Institute of Experimental Mineralogy
Russian Academy of Sciences
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142432, Chernogolovka, Moscow district
A.V. Chichagov +7(496)52-22320
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*** W W W - X R A Y P O L ***
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FLUORAPOPHYLLITE-(NH4)
1, t-apophyllite, f-apophyllite, s-apophyllite
NH(4)Ca(4)[Si(8)O(20)]F.8H(2)O
Tetragonal P 4/mnc Z = 2
R =0.0299 NR =743
2 .11 .20
Ref.Str.:
Stevko M., Sejkora J., Plasil J., Dolnicek Z., Skoda R. (2020)
* Mineral. Mag., 84, 533-539, DOI:10.1180/mgm.2020.44
L: $N0.656 K0.344 Ca3.956 Mg0.044 Si8 F1 O28 H18.65$
R: Locality - Vechec quarry, Vechec, Vranov nad Toplou District,
Presov Region, Slovakia. IMA2019-083.
N.A.D.
Initial data from BDM-file
Lattice parameters (cub. angs.,degr.):
a = 8.9934 alpha = 90.0
b = 8.9934 beta = 90.0
c = 15.791 gamma = 90.0
Unit cell volume (cub. angs.) = 1277.18
Molar volume ( cub.cm/mol.) = 384.65
Co-ordinates, thermal parameters, occupation for atomic positions:
NoP x/a y/b z/c B(j) atom / occupation
1 0.0 0.0 0.0 0.0 F = 1.00
2 0.0 0.0 0.5 0.0 NH(4) = 0.66, K = 0.34
3 0.1085 0.2461 0.0 0.0 Ca = 0.99, Mg = 0.01
4 0.2251 0.0873 0.19 0.0 Si = 1.00
5 0.3623 0.1377 0.25 0.0 O = 1.00
6 0.0834 0.1901 0.2177 0.0 O = 1.00
7 0.2628 0.1029 0.0924 0.0 O = 1.00
8 0.21 0.4491 0.09 0.0 O = 1.00
9 0.193 0.5499 0.0913 0.0 H = 1.00
10 0.214 0.421 0.1474 0.0 H = 1.00
Co-ordinates for all atomic positions :
No NoP x/a y/b z/c
1 1 0.0 0.0 0.0
2 2 0.0 0.0 0.5
3 3 0.1085 0.2461 0.0
4 4 0.2251 0.0873 0.19
5 5 0.3623 0.1377 0.25
6 6 0.0834 0.1901 0.2177
7 7 0.2628 0.1029 0.0924
8 8 0.21 0.4491 0.09
9 9 0.193 0.5499 0.0913
10 10 0.214 0.421 0.1474
11 3 0.7539 0.1085 0.0
12 3 0.8915 0.7539 0.0
13 3 0.2461 0.8915 0.0
14 4 0.9127 0.2251 0.19
15 4 0.7749 0.9127 0.19
16 4 0.0873 0.7749 0.19
17 5 0.8623 0.3623 0.25
18 5 0.6377 0.8623 0.25
19 5 0.1377 0.6377 0.25
20 6 0.8098 0.0834 0.2177
21 6 0.9166 0.8098 0.2177
22 6 0.1901 0.9166 0.2177
23 7 0.8971 0.2628 0.0924
24 7 0.7372 0.8971 0.0924
25 7 0.1029 0.7372 0.0924
26 8 0.5509 0.21 0.09
27 8 0.79 0.5509 0.09
28 8 0.4491 0.79 0.09
29 9 0.4501 0.193 0.0913
30 9 0.807 0.4501 0.0913
31 9 0.5499 0.807 0.0913
32 10 0.579 0.214 0.1474
33 10 0.786 0.579 0.1474
34 10 0.421 0.786 0.1474
35 1 0.5 0.5 0.5
36 2 0.5 0.5 0.0
37 3 0.3915 0.7461 0.5
38 4 0.2749 0.5873 0.69
39 5 0.1377 0.6377 0.75
40 6 0.4166 0.6902 0.7177
41 7 0.2372 0.6029 0.5924
42 8 0.29 0.9491 0.59
43 9 0.307 0.0499 0.5913
44 10 0.286 0.921 0.6474
45 3 0.7461 0.6085 0.5
46 3 0.6085 0.2539 0.5
47 3 0.2539 0.3915 0.5
48 4 0.5873 0.7251 0.69
49 4 0.7251 0.4127 0.69
50 4 0.4127 0.2749 0.69
51 5 0.6377 0.8623 0.75
52 5 0.8623 0.3623 0.75
53 5 0.3623 0.1377 0.75
54 6 0.6902 0.5834 0.7177
55 6 0.5834 0.3098 0.7177
56 6 0.3099 0.4166 0.7177
57 7 0.6029 0.7628 0.5924
58 7 0.7628 0.3971 0.5924
59 7 0.3971 0.2372 0.5924
60 8 0.9491 0.71 0.59
61 8 0.71 0.0509 0.59
