42.103 84.206 0.435 3.03 4 394.5 224.3 391 8 3 2 42.266 84.532 0.437 3.01 8 150.6 65.1 392 8 9 1 42.389 84.778 0.438 3.0 8 125.1 44.7 393 2 17 0 42.398 84.797 0.438 3.0 4 108.6 16.9 394 5 15 0 42.444 84.888 0.438 3.0 4 0.3 0.0 395 2 14 2 42.495 84.99 0.438 2.99 8 106.4 32.3 396 6 13 1 42.559 85.119 0.439 2.99 8 122.9 43.0 397 3 8 3 42.582 85.163 0.439 2.99 8 104.8 31.2 398 5 4 3 42.683 85.365 0.44 2.98 8 2.4 0.0 399 6 10 2 42.697 85.393 0.44 2.98 8 336.7 321.1 400 2 9 3 42.724 85.447 0.44 2.98 8 176.4 88.1 401 4 16 0 42.734 85.469 0.44 2.97 4 308.6 134.8 402 6 14 0 42.86 85.721 0.442 2.96 4 53.4 4.0 403 8 4 2 42.873 85.746 0.442 2.96 8 347.2 339.9 404 3 16 1 42.909 85.819 0.442 2.96 8 22.4 1.4 405 10 0 0 42.917 85.834 0.442 2.96 2 250.3 44.1 406 10 1 0 43.004 86.008 0.443 2.95 4 277.9 108.5 407 9 6 1 43.017 86.033 0.443 2.95 8 82.2 19.0 408 7 8 2 43.039 86.077 0.443 2.95 8 4.8 0.1 409 4 7 3 43.146 86.292 0.444 2.94 8 170.3 81.2 410 10 2 0 43.264 86.528 0.445 2.93 4 219.3 67.1 411 0 10 3 43.305 86.61 0.445 2.93 4 393.9 216.4 412 4 13 2 43.351 86.701 0.446 2.93 8 1.2 0.0 413 9 8 0 43.404 86.808 0.446 2.92 4 166.5 38.6 414 5 5 3 43.463 86.925 0.447 2.92 8 249.8 173.4 415 1 10 3 43.571 87.142 0.447 2.91 8 146.6 59.6 416 5 12 2 43.58 87.161 0.447 2.91 8 12.4 0.4 417 1 17 1 43.639 87.277 0.448 2.91 8 60.7 10.2 418 8 5 2 43.653 87.306 0.448 2.91 8 0.4 0.0 419 10 3 0 43.697 87.393 0.448 2.9 4 31.7 1.4 420 3 17 0 43.73 87.46 0.449 2.9 4 375.0 194.2 421 8 11 0 43.816 87.633 0.449 2.9 4 79.0 8.6 422 3 14 2 43.826 87.652 0.449 2.9 8 69.5 13.3 423 7 12 1 43.854 87.708 0.45 2.89 8 33.9 3.2 424 7 13 0 43.982 87.963 0.451 2.89 4 35.9 1.8 425 8 10 1 44.035 88.07 0.451 2.88 8 162.3 72.2 426 3 9 3 44.054 88.109 0.451 2.88 8 388.5 413.7 427 9 7 1 44.142 88.284 0.452 2.88 8 187.8 96.5 428 1 15 2 44.208 88.416 0.453 2.87 8 291.6 232.3 429 10 4 0 44.302 88.605 0.453 2.87 4 26.4 0.9 430 6 1 3 44.311 88.621 0.453 2.87 8 163.4 72.8 431 0 18 0 44.365 88.731 0.454 2.86 2 262.9 47.1 432 2 10 3 44.369 88.738 0.454 2.86 8 12.1 0.4 433 5 6 3 44.414 88.829 0.454 2.86 8 92.5 23.3 434 2 17 1 44.436 88.872 0.454 2.86 8 0.6 0.0 435 4 8 3 44.444 88.888 0.455 2.86 8 55.1 8.3 436 5 15 1 44.482 88.963 0.455 2.86 8 180.8 88.8 437 7 9 2 44.51 89.02 0.455 2.85 8 11.9 0.4 438 6 11 2 44.515 89.03 0.455 2.85 8 157.6 67.4 439 6 2 3 44.57 89.14 0.456 2.85 8 179.3 87.2 440 8 6 2 44.604 89.209 0.456 2.85 8 183.6 91.3 441 1 18 0 44.631 89.262 0.456 2.85 4 197.4 52.8 442 4 16 1 44.771 89.542 0.457 2.84 8 77.4 16.2 443 9 9 0 44.875 89.749 0.458 2.83 4 145.5 28.6 444 6 14 1 44.897 89.793 0.458 2.83 8 28.2 2.1 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 2 0 4.456 8.912 9.9145 86.2 1.3 1.3 5.6 2 1 1 0 4.496 8.993 9.82559 103.1 1.6 1.6 5.6 3 1 2 0 5.93 11.86 7.45603 145.9 2.2 2.3 5.6 4 1 3 0 7.757 15.514 5.70687 776.1 11.9 12.0 5.6 5 2 1 0 8.142 16.283 5.43906 223.0 3.4 3.4 5.6 6 0 4 0 8.939 17.878 4.95725 235.2 3.6 3.6 5.6 7 2 2 0 9.021 18.041 4.91279 156.5 2.4 2.4 5.6 8 1 4 0 9.767 19.535 4.5404 89.5 1.4 1.4 5.6 9 2 3 0 10.326 20.651 4.29738 1264.2 19.4 19.5 5.6 10 1 0 1 11.558 23.115 3.84465 529.7 8.1 8.2 5.6 11 1 1 1 11.776 23.552 3.77436 1289.1 19.7 19.8 5.6 12 1 5 0 11.878 23.755 3.74247 2284.7 35.0 35.2 5.6 13 2 4 0 11.924 23.849 3.72801 2248.4 34.4 34.6 5.6 14 3 1 0 12.002 24.004 3.70429 4824.3 73.9 74.2 5.6 15 1 2 1 12.409 24.818 3.58457 3795.0 58.1 58.3 5.6 16 3 2 0 12.624 25.249 3.52438 315.1 4.8 4.8 5.6 17 1 3 1 13.402 26.804 3.32333 4705.0 72.0 72.2 5.6 18 0 6 0 13.478 26.957 3.30483 76.9 1.2 1.2 5.6 19 3 3 0 13.603 27.205 3.2752 628.1 9.6 9.6 5.6 20 2 1 1 13.634 27.267 3.26789 297.9 4.6 4.6 5.6 21 2 5 0 13.722 27.445 3.24713 2188.1 33.5 33.6 5.6 22 1 6 0 14.053 28.106 3.17223 3142.2 48.1 48.2 5.6 23 0 4 1 14.136 28.273 3.15391 316.8 4.9 4.9 5.6 24 2 2 1 14.189 28.379 3.14237 1659.0 25.4 25.4 5.6 25 1 4 1 14.687 29.375 3.03804 352.8 5.4 5.4 5.6 26 2 3 1 15.074 30.147 2.96191 6531.3 100.0 100.0 5.6 27 2 6 0 15.661 31.322 2.85344 2642.8 40.5 40.4 5.6 28 4 1 0 15.97 31.94 2.79967 542.8 8.3 8.3 5.6 29 3 0 1 16.136 32.271 2.77167 1598.8 24.5 24.4 5.6 30 1 5 1 16.203 32.406 2.76041 105.7 1.6 1.6 5.6 31 2 4 1 16.238 32.477 2.7546 4941.6 75.7 75.5 5.6 32 3 1 1 16.297 32.594 2.74498 2795.0 42.8 42.7 5.6 33 4 2 0 16.454 32.907 2.71953 251.1 3.8 3.8 5.6 34 3 2 1 16.772 33.544 2.66932 428.7 6.6 6.5 5.7 35 4 3 0 17.233 34.466 2.60001 246.6 3.8 3.8 5.7 36 0 6 1 17.44 