62 8 0.0509 0.29 0.59
63 9 0.0499 0.693 0.5913
64 9 0.693 0.9501 0.5913
65 9 0.9501 0.307 0.5913
66 10 0.921 0.714 0.6474
67 10 0.714 0.079 0.6474
68 10 0.079 0.286 0.6474
69 4 0.2251 0.0873 0.81
70 6 0.0834 0.1901 0.7823
71 7 0.2628 0.1029 0.9076
72 8 0.21 0.4491 0.91
73 9 0.193 0.5499 0.9087
74 10 0.214 0.421 0.8526
75 4 0.9127 0.2251 0.81
76 4 0.7749 0.9127 0.81
77 4 0.0873 0.7749 0.81
78 6 0.8098 0.0834 0.7823
79 6 0.9166 0.8098 0.7823
80 6 0.1901 0.9166 0.7823
81 7 0.8971 0.2628 0.9076
82 7 0.7372 0.8971 0.9076
83 7 0.1029 0.7372 0.9076
84 8 0.5509 0.21 0.91
85 8 0.79 0.5509 0.91
86 8 0.4491 0.79 0.91
87 9 0.4501 0.193 0.9087
88 9 0.807 0.4501 0.9087
89 9 0.5499 0.807 0.9087
90 10 0.579 0.214 0.8526
91 10 0.786 0.579 0.8526
92 10 0.421 0.786 0.8526
93 4 0.2749 0.5873 0.31
94 6 0.4166 0.6902 0.2823
95 7 0.2372 0.6029 0.4076
96 8 0.29 0.9491 0.41
97 9 0.307 0.0499 0.4087
98 10 0.286 0.921 0.3526
99 4 0.5873 0.7251 0.31
100 4 0.7251 0.4127 0.31
101 4 0.4127 0.2749 0.31
102 6 0.6902 0.5834 0.2823
103 6 0.5834 0.3098 0.2823
104 6 0.3099 0.4166 0.2823
105 7 0.6029 0.7628 0.4076
106 7 0.7628 0.3971 0.4076
107 7 0.3971 0.2372 0.4076
108 8 0.9491 0.71 0.41
109 8 0.71 0.0509 0.41
110 8 0.0509 0.29 0.41
111 9 0.0499 0.693 0.4087
112 9 0.693 0.9501 0.4087
113 9 0.9501 0.307 0.4087
114 10 0.921 0.714 0.3526
115 10 0.714 0.079 0.3526
116 10 0.079 0.286 0.3526
X-ray density (g/cm cub.) = 2.32
MU (1/cm) = 121.52 Mass attenuation coefficient (cm**2/g) = 52.395
Selected interatomic distances (cation-anion,anion-anion):
NoP Atom Rad.sph. C.N. Distance NoP N.
(angs.) (angs.)
1 F 3.228 8
2.9273 7
2.9273 7
2.9273 7
2.9273 7
2.9273 7
2.9273 7
2.9273 7
2.9273 7
2 NH(4),K 3.228 8
3.0055 8
3.0055 8
3.0055 8
3.0055 8
3.0055 8
3.0055 8
3.0055 8
3.0055 8
3 Ca ,Mg 2.88 7
2.4184 1
2.3897 7
2.4878 8
2.4008 7
2.3897 7
2.4878 8
2.4008 7
4 Si 2.1 4
1.6207 5
1.6341 6
1.5848 7
1.6266 6
5 O 3.264 8
2.6031 6
2.6637 7
2.5709 6
3.1113 8
3.1112 8
2.571 6
2.6032 6
2.6637 7
6 O 3.264 8
2.6031 5
2.6714 7
2.5709 5
2.6406 6
2.6406 6
2.6735 7
3.0562 6
3.1799 8
7 O 3.264 7
2.9273 1
2.6637 5
2.6714 6
3.15 8
2.6735 6
2.7645 8
2.9169 7
8 O 3.264 5
3.15 7
3.1113 5
2.7645 7
2.8436 8
3.1799 6
9 H 1.632 1
0.9195 8
10 H 1.632 1
0.9411 8
X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.):
No H K L Theta 2*Theta S LPG MF F I int.
( degree ) *100
1 0 0 2 5.599 11.197 0.063 207.16 2 37.8 36.3
2 1 0 1 5.657 11.313 0.064 202.89 8 105.6 1110.6
3 1 1 0 6.957 13.914 0.079 133.36 4 37.5 46.0
4 1 1 2 8.948 17.895 0.101 79.75 8 5.2 1.1
5 1 0 3 9.762 19.525 0.11 66.64 8 73.9 178.5
6 2 0 0 9.863 19.727 0.111 65.24 4 135.5 293.9
7 2 1 0 11.041 22.083 0.124 51.63 8 36.0 32.9
8 0 0 4 11.252 22.503 0.127 49.64 2 146.6 130.8
9 2 0 2 11.369 22.739 0.128 48.57 8 19.2 8.8
10 2 1 1 11.399 22.797 0.128 48.31 16 65.1 201.0
11 2 1 2 12.412 24.824 0.14 40.42 16 117.0 542.9
12 1 1 4 13.277 26.554 0.149 35.07 8 62.8 67.8
13 2 1 3 13.947 27.894 0.156 31.59 16 15.0 7.0