34.881 2.57005 326.9 5.0 5.0 5.7 37 3 3 1 17.539 35.078 2.55604 250.7 3.8 3.8 5.7 38 2 5 1 17.635 35.269 2.54263 84.5 1.3 1.3 5.7 39 2 7 0 17.705 35.411 2.53281 1103.2 16.9 16.8 5.7 40 1 6 1 17.9 35.799 2.50618 333.1 5.1 5.1 5.7 41 0 8 0 18.106 36.211 2.47863 174.9 2.7 2.7 5.7 42 3 4 1 18.566 37.133 2.41921 244.5 3.7 3.7 5.7 43 2 6 1 19.221 38.441 2.33982 521.1 8.0 7.9 5.7 44 4 1 1 19.479 38.959 2.3099 233.1 3.6 3.5 5.7 45 4 5 0 19.544 39.089 2.30253 276.7 4.2 4.2 5.7 46 1 7 1 19.741 39.481 2.28054 1412.4 21.6 21.4 5.7 47 3 5 1 19.82 39.639 2.27182 226.5 3.5 3.4 5.7 48 4 2 1 19.888 39.777 2.26427 2541.6 38.9 38.6 5.7 49 4 3 1 20.555 41.11 2.19388 1676.4 25.7 25.4 5.7 50 2 7 1 20.963 41.926 2.15306 211.3 3.2 3.2 5.7 51 4 6 0 21.007 42.015 2.14869 308.1 4.7 4.7 5.7 52 5 3 0 21.092 42.184 2.14048 432.0 6.6 6.5 5.7 53 3 6 1 21.267 42.534 2.12367 141.4 2.2 2.1 5.7 54 0 8 1 21.311 42.622 2.11947 2697.0 41.3 40.8 5.7 55 4 4 1 21.459 42.918 2.10553 558.4 8.6 8.4 5.7 56 3 8 0 21.833 43.666 2.07121 113.8 1.7 1.7 5.7 57 5 4 0 21.978 43.956 2.05819 394.4 6.0 6.0 5.7 58 2 9 0 22.037 44.074 2.05296 302.7 4.6 4.6 5.7 59 0 0 2 22.139 44.277 2.044 3202.7 49.0 48.4 5.7 60 4 5 1 22.579 45.157 2.00619 77.7 1.2 1.2 5.7 61 1 1 2 22.639 45.277 2.00116 292.9 4.5 4.4 5.7 62 0 10 0 22.859 45.718 1.9829 370.6 5.7 5.6 5.7 63 5 0 1 22.901 45.801 1.97948 992.1 15.2 15.0 5.7 64 5 5 0 23.078 46.155 1.96512 2150.5 32.9 32.4 5.7 65 1 10 0 23.228 46.455 1.95312 135.8 2.1 2.0 5.7 66 5 2 1 23.379 46.758 1.94117 339.0 5.2 5.1 5.7 67 1 3 2 23.596 47.193 1.9243 88.8 1.4 1.3 5.7 68 1 9 1 23.763 47.526 1.91159 80.9 1.2 1.2 5.7 69 4 6 1 23.891 47.781 1.90197 2311.7 35.4 34.8 5.7 70 5 3 1 23.967 47.934 1.89627 658.1 10.1 9.9 5.7 71 6 0 0 24.115 48.229 1.88533 681.8 10.4 10.3 5.7 72 6 1 0 24.23 48.461 1.87687 130.4 2.0 2.0 5.7 73 5 6 0 24.369 48.737 1.86686 385.3 5.9 5.8 5.7 74 4 8 0 24.408 48.817 1.86401 82.3 1.3 1.2 5.7 75 2 3 2 24.665 49.329 1.84584 420.7 6.4 6.3 5.7 76 2 9 1 24.826 49.651 1.83461 406.9 6.2 6.1 5.7 77 6 3 0 25.142 50.284 1.81302 109.1 1.7 1.6 5.8 78 4 7 1 25.374 50.748 1.79751 359.0 5.5 5.4 5.8 79 2 4 2 25.453 50.907 1.79228 1247.5 19.1 18.7 5.8 80 3 1 2 25.494 50.988 1.78963 1340.5 20.5 20.1 5.8 81 0 10 1 25.579 51.157 1.7841 953.7 14.6 14.3 5.8 82 1 11 0 25.639 51.278 1.78018 469.5 7.2 7.0 5.8 83 5 5 1 25.78 51.56 1.77111 751.4 11.5 11.3 5.8 84 3 2 2 25.826 51.652 1.76815 113.9 1.7 1.7 5.8 85 1 10 1 25.918 51.836 1.76231 251.1 3.8 3.8 5.8 86 3 10 0 26.034 52.067 1.75502 414.6 6.3 6.2 5.8 87 3 3 2 26.373 52.746 1.73402 214.5 3.3 3.2 5.8 88 2 5 2 26.442 52.885 1.72982 680.2 10.4 10.2 5.8 89 3 9 1 26.527 53.054 1.7247 1675.7 25.7 25.1 5.8 90 1 6 2 26.635 53.27 1.71821 1282.2 19.6 19.2 5.8 91 6 1 1 26.846 53.692 1.70569 294.2 4.5 4.4 5.8 92 5 6 1 26.975 53.949 1.69817 89.8 1.4 1.3 5.8 93 6 2 1 27.167 54.333 1.68707 332.4 5.1 5.0 5.8 94 5 8 0 27.45 54.9 1.67098 65.8 1.0 1.0 5.8 95 2 6 2 27.617 55.234 1.66166 1023.6 15.7 15.3 5.8 96 4 1 2 27.814 55.627 1.65084 336.1 5.1 5.0 5.8 97 6 6 0 28.058 56.117 1.6376 105.0 1.6 1.6 5.8 98 4 2 2 28.127 56.254 1.63394 177.9 2.7 2.6 5.8 99 4 10 0 28.323 56.645 1.62356 70.7 1.1 1.1 5.8 100 7 1 0 28.57 57.141 1.61066 194.8 3.0 2.9 5.8 101 4 3 2 28.644 57.287 1.60689 109.1 1.7 1.6 5.8 102 4 9 1 28.789 57.578 1.59947 79.7 1.2 1.2 5.8 103 7 2 0 28.878 57.756 1.59495 361.0 5.5 5.4 5.8 104 2 7 2 28.964 57.928 1.59064 524.6 8.0 7.8 5.8 105 2 12 0 29.054 58.109 1.58611 270.0 4.1 4.0 5.8 106 2 11 1 29.108 58.216 1.58344 228.8 3.5 3.4 5.8 107 0 8 2 29.239 58.479 1.57696 84.9 1.3 1.3 5.8 108 7 3 0 29.386 58.773 1.56976 204.6 3.1 3.0 5.8 109 4 5 2 30.259 60.519 1.52859 152.5 2.3 2.3 5.8 110 4 11 0 30.447 60.893 1.52008 377.2 5.8 5.6 5.8 111 1 12 1 30.49 60.98 1.51814 549.9 8.4 8.1 5.8 112 3 11 1 30.646 61.292 1.51115 131.7 2.0 1.9 5.8 113 7 1 1 30.932 61.864 1.49854 112.6 1.7 1.7 5.8 114 7 5 0 30.978 61.956 1.49653 67.9 1.0 1.0 5.8 115 7 2 1 31.225 62.451 1.48587 480.8 7.4 7.1 5.8 116 4 6 2 31.341 62.681 1.48095 189.4 2.9 2.8 5.8 117 2 12 1 31.394 62.787 1.47871 702.8 10.8 10.4 5.9 118 7 3 1 31.711 63.422 1.46544 621.6 9.5 9.2 5.9 119 3 8 2 31.969 63.937 1.45485 72.0 1.1 1.1 5.9 120 5 4 2 32.081 64.161 1.45032 251.6 3.9 3.7 5.9 121 2 9 2 32.126 64.252 1.44849 198.2 3.0 2.9 5.9 122 7 4 1 32.384 64.767 1.4382 94.4 1.4 1.4 5.9 123 6 9 0 32.529 65.059 1.43246 91.5 1.4 1.3 5.9 124 4 7 2 32.592 65.184 1.43001 189.3 2.9 2.8 5.9 