14 2 2 0 14.02 28.039 0.157 31.24 4 216.7 359.6
15 1 0 5 14.981 29.962 0.168 27.12 8 182.5 443.1
16 2 0 4 15.049 30.098 0.169 26.86 8 7.8 0.8
17 2 2 2 15.139 30.278 0.17 26.52 8 50.2 32.7
18 3 0 1 15.161 30.323 0.17 26.43 8 126.9 208.8
19 3 1 0 15.715 31.43 0.176 24.47 8 23.9 6.9
20 2 1 4 15.867 31.734 0.177 23.97 16 43.3 44.1
21 3 1 1 15.974 31.949 0.179 23.62 16 44.1 45.1
22 3 1 2 16.731 33.463 0.187 21.37 16 72.5 110.1
23 0 0 6 17.018 34.037 0.19 20.59 2 7.3 0.1
24 3 0 3 17.199 34.399 0.192 20.12 8 41.4 16.9
25 3 1 3 17.93 35.86 0.2 18.37 16 185.7 621.6
26 3 2 0 17.988 35.976 0.2 18.24 8 11.5 1.2
27 2 1 5 18.066 36.131 0.201 18.07 16 133.6 316.2
28 2 2 4 18.123 36.246 0.202 17.95 8 44.0 17.1
29 3 2 1 18.219 36.437 0.203 17.74 16 27.7 13.4
30 1 1 6 18.467 36.933 0.206 17.22 8 80.8 55.1
31 3 2 2 18.896 37.793 0.21 16.37 16 43.0 29.6
32 3 1 4 19.5 39.001 0.217 15.27 16 1.2 0.0
33 2 0 6 19.823 39.647 0.22 14.72 8 0.4 0.0
34 3 2 3 19.983 39.965 0.222 14.46 16 41.4 24.3
35 4 0 0 20.035 40.071 0.222 14.38 4 32.5 3.7
36 2 1 6 20.473 40.947 0.227 13.7 16 60.4 49.1
37 1 0 7 20.612 41.224 0.229 13.5 8 44.3 13.0
38 4 1 0 20.68 41.359 0.229 13.4 8 19.4 2.5
39 3 0 5 20.749 41.498 0.23 13.3 8 40.8 10.8
40 4 0 2 20.868 41.736 0.231 13.13 8 91.1 53.5
41 4 1 1 20.885 41.77 0.231 13.11 16 66.5 56.8
42 3 3 0 21.308 42.616 0.236 12.53 4 35.0 3.8
43 3 1 5 21.376 42.751 0.237 12.44 16 115.5 162.7
44 3 2 4 21.426 42.851 0.237 12.38 16 119.7 174.0
45 4 1 2 21.492 42.984 0.238 12.29 16 31.8 12.2
46 3 3 2 22.102 44.203 0.244 11.54 8 66.8 25.3
47 2 2 6 22.329 44.659 0.247 11.28 8 47.3 12.4
48 4 1 3 22.474 44.948 0.248 11.12 16 0.1 0.0
49 4 2 0 22.522 45.044 0.249 11.06 8 226.2 277.6
50 4 2 1 22.714 45.428 0.251 10.85 16 39.8 16.8
51 0 0 8 22.969 45.939 0.253 10.58 2 3.4 0.0
52 2 1 7 23.048 46.096 0.254 10.5 16 6.9 0.5
53 3 2 5 23.173 46.347 0.255 10.37 16 15.7 2.5
54 4 0 4 23.22 46.44 0.256 10.32 8 41.4 8.7
55 4 2 2 23.283 46.565 0.257 10.26 16 34.1 11.7
56 3 1 6 23.501 47.003 0.259 10.05 16 34.7 11.9
57 4 1 4 23.795 47.59 0.262 9.77 16 54.2 28.1
58 1 1 8 24.117 48.234 0.265 9.47 8 5.8 0.2
59 4 2 3 24.207 48.415 0.266 9.39 16 15.5 2.2
60 3 3 4 24.359 48.718 0.268 9.26 8 15.2 1.0
61 3 2 6 25.181 50.361 0.276 8.59 16 4.5 0.2
62 2 0 8 25.225 50.451 0.277 8.55 8 15.0 0.9
63 3 0 7 25.299 50.597 0.277 8.5 8 55.1 12.6
64 4 3 0 25.357 50.713 0.278 8.45 8 0.6 0.0
65 4 1 5 25.416 50.831 0.279 8.41 16 58.4 28.1
66 4 2 4 25.459 50.919 0.279 8.38 16 66.7 36.6
67 4 3 1 25.532 51.064 0.28 8.32 16 44.4 16.1
68 5 0 1 25.532 51.064 0.28 8.32 8 55.2 12.4
69 2 1 8 25.766 51.533 0.282 8.15 16 68.9 38.0
70 3 1 7 25.838 51.677 0.283 8.1 16 135.4 145.6
71 5 1 0 25.895 51.791 0.283 8.06 8 41.1 6.7
72 4 3 2 26.054 52.108 0.285 7.95 16 54.8 23.4
73 5 1 1 26.069 52.137 0.285 7.94 16 45.1 15.9
74 1 0 9 26.57 53.14 0.29 7.6 8 64.1 15.3
75 5 1 2 26.583 53.166 0.29 7.59 16 37.5 10.5
76 4 0 6 26.782 53.564 0.292 7.46 8 42.9 6.7
77 4 3 3 26.908 53.816 0.294 7.38 16 37.2 10.0
78 5 0 3 26.908 53.816 0.294 7.38 8 32.0 3.7
79 4 2 5 27.007 54.014 0.295 7.32 16 43.6 13.7
80 4 1 6 27.301 54.602 0.298 7.14 16 57.0 22.7
81 2 2 8 27.343 54.686 0.298 7.12 8 72.7 18.4
82 3 2 7 27.412 54.825 0.299 7.08 16 31.0 6.7
83 5 1 3 27.426 54.851 0.299 7.07 16 53.1 19.6
84 5 2 0 27.467 54.934 0.299 7.05 8 16.4 0.9
85 5 2 1 27.633 55.267 0.301 6.95 16 129.1 113.6
86 3 3 6 27.813 55.626 0.303 6.85 8 30.3 3.1
87 4 3 4 28.074 56.147 0.305 6.71 16 17.1 1.9
88 5 2 2 28.128 56.256 0.306 6.68 16 57.1 21.4
89 3 1 8 28.361 56.721 0.308 6.55 16 61.2 24.1
90 5 1 4 28.577 57.153 0.31 6.44 16 72.3 33.0
91 2 1 9 28.618 57.237 0.311 6.42 16 40.0 10.1
92 4 2 6 28.82 57.64 0.313 6.32 16 67.4 28.2
93 5 2 3 28.94 57.88 0.314 6.26 16 55.5 18.9
94 4 4 0 28.98 57.961 0.315 6.24 4 142.5 31.1
95 0 0 10 29.196 58.392 0.317 6.14 2 324.5 79.2
96 4 1 7 29.421 58.842 0.319 6.03 16 9.9 0.6
97 4 3 5 29.527 59.054 0.32 5.98 16 37.2 8.1
98 5 0 5 29.527 59.054 0.32 5.98 8 41.6 5.1
99 4 4 2 29.619 59.238 0.321 5.94 8 58.8 10.1
100 3 2 8 29.844 59.689 0.323 5.84 16 134.5 103.6
101 5 3 0 29.962 59.923 0.324 5.79 8 36.8 3.9
102 5 1 5 30.015 60.029 0.325 5.77 16 21.5 2.6
103 5 2 4 30.054 60.107 0.325 5.75 16 62.9 22.3
104 5 3 1 30.119 60.238 0.326 5.72 16 43.4 10.6
105 1 1 10 30.173 60.346 0.326 5.7 8 42.6 5.1
106 3 0 9 30.576 61.152 0.33 5.53 8 60.2 9.8
107 5 3 2 30.588 61.176 0.33 5.53 16 16.5 1.5
108 4 2 7 30.873 61.746 0.333 5.42 16 36.2 7.0
109 6 0 0 30.924 61.848 0.334 5.4 4 212.7 59.9
110 3 1 9 31.054 62.108 0.335 5.35 16 93.5 45.8
111 2 0 10 31.131 62.263 0.336 5.32 8 59.2 9.1
112 4 3 6 31.246 62.491 0.337 5.27 16 7.2 0.3
113 4 0 8 31.284 62.569 0.337 5.26 8 22.6 1.3
114 5 3 3 31.36 62.721 0.338 5.23 16 99.9 51.3
115 6 1 0 31.399 62.797 0.338 5.22 8 51.1 6.7
116 5 2 5 31.45 62.9 0.339 5.2 16 96.4 47.4
117 4 4 4 31.488 62.976 0.339 5.19 8 12.6 0.4
118 6 0 2 31.539 63.078 0.34 5.17 8 2.3 0.0
119 6 1 1 31.552 63.103 0.34 5.16 16 68.9 24.0
120 2 1 10 31.604 63.208 0.34 5.14 16 19.1 1.8
121 5 1 6 31.718 63.435 0.341 5.1 16 62.4 19.5
122 4 1 8 31.756 63.512 0.342 5.09 16 94.0 44.1
123 6 1 2 32.008 64.017 0.344 5.0 16 57.6 16.3
124 3 3 8 32.224 64.448 0.346 4.93 8 6.5 0.1
125 5 3 4 32.424 64.848 0.348 4.87 16 41.9 8.4
126 3 2 9 32.463 64.926 0.348 4.85 16 12.5 0.7
127 6 1 3 32.762 65.524 0.351 4.76 16 2.4 0.0
128 6 2 0 32.799 65.599 0.352 4.75 8 129.7 39.2
129 1 0 11 32.913 65.827 0.353 4.71 8 59.9 8.3
130 6 2 1 32.949 65.898 0.353 4.7 16 11.5 0.6
131 2 2 10 33.0 66.0 0.354 4.68 8 98.2 22.2
132 5 2 6 33.111 66.222 0.355 4.65 16 9.0 0.4
133 4 2 8 33.149 66.297 0.355 4.64 16 10.8 0.5
134 4 3 7 33.21 66.421 0.356 4.62 16 17.7 1.4
135 5 0 7 33.21 66.421 0.356 4.62 8 27.3 1.7
136 5 4 0 33.259 66.518 0.356 4.61 8 63.6 9.1
137 6 0 4 33.346 66.692 0.357 4.58 8 9.3 0.2
138 6 2 2 33.395 66.791 0.357 4.57 16 11.5 0.6
139 5 4 1 33.408 66.815 0.357 4.56 16 84.8 32.2
140 5 1 7 33.667 67.335 0.36 4.49 16 50.8 11.3
141 5 3 5 33.765 67.531 0.361 4.46 16 7.3 0.2
142 6 1 4 33.802 67.604 0.361 4.45 16 53.6 12.5
143 5 4 2 33.851 67.702 0.362 4.44 16 43.7 8.3
144 3 1 10 33.914 67.828 0.362 4.42 16 12.2 0.6
145 6 2 3 34.133 68.266 0.364 4.36 16 36.4 5.7
146 4 1 9 34.293 68.586 0.366 4.32 16 24.3 2.5
147 4 4 6 34.475 68.95 0.367 4.27 8 87.4 16.0
148 5 4 3 34.584 69.168 0.368 4.25 16 27.7 3.2
149 2 1 11 34.731 69.463 0.37 4.21 16 57.2 13.5
150 5 2 7 35.021 70.042 0.373 4.14 16 53.9 11.8
151 6 3 0 35.069 70.137 0.373 4.13 8 37.6 2.9
152 6 1 5 35.117 70.235 0.373 4.12 16 51.0 10.5
153 6 2 4 35.153 70.307 0.374 4.11 16 39.1 6.2
154 6 3 1 35.213 70.427 0.374 4.09 16 44.4 7.9
155 3 2 10 35.263 70.526 0.375 4.08 16 31.0 3.8
156 5 3 6 35.371 70.741 0.376 4.06 16 51.7 10.6
157 4 3 8 35.407 70.814 0.376 4.05 16 14.2 0.8
158 5 4 4 35.599 71.197 0.378 4.01 16 26.1 2.7
159 4 2 9 35.636 71.271 0.378 4.0 16 65.9 17.0
160 6 3 2 35.646 71.293 0.378 4.0 16 5.8 0.1
161 0 0 12 35.828 71.656 0.38 3.96 2 153.1 11.4
162 5 1 8 35.851 71.702 0.38 3.95 16 3.4 0.0
163 6 0 6 36.256 72.513 0.384 3.87 8 68.9 9.0
164 6 3 3 36.363 72.726 0.385 3.84 16 24.5 2.3
165 6 2 5 36.447 72.893 0.386 3.83 16 39.6 5.9
166 3 0 11 36.507 73.015 0.386 3.82 8 69.3 9.0
167 4 0 10 36.59 73.18 0.387 3.8 8 70.9 9.4
168 6 1 6 36.696 73.392 0.388 3.78 16 65.5 15.9
169 1 1 12 36.709 73.419 0.388 3.78 8 20.4 0.8
170 5 4 5 36.885 73.771 0.39 3.74 16 116.2 49.5
171 3 1 11 36.946 73.892 0.39 3.73 16 95.8 33.6
172 7 0 1 36.98 73.959 0.39 3.72 8 50.8 4.7
173 4 1 10 37.028 74.057 0.391 3.71 16 22.3 1.8
174 5 2 8 37.169 74.339 0.392 3.69 16 93.0 31.3
175 5 3 7 37.228 74.456 0.393 3.68 16 84.6 25.8
176 5 5 0 37.275 74.549 0.393 3.67 4 92.1 7.6
177 7 1 0 37.275 74.549 0.393 3.67 8 33.9 2.1
178 6 3 4 37.357 74.715 0.394 3.65 16 43.6 6.8
179 7 1 1 37.416 74.832 0.394 3.64 16 14.9 0.8
180 3 3 10 37.464 74.929 0.395 3.64 8 55.0 5.4
181 2 0 12 37.583 75.165 0.396 3.61 8 23.7 1.0
182 4 3 9 37.828 75.657 0.398 3.57 16 21.3 1.6
183 5 0 9 37.828 75.657 0.398 3.57 8 38.7 2.6
184 5 5 2 37.839 75.678 0.398 3.57 8 113.1 22.4
185 7 1 2 37.839 75.678 0.398 3.57 16 98.5 34.0
186 6 2 6 38.003 76.007 0.4 3.54 16 33.8 4.0
187 2 1 12 38.017 76.033 0.4 3.54 16 13.6 0.6
188 7 0 3 38.108 76.217 0.401 3.53 8 101.6 17.8
189 6 4 0 38.143 76.287 0.401 3.52 8 21.2 0.8
190 3 2 11 38.25 76.5 0.402 3.5 16 26.3 2.4
191 5 1 9 38.261 76.523 0.402 3.5 16 20.0 1.4
192 6 4 1 38.284 76.567 0.402 3.5 16 25.4 2.2
193 4 2 10 38.332 76.663 0.403 3.49 16 132.9 60.5
194 5 4 6 38.436 76.872 0.404 3.47 16 12.3 0.5
195 4 4 8 38.471 76.942 0.404 3.47 8 23.7 1.0
196 6 1 7 38.529 77.058 0.404 3.46 16 8.2 0.2
197 7 1 3 38.54 77.081 0.404 3.46 16 24.2 2.0
198 7 2 0 38.575 77.15 0.405 3.45 8 41.7 2.9
199 6 3 5 38.622 77.244 0.405 3.45 16 54.3 10.0
200 6 4 2 38.703 77.407 0.406 3.43 16 67.5 15.3
201 7 2 1 38.715 77.43 0.406 3.43 16 19.6 1.3
202 7 2 2 39.133 78.267 0.41 3.37 16 60.5 12.1
203 2 2 12 39.309 78.618 0.411 3.35 8 16.6 0.4
204 5 3 8 39.331 78.662 0.411 3.34 16 10.0 0.3
205 6 4 3 39.4 78.8 0.412 3.33 16 14.0 0.6
206 5 5 4 39.516 79.032 0.413 3.32 8 42.4 2.9
207 7 1 4 39.516 79.032 0.413 3.32 16 43.9 6.3
208 5 2 9 39.551 79.103 0.413 3.31 16 61.4 12.3
209 1 0 13 39.784 79.568 0.415 3.28 8 18.9 0.6
210 6 2 7 39.817 79.634 0.416 3.28 16 3.9 0.0
211 7 2 3 39.828 79.656 0.416 3.28 16 23.5 1.8
212 4 1 11 39.968 79.936 0.417 3.26 16 68.5 15.0
213 6 3 6 40.151 80.302 0.419 3.24 16 68.7 15.0
214 3 1 12 40.164 80.329 0.419 3.23 16 60.1 11.5
215 6 0 8 40.186 80.372 0.419 3.23 8 61.9 6.1
216 5 4 7 40.244 80.487 0.419 3.22 16 5.1 0.1
217 7 0 5 40.335 80.671 0.42 3.21 8 124.5 24.4
218 6 4 4 40.37 80.739 0.42 3.21 16 14.0 0.6
219 4 3 10 40.474 80.949 0.421 3.2 16 9.0 0.3
220 6 1 8 40.612 81.224 0.423 3.18 16 56.9 10.1
221 7 3 0 40.714 81.429 0.423 3.17 8 77.3 9.3
222 7 1 5 40.761 81.522 0.424 3.16 16 6.0 0.1
223 7 2 4 40.795 81.59 0.424 3.16 16 33.3 3.4
224 7 3 1 40.852 81.705 0.425 3.15 16 26.2 2.1
225 5 1 10 40.9 81.799 0.425 3.15 16 18.6 1.1
226 4 2 11 41.244 82.488 0.428 3.11 16 30.9 2.9
227 7 3 2 41.265 82.53 0.428 3.11 16 34.1 3.5
228 3 2 12 41.439 82.878 0.43 3.09 16 31.4 3.0
229 2 1 13 41.485 82.97 0.43 3.09 16 12.5 0.5
230 6 4 5 41.609 83.218 0.431 3.08 16 55.2 9.2
231 5 3 9 41.678 83.357 0.432 3.07 16 20.6 1.3
232 6 2 8 41.884 83.768 0.433 3.05 16 12.0 0.4
233 6 3 7 41.941 83.882 0.434 3.04 16 22.2 1.5
234 7 3 3 41.952 83.903 0.434 3.04 16 137.3 56.3
235 6 5 0 41.986 83.972 0.434 3.04 8 11.5 0.2
236 7 2 5 42.032 84.064 0.435 3.04 16 41.4 5.1
237 6 5 1 42.123 84.246 0.435 3.03 16 35.7 3.8
238 5 2 10 42.17 84.34 0.436 3.02 16 19.2 1.1
239 5 5 6 42.272 84.544 0.437 3.01 8 40.6 2.4
240 7 1 6 42.272 84.544 0.437 3.01 16 33.6 3.3
241 5 4 8 42.306 84.613 0.437 3.01 16 55.5 9.1
242 6 5 2 42.534 85.067 0.439 2.99 16 2.8 0.0
243 4 0 12 42.707 85.413 0.44 2.98 8 20.9 0.6
244 7 3 4 42.91 85.82 0.442 2.96 16 52.3 7.9
245 6 1 9 42.945 85.89 0.442 2.96 16 25.7 1.9
246 0 0 14 43.072 86.144 0.443 2.95 2 36.9 0.5
247 6 4 6 43.115 86.23 0.444 2.95 16 26.6 2.0
248 4 1 12 43.128 86.256 0.444 2.94 16 19.0 1.0
249 3 0 13 43.174 86.348 0.444 2.94 8 17.5 0.4
250 6 5 3 43.217 86.434 0.444 2.94 16 54.9 8.7
251 8 0 0 43.251 86.503 0.445 2.94 4 58.7 2.5
252 4 3 11 43.355 86.711 0.446 2.93 16 37.8 4.1
253 5 0 11 43.355 86.711 0.446 2.93 8 54.2 4.2
254 4 4 10 43.435 86.869 0.446 2.92 8 139.9 28.0
255 7 2 6 43.536 87.072 0.447 2.91 16 68.5 13.4
256 3 3 12 43.549 87.098 0.447 2.91 8 14.6 0.3
257 3 1 13 43.595 87.19 0.448 2.91 16 126.5 45.7
258 7 0 7 43.627 87.255 0.448 2.91 8 67.9 6.6
259 7 4 0 43.672 87.344 0.448 2.91 8 20.4 0.6
260 8 1 0 43.672 87.344 0.448 2.91 8 6.9 0.1
261 5 1 11 43.776 87.552 0.449 2.9 16 47.4 6.4
262 8 0 2 43.797 87.595 0.449 2.9 8 87.8 10.9
263 7 4 1 43.809 87.617 0.449 2.9 16 5.3 0.1
264 8 1 1 43.809 87.617 0.449 2.9 16 41.5 4.9
265 1 1 14 43.914 87.827 0.45 2.89 8 32.2 1.5
266 6 3 8 43.991 87.983 0.451 2.88 16 0.1 0.0
267 7 1 7 44.048 88.096 0.451 2.88 16 1.3 0.0
268 7 3 5 44.139 88.277 0.452 2.88 16 24.9 1.7
269 6 5 4 44.173 88.345 0.452 2.87 16 77.2 16.8
270 6 2 9 44.208 88.415 0.453 2.87 16 37.9 4.0
271 7 4 2 44.218 88.436 0.453 2.87 16 55.4 8.6
272 8 1 2 44.218 88.436 0.453 2.87 16 3.2 0.0
273 5 3 10 44.276 88.552 0.453 2.87 16 35.2 3.5
274 4 2 12 44.39 88.781 0.454 2.86 16 65.1 11.9
275 5 4 9 44.628 89.256 0.456 2.85 16 40.4 4.6
276 2 0 14 44.755 89.509 0.457 2.84 8 3.6 0.0
277 3 2 13 44.856 89.713 0.458 2.84 16 18.5 1.0
278 6 4 7 44.889 89.778 0.458 2.83 16 22.9 1.5
279 7 4 3 44.9 89.799 0.458 2.83 16 9.6 0.3
280 8 1 3 44.9 89.799 0.458 2.83 16 25.0 1.7
281 8 2 0 44.934 89.867 0.458 2.83 8 21.2 0.6
X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.):
No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si)
( degree ) (angstrem) *100 *100
1 0 0 2 5.599 11.197 7.8955 36.3 3.3 3.3 5.6
2 1 0 1 5.657 11.313 7.81483 1110.6 100.0 100.0 5.6
3 1 1 0 6.957 13.914 6.35927 46.0 4.1 4.1 5.6
4 1 0 3 9.762 19.525 4.54278 178.5 16.1 16.0 5.6
5 2 0 0 9.863 19.727 4.49668 293.9 26.5 26.3 5.6
6 2 1 0 11.041 22.083 4.02195 32.9 3.0 2.9 5.6
7 0 0 4 11.252 22.503 3.94775 130.8 11.8 11.7 5.6
8 2 1 1 11.399 22.797 3.89752 201.0 18.1 18.0 5.6
9 2 1 2 12.412 24.824 3.58377 542.9 48.9 48.5 5.6
10 1 1 4 13.277 26.554 3.35402 67.8 6.1 6.0 5.6
11 2 2 0 14.02 28.039 3.17963 359.6 32.4 32.0 5.6
12 1 0 5 14.981 29.962 2.9798 443.1 39.9 39.4 5.6
13 3 0 1 15.161 30.323 2.94518 241.6 21.8 21.5 5.6
14 2 1 4 15.867 31.734 2.81735 44.1 4.0 3.9 5.6
15 3 1 1 15.974 31.949 2.79892 45.1 4.1 4.0 5.6
16 3 1 2 16.731 33.463 2.67567 110.1 9.9 9.8 5.7
17 3 0 3 17.199 34.399 2.60494 16.9 1.5 1.5 5.7
18 3 1 3 17.93 35.86 2.50209 621.6 56.0 55.0 5.7
19 2 1 5 18.066 36.131 2.48392 316.2 28.5 28.0 5.7
20 2 2 4 18.123 36.246 2.4763 17.1 1.5 1.5 5.7
21 3 2 1 18.219 36.437 2.46376 13.4 1.2 1.2 5.7
22 1 1 6 18.467 36.933 2.4318 55.1 5.0 4.9 5.7
23 3 2 2 18.896 37.793 2.37844 29.6 2.7 2.6 5.7
24 3 2 3 19.983 39.965 2.25404 24.3 2.2 2.1 5.7
25 2 1 6 20.473 40.947 2.20224 49.1 4.4 4.3 5.7
26 1 0 7 20.612 41.224 2.18807 13.0 1.2 1.1 5.7
27 4 1 1 20.885 41.77 2.16069 110.3 9.9 9.7 5.7
28 3 1 5 21.376 42.751 2.11337 162.7 14.7 14.3 5.7
29 3 2 4 21.426 42.851 2.10867 174.0 15.7 15.3 5.7
30 4 1 2 21.492 42.984 2.10246 12.2 1.1 1.1 5.7
31 3 3 2 22.102 44.203 2.04726 25.3 2.3 2.2 5.7
32 2 2 6 22.329 44.659 2.02742 12.4 1.1 1.1 5.7
33 4 2 0 22.522 45.044 2.01098 277.6 25.0 24.3 5.7
34 4 2 1 22.714 45.428 1.99487 16.8 1.5 1.5 5.7
35 4 2 2 23.283 46.565 1.94876 11.7 1.1 1.0 5.7
36 3 1 6 23.501 47.003 1.93163 11.9 1.1 1.0 5.7
37 4 1 4 23.795 47.59 1.90918 28.1 2.5 2.5 5.7
38 3 0 7 25.299 50.597 1.80251 12.6 1.1 1.1 5.8
39 4 1 5 25.416 50.831 1.79477 28.1 2.5 2.4 5.8
40 4 2 4 25.459 50.919 1.79189 36.6 3.3 3.2 5.8
41 4 3 1 25.532 51.064 1.78712 28.5 2.6 2.5 5.8
42 2 1 8 25.766 51.533 1.77198 38.0 3.4 3.3 5.8
43 3 1 7 25.838 51.677 1.76736 145.6 13.1 12.7 5.8
44 4 3 2 26.054 52.108 1.75374 39.3 3.5 3.4 5.8
45 1 0 9 26.57 53.14 1.72209 25.8 2.3 2.2 5.8
46 4 3 3 26.908 53.816 1.70204 13.7 1.2 1.2 5.8
47 4 2 5 27.007 54.014 1.69629 13.7 1.2 1.2 5.8
48 4 1 6 27.301 54.602 1.67941 22.7 2.0 2.0 5.8
49 2 2 8 27.343 54.686 1.67701 18.4 1.7 1.6 5.8
50 5 1 3 27.426 54.851 1.67236 26.2 2.4 2.3 5.8
51 5 2 1 27.633 55.267 1.66076 113.6 10.2 9.8 5.8
52 5 2 2 28.128 56.256 1.63388 21.4 1.9 1.8 5.8
53 3 1 8 28.361 56.721 1.62157 24.1 2.2 2.1 5.8
54 5 1 4 28.577 57.153 1.61033 33.0 3.0 2.8 5.8
55 4 2 6 28.82 57.64 1.5979 28.2 2.5 2.4 5.8
56 5 2 3 28.94 57.88 1.59183 18.9 1.7 1.6 5.8
57 4 4 0 28.98 57.961 1.58982 31.1 2.8 2.7 5.8
58 0 0 10 29.196 58.392 1.5791 79.2 7.1 6.8 5.8
59 4 3 5 29.527 59.054 1.56297 13.2 1.2 1.1 5.8
60 3 2 8 29.844 59.689 1.54785 103.6 9.3 8.9 5.8
61 5 2 4 30.054 60.107 1.53806 22.3 2.0 1.9 5.8
62 3 0 9 30.576 61.152 1.51426 11.3 1.0 1.0 5.8
63 6 0 0 30.924 61.848 1.49889 59.9 5.4 5.1 5.8
64 3 1 9 31.054 62.108 1.49324 45.8 4.1 3.9 5.8
65 5 3 3 31.36 62.721 1.48012 51.3 4.6 4.4 5.8
66 5 2 5 31.45 62.9 1.47633 47.4 4.3 4.1 5.9
67 6 1 1 31.552 63.103 1.47206 24.0 2.2 2.1 5.9
68 5 1 6 31.718 63.435 1.46516 19.5 1.8 1.7 5.9
69 4 1 8 31.756 63.512 1.46357 44.1 4.0 3.8 5.9
70 6 1 2 32.008 64.017 1.45324 16.3 1.5 1.4 5.9
71 6 2 0 32.799 65.599 1.42198 39.2 3.5 3.3 5.9
72 2 2 10 33.0 66.0 1.41429 22.2 2.0 1.9 5.9
73 5 4 1 33.408 66.815 1.399 32.2 2.9 2.7 5.9
74 5 1 7 33.667 67.335 1.38947 11.3 1.0 1.0 5.9
75 6 1 4 33.802 67.604 1.38458 12.5 1.1 1.1 5.9
76 4 4 6 34.475 68.95 1.36081 16.0 1.4 1.4 5.9
77 2 1 11 34.731 69.463 1.35201 13.5 1.2 1.1 5.9
78 5 2 7 35.021 70.042 1.34224 11.8 1.1 1.0 5.9
79 4 2 9 35.636 71.271 1.32208 17.2 1.5 1.4 5.9
80 0 0 12 35.828 71.656 1.31592 11.4 1.0 1.0 5.9
81 6 1 6 36.696 73.392 1.28902 16.7 1.5 1.4 6.0
82 5 4 5 36.885 73.771 1.28334 49.5 4.5 4.2 6.0
83 3 1 11 36.946 73.892 1.28154 33.6 3.0 2.8 6.0
84 5 2 8 37.169 74.339 1.27493 31.3 2.8 2.6 6.0
85 5 3 7 37.228 74.456 1.27321 25.8 2.3 2.2 6.0
86 7 1 2 37.839 75.678 1.25567 60.6 5.5 5.1 6.0
87 7 0 3 38.108 76.217 1.24812 17.8 1.6 1.5 6.0
88 4 2 10 38.332 76.663 1.24196 60.5 5.4 5.1 6.0
89 6 4 2 38.703 77.407 1.23188 16.6 1.5 1.4 6.0
90 7 2 2 39.133 78.267 1.22048 12.1 1.1 1.0 6.0
91 5 2 9 39.551 79.103 1.20967 12.3 1.1 1.0 6.0
92 4 1 11 39.968 79.936 1.19914 15.0 1.4 1.2 6.0
93 6 3 6 40.151 80.302 1.19459 26.4 2.4 2.2 6.0
94 7 0 5 40.335 80.671 1.19006 24.4 2.2 2.0 6.1
95 7 3 3 41.952 83.903 1.15224 57.8 5.2 4.7 6.1
96 4 4 10 43.435 86.869 1.12036 28.0 2.5 2.3 6.1
97 7 2 6 43.536 87.072 1.11827 13.7 1.2 1.1 6.1
98 3 1 13 43.595 87.19 1.11707 45.7 4.1 3.7 6.2
99 8 0 2 43.797 87.595 1.11295 22.2 2.0 1.8 6.2
100 6 5 4 44.173 88.345 1.10542 16.8 1.5 1.4 6.2
101 7 4 2 44.218 88.436 1.10452 12.7 1.1 1.0 6.2
102 4 2 12 44.39 88.781 1.10112 11.9 1.1 1.0 6.2
Reference:
Chichagov A.V. et al.
Information-Calculating System on Crystal Structure Data of Minerals
(MINCRYST)
- Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian)
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