125 4 12 0 32.677 65.353 1.42672 405.2 6.2 5.9 5.9 126 0 10 2 32.767 65.533 1.42323 256.1 3.9 3.8 5.9 127 1 13 1 32.908 65.816 1.4178 267.2 4.1 3.9 5.9 128 5 5 2 32.939 65.878 1.41661 1483.8 22.7 21.8 5.9 129 3 13 0 33.008 66.016 1.414 115.5 1.8 1.7 5.9 130 1 10 2 33.058 66.116 1.4121 93.7 1.4 1.4 5.9 131 5 11 0 33.118 66.236 1.40983 100.5 1.5 1.5 5.9 132 6 8 1 33.149 66.297 1.40867 860.9 13.2 12.6 5.9 133 7 5 1 33.238 66.476 1.40532 91.6 1.4 1.3 5.9 134 5 10 1 33.356 66.712 1.40091 69.9 1.1 1.0 5.9 135 3 9 2 33.584 67.167 1.39253 470.5 7.2 6.9 5.9 136 6 0 2 33.767 67.535 1.38583 497.6 7.6 7.3 5.9 137 6 1 2 33.861 67.722 1.38246 154.2 2.4 2.3 5.9 138 5 6 2 33.973 67.946 1.37845 287.7 4.4 4.2 5.9 139 6 10 0 34.316 68.633 1.36632 281.9 4.3 4.1 5.9 140 8 4 0 34.505 69.01 1.35977 298.9 4.6 4.4 5.9 141 6 3 2 34.605 69.209 1.35634 83.2 1.3 1.2 5.9 142 4 12 1 34.878 69.756 1.34704 91.9 1.4 1.3 5.9 143 1 11 2 35.015 70.031 1.34242 371.6 5.7 5.4 5.9 144 1 2 3 35.074 70.148 1.34046 222.5 3.4 3.2 5.9 145 3 10 2 35.344 70.689 1.33154 329.3 5.0 4.8 5.9 146 1 14 1 35.421 70.842 1.32904 266.4 4.1 3.9 5.9 147 7 7 1 35.466 70.931 1.32758 735.6 11.3 10.7 5.9 148 1 3 3 35.533 71.065 1.32541 343.9 5.3 5.0 5.9 149 2 11 2 35.859 71.718 1.31493 138.8 2.1 2.0 5.9 150 1 15 0 35.92 71.84 1.313 333.9 5.1 4.8 5.9 151 2 14 1 36.26 72.521 1.30235 341.5 5.2 5.0 5.9 152 8 6 0 36.336 72.672 1.30001 74.8 1.1 1.1 6.0 153 2 3 3 36.371 72.742 1.29893 513.4 7.9 7.4 6.0 154 8 4 1 36.655 73.31 1.29026 233.7 3.6 3.4 6.0 155 2 15 0 36.755 73.51 1.28724 180.5 2.8 2.6 6.0 156 7 8 1 36.827 73.654 1.28508 395.8 6.1 5.7 6.0 157 3 0 3 36.945 73.891 1.28155 136.9 2.1 2.0 6.0 158 2 4 3 37.003 74.005 1.27985 462.7 7.1 6.7 6.0 159 3 1 3 37.035 74.071 1.27888 352.4 5.4 5.1 6.0 160 4 10 2 37.293 74.586 1.27131 101.6 1.6 1.5 6.0 161 5 12 1 37.389 74.778 1.26852 248.5 3.8 3.6 6.0 162 8 5 1 37.464 74.928 1.26636 274.0 4.2 4.0 6.0 163 7 1 2 37.508 75.016 1.26509 175.8 2.7 2.5 6.0 164 7 2 2 37.776 75.553 1.25743 355.0 5.4 5.1 6.0 165 2 12 2 37.93 75.861 1.25309 378.8 5.8 5.5 6.0 166 9 2 0 38.152 76.304 1.24691 84.3 1.3 1.2 6.0 167 7 3 2 38.222 76.444 1.24498 189.9 2.9 2.7 6.0 168 7 9 1 38.348 76.696 1.24152 141.1 2.2 2.0 6.0 169 1 16 0 38.701 77.402 1.23194 109.7 1.7 1.6 6.0 170 2 6 3 38.787 77.574 1.22965 68.1 1.0 1.0 6.0 171 2 15 1 38.856 77.711 1.22781 525.3 8.0 7.5 6.0 172 1 7 3 39.121 78.242 1.2208 194.3 3.0 2.8 6.0 173 4 11 2 39.161 78.322 1.21976 358.2 5.5 5.1 6.0 174 4 2 3 39.217 78.435 1.21829 320.6 4.9 4.6 6.0 175 5 13 1 39.608 79.216 1.20822 1148.7 17.6 16.4 6.0 176 4 3 3 39.658 79.316 1.20695 314.8 4.8 4.5 6.0 177 7 11 0 39.803 79.606 1.20328 173.8 2.7 2.5 6.0 178 9 0 1 39.878 79.757 1.20139 94.4 1.4 1.3 6.0 179 9 1 1 39.966 79.932 1.19919 584.3 8.9 8.3 6.0 180 4 15 0 40.032 80.063 1.19756 153.4 2.3 2.2 6.0 181 0 8 3 40.171 80.341 1.19411 430.5 6.6 6.1 6.0 182 9 2 1 40.229 80.459 1.19266 177.9 2.7 2.5 6.0 183 4 4 3 40.273 80.545 1.1916 92.0 1.4 1.3 6.1 184 6 12 1 40.381 80.762 1.18895 67.4 1.0 1.0 6.1 185 9 3 1 40.667 81.334 1.18202 73.7 1.1 1.0 6.1 186 6 9 2 41.044 82.088 1.17307 109.8 1.7 1.6 6.1 187 4 12 2 41.179 82.357 1.16991 433.5 6.6 6.2 6.1 188 5 0 3 41.291 82.583 1.16729 182.9 2.8 2.6 6.1 189 3 13 2 41.483 82.966 1.16287 125.1 1.9 1.8 6.1 190 5 11 2 41.584 83.169 1.16055 125.4 1.9 1.8 6.1 191 5 2 3 41.64 83.28 1.15928 65.4 1.0 0.9 6.1 192 4 6 3 42.018 84.036 1.15076 333.3 5.1 4.7 6.1 193 9 7 0 42.103 84.206 1.14887 511.8 7.8 7.2 6.1 194 6 13 1 42.559 85.119 1.13887 74.2 1.1 1.0 6.1 195 6 10 2 42.697 85.393 1.13591 409.2 6.3 5.8 6.1 196 4 16 0 42.734 85.469 1.1351 134.8 2.1 1.9 6.1 197 8 4 2 42.873 85.746 1.13213 343.9 5.3 4.8 6.1 198 10 1 0 43.004 86.008 1.12936 127.5 2.0 1.8 6.1 199 4 7 3 43.146 86.292 1.12637 81.2 1.2 1.1 6.1 200 10 2 0 43.264 86.528 1.12391 67.1 1.0 0.9 6.1 201 0 10 3 43.305 86.61 1.12305 216.4 3.3 3.0 6.1 202 5 5 3 43.463 86.925 1.11979 173.4 2.7 2.4 6.1 203 3 17 0 43.73 87.46 1.11432 194.2 3.0 2.7 6.2 204 3 9 3 44.054 88.109 1.10778 486.0 7.4 6.8 6.2 205 9 7 1 44.142 88.284 1.10603 96.5 1.5 1.3 6.2 206 1 15 2 44.208 88.416 1.10471 232.3 3.6 3.2 6.2 207 6 1 3 44.311 88.621 1.10269 72.8 1.1 1.0 6.2 208 5 15 1 44.482 88.963 1.09933 89.2 1.4 1.2 6.2 209 6 11 2 44.515 89.03 1.09868 67.4 1.0 0.9 6.2 210 6 2 3 44.57 89.14 1.09761 87.2 1.3 1.2 6.2 211 8 6 2 44.604 89.209 1.09694 144.1 2.2 2.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |