Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** CREEDITE 3, t-creedite Ca(3)Al(2)F(8)(OH)(2)[SO(4)].2H(2)O Monoclinic C 2/c Z = 4 R =0.023 NR =535 24 .11 .15 Ref.Str.: D.A. Ksenofontov, Yu.K. Kabalov, N.V. Zubkova, R.R. Shiyapova (2011) * Inorg. Materials, 47, 1402-1405 L: $Ca2.93 Al2.09 S0.96 F8.34 O7.66 H5.5$ R: Locality - the Akchatau mine, Kazakhstan. Coordinate Z of Ca(pos.2) corrected. N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 13.948 alpha = 90.0 b = 8.6051 beta = 94.37 c = 9.9823 gamma = 90.0 Unit cell volume (cub. angs.) = 1194.63 Molar volume ( cub.cm/mol.) = 179.89 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.2475 0.2193 0.1923 0.54 Ca = 0.99, Ca = 0.0 2 0.0 0.0251 0.25 0.88 Ca = 0.98, Ca = 0.0 3 0.2982 0.3996 0.4875 0.25 Al = 0.99, Al = 0.0 4 0.0 0.6575 0.25 0.85 S = 0.96, S = 0.0 5 0.1404 0.1227 0.3473 0.4 F = 1.00 6 0.407 0.4524 0.4271 0.8 F = 1.00 7 0.2649 0.4027 0.028 0.4 F = 1.00 8 0.234 0.4388 0.322 0.8 F = 1.00 9 0.4183 0.2612 0.1906 0.7 O = 1.00 10 0.4702 0.0585 0.3622 1.2 O = 1.00 11 0.0724 0.2613 0.1167 1.1 H(2)O = 1.00 12 0.3062 0.1869 0.4363 0.5 OH = 0.87, F = 0.17 13 0.064 0.246 0.038 3.3 H = 1.00 14 0.054 0.349 0.128 3.1 H = 1.00 15 0.355 0.154 0.434 1.4 H = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.2475 0.2193 0.1923 2 2 0.0 0.0251 0.25 3 3 0.2982 0.3996 0.4875 4 4 0.0 0.6575 0.25 5 5 0.1404 0.1227 0.3473 6 6 0.407 0.4524 0.4271 7 7 0.2649 0.4027 0.028 8 8 0.234 0.4388 0.322 9 9 0.4183 0.2612 0.1906 10 10 0.4702 0.0585 0.3622 11 11 0.0724 0.2613 0.1167 12 12 0.3062 0.1869 0.4363 13 13 0.064 0.246 0.038 14 14 0.054 0.349 0.128 15 15 0.355 0.154 0.434 16 1 0.7525 0.7807 0.8077 17 2 0.0 0.9749 0.75 18 3 0.7018 0.6004 0.5125 19 4 0.0 0.3425 0.75 20 5 0.8596 0.8773 0.6527 21 6 0.593 0.5476 0.5729 22 7 0.7351 0.5973 0.972 23 8 0.766 0.5612 0.678 24 9 0.5817 0.7388 0.8094 25 10 0.5298 0.9415 0.6378 26 11 0.9276 0.7387 0.8833 27 12 0.6938 0.8131 0.5637 28 13 0.936 0.754 0.962 29 14 0.946 0.651 0.872 30 15 0.645 0.846 0.566 31 1 0.2475 0.7807 0.6923 32 3 0.2982 0.6004 0.9875 33 5 0.1404 0.8773 0.8473 34 6 0.407 0.5476 0.9271 35 7 0.2649 0.5973 0.528 36 8 0.234 0.5612 0.822 37 9 0.4183 0.7388 0.6906 38 10 0.4702 0.9415 0.8622 39 11 0.0724 0.7387 0.6167 40 12 0.3062 0.8131 0.9363 41 13 0.064 0.754 0.538 42 14 0.054 0.651 0.628 43 15 0.355 0.846 0.934 44 1 0.7525 0.2193 0.3077 45 3 0.7018 0.3996 0.0125 46 5 0.8596 0.1227 0.1527 47 6 0.593 0.4524 0.0729 48 7 0.7351 0.4027 0.472 49 8 0.766 0.4388 0.178 50 9 0.5817 0.2612 0.3094 51 10 0.5298 0.0585 0.1378 52 11 0.9276 0.2613 0.3833 53 12 0.6938 0.1869 0.0637 54 13 0.936 0.246 0.462 55 14 0.946 0.349 0.372 56 15 0.645 0.154 0.066 57 1 0.7475 0.2807 0.6923 58 2 0.5 0.4749 0.75 59 3 0.7982 0.1004 0.9875 60 4 0.5 0.8425 0.75 61 5 0.6404 0.3773 0.8473 62 6 0.907 0.0476 0.9271 63 7 0.7649 0.0973 0.528 64 8 0.734 0.0612 0.822 65 9 0.9183 0.2388 0.6906 66 10 0.9702 0.4415 0.8622 67 11 0.5724 0.2387 0.6167 68 12 0.8062 0.3131 0.9363 69 13 0.564 0.254 0.538 70 14 0.554 0.151 0.628 71 15 0.855 0.346 0.934 72 1 0.2525 0.7193 0.3077 73 2 0.5 0.5251 0.25 74 3 0.2018 0.8996 0.0125 75 4 0.5 0.1575 0.25 76 5 0.3596 0.6227 0.1527 77 6 0.093 0.9524 0.0729 78 7 0.2351 0.9027 0.472 79 8 0.266 0.9388 0.178 80 9 0.0817 0.7612 0.3094 81 10 0.0298 0.5585 0.1378 82 11 0.4276 0.7613 0.3833 83 12 0.1938 0.6869 0.0637 84 13 0.436 0.746 0.462 85 14 0.446 0.849 0.372 86 15 0.145 0.654 0.066 87 1 0.7475 0.7193 0.1923 88 3 0.7982 0.8996 0.4875 89 5 0.6404 0.6227 0.3473 90 6 0.907 0.9524 0.4271 91 7 0.7649 0.9027 0.028 92 8 0.734 0.9388 0.322 93 9 0.9183 0.7612 0.1906 94 10 0.9702 0.5585 0.3622 95 11 0.5724 0.7613 0.1167 96 12 0.8062 0.6869 0.4363 97 13 0.564 0.746 0.038 98 14 0.554 0.849 0.128 99 15 0.855 0.654 0.434 100 1 0.2525 0.2807 0.8077 101 3 0.2018 0.1004 0.5125 102 5 0.3596 0.3773 0.6527 103 6 0.093 0.0476 0.5729 104 7 0.2351 0.0973 0.972 105 8 0.266 0.0612 0.678 106 9 0.0817 0.2388 0.8094 107 10 0.0298 0.4415 0.6378 108 11 0.4276 0.2387 0.8833 109 12 0.1938 0.3131 0.5637 110 13 0.436 0.254 0.962 111 14 0.446 0.151 0.872 112 15 0.145 0.346 0.566 X-ray density (g/cm cub.) = 2.76 MU (1/cm) = 159.239 Mass attenuation coefficient (cm**2/g) = 57.651 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Ca ,Ca 3.048 8 2.3809 5 2.3022 7 2.3058 8 2.4108 9 2.5267 11 2.5252 12 2.4328 8 2.4311 7 2 Ca ,Ca 3.048 8 2.279 5 2.6695 11 2.279 5 2.6695 11 2.3556 6 2.5892 9 2.3556 6 2.5892 9 3 Al ,Al 2.484 6 1.7356 6 1.8492 8 1.9059 12 1.8171 7 1.8096 5 1.8498 12 4 S ,S 2.148 4 1.5308 9 1.4913 10 1.5308 9 1.4913 10 5 F 3.396 10 3.036 8 2.6997 11 2.4758 12 3.2441 11 3.1323 6 2.5744 7 2.98 8 3.2316 9 2.4806 6 2.7677 12 6 F 3.396 9 2.5595 8 2.8917 9 2.6878 12 2.9907 6 2.608 7 3.2344 9 3.1323 5 2.7126 11 2.4806 5 7 F 3.396 9 3.0146 8 2.8576 9 3.1362 11 2.608 6 2.4778 8 2.5744 5 2.673 12 2.7122 7 3.1189 11 8 F 3.396 10 3.036 5 2.5595 6 3.0146 7 3.3434 9 3.3029 11 2.6152 12 2.4778 7 2.98 5 3.3616 12 2.7408 12 9 O 3.432 10 2.8917 6 2.8576 7 3.3434 8 2.5123 10 3.0746 12 3.2344 6 2.4877 9 2.4215 10 3.2316 5 3.0862 11 10 O 3.432 8 2.5123 9 2.6941 12 2.9874 10 2.4215 9 2.448 10 3.2154 11 3.4287 8 2.6376 11 11 H(2)O 3.6 11 2.6997 5 3.1362 7 3.3029 8 3.2441 5 3.4613 11 3.4089 6 3.2154 10 2.7126 6 2.6376 10 3.1189 7 3.0862 9 12 OH ,F 3.48 10 2.4758 5 2.6878 6 2.6152 8 3.0746 9 2.6941 10 2.673 7 3.3616 8 2.7677 5 2.7408 8 2.3576 12 13 H 1.8 1 0.7964 11 14 H 1.8 1 0.8078 11 15 H 1.8 1 0.7392 12 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 1 1 0 6.042 12.085 0.068 177.53 4 78.9 309.9 2 2 0 0 6.36 12.72 0.072 160.03 2 132.7 394.8 3 1 1 -1 7.361 14.723 0.083 118.87 4 19.8 13.0 4 1 1 1 7.65 15.301 0.086 109.9 4 78.7 190.6 5 0 0 2 8.904 17.808 0.1 80.55 2 92.3 96.2 6 0 2 0 10.313 20.626 0.116 59.49 2 54.4 24.7 7 2 0 -2 10.564 21.129 0.119 56.59 2 92.0 67.2 8 1 1 -2 10.583 21.166 0.119 56.39 4 29.9 14.1 9 3 1 0 10.879 21.758 0.123 53.25 4 91.0 123.5 10 1 1 2 10.99 21.98 0.124 52.13 4 6.0 0.5 11 0 2 1 11.247 22.494 0.127 49.68 4 124.1 214.4 12 2 0 2 11.366 22.732 0.128 48.6 2 192.9 253.6 13 3 1 -1 11.486 22.972 0.129 47.55 4 69.2 63.8 14 3 1 1 12.048 24.096 0.135 43.02 4 39.7 19.0 15 2 2 0 12.153 24.307 0.137 42.25 4 97.4 112.3 16 2 2 -1 12.789 25.579 0.144 37.95 4 119.1 151.0 17 4 0 0 12.8 25.6 0.144 37.89 2 288.1 440.7 18 2 2 1 13.132 26.264 0.147 35.89 4 0.3 0.0 19 3 1 -2 13.646 27.292 0.153 33.09 4 127.9 151.7 20 0 2 2 13.689 27.379 0.154 32.87 4 87.0 69.7 21 1 1 -3 14.539 29.079 0.163 28.91 4 168.9 231.1 22 3 1 2 14.595 29.19 0.164 28.68 4 30.3 7.4 23 2 2 -2 14.848 29.696 0.166 27.64 4 89.5 62.0 24 1 1 3 14.995 29.99 0.168 27.07 4 70.6 37.8 25 4 0 -2 15.094 30.189 0.169 26.68 2 65.9 16.2 26 2 2 2 15.441 30.883 0.173 25.41 4 103.5 76.2 27 1 3 0 15.914 31.828 0.178 23.82 4 91.9 56.4 28 4 0 2 16.246 32.491 0.182 22.78 2 216.5 149.6 29 1 3 -1 16.485 32.969 0.184 22.07 4 131.7 107.3 30 4 2 0 16.549 33.098 0.185 21.88 4 10.4 0.7 31 1 3 1 16.622 33.243 0.186 21.68 4 118.8 85.7 32 3 1 -3 16.811 33.622 0.188 21.15 4 36.1 7.7 33 4 2 -1 16.9 33.8 0.189 20.91 4 38.4 8.6 34 5 1 0 16.92 33.84 0.189 20.85 4 15.3 1.4 35 0 2 3 17.048 34.097 0.19 20.51 4 80.9 37.6 36 5 1 -1 17.198 34.397 0.192 20.13 4 146.1 120.4 37 4 2 1 17.431 34.862 0.194 19.54 4 52.4 15.1 38 5 1 1 17.85 35.7 0.199 18.56 4 89.1 41.3 39 2 2 -3 17.884 35.768 0.199 18.48 4 40.8 8.6 40 3 1 3 17.991 35.983 0.2 18.24 4 124.4 79.1 41 0 0 4 18.033 36.065 0.201 18.15 2 71.9 13.1 42 1 3 -2 18.227 36.454 0.203 17.72 4 2.8 0.0 43 3 3 0 18.409 36.817 0.205 17.34 4 92.3 41.4 44 4 2 -2 18.422 36.844 0.205 17.31 4 74.2 26.7 45 1 3 2 18.477 36.955 0.206 17.2 4 103.6 51.7 46 5 1 -2 18.637 37.274 0.207 16.88 4 70.0 23.2 47 2 2 3 18.639 37.277 0.207 16.87 4 27.5 3.6 48 2 0 -4 18.707 37.415 0.208 16.74 2 106.6 26.6 49 3 3 -1 18.79 37.581 0.209 16.57 4 25.1 2.9 50 1 1 -4 18.841 37.682 0.21 16.48 4 16.9 1.3 51 3 3 1 19.156 38.311 0.213 15.89 4 108.1 52.0 52 1 1 4 19.326 38.651 0.215 15.58 4 110.7 53.5 53 4 2 2 19.399 38.797 0.216 15.45 4 57.5 14.3 54 6 0 0 19.409 38.819 0.216 15.43 2 140.9 42.9 55 2 0 4 19.672 39.344 0.219 14.98 2 218.9 100.6 56 5 1 2 19.84 39.681 0.22 14.7 4 17.1 1.2 57 3 3 -2 20.247 40.494 0.225 14.05 4 54.1 11.5 58 3 1 -4 20.584 41.168 0.228 13.54 4 178.8 121.2 59 6 0 -2 20.839 41.678 0.231 13.17 2 80.9 12.1 60 1 3 -3 20.888 41.777 0.231 13.1 4 265.0 257.9 61 4 2 -3 20.894 41.789 0.232 13.09 4 87.3 27.9 62 3 3 2 20.929 41.858 0.232 13.05 4 160.6 94.3 63 0 2 4 20.953 41.906 0.232 13.01 4 42.8 6.7 64 0 4 0 20.981 41.962 0.232 12.97 2 43.7 3.5 65 5 1 -3 21.033 42.065 0.233 12.9 4 50.4 9.2 66 1 3 3 21.223 42.446 0.235 12.64 4 54.2 10.4 67 0 4 1 21.489 42.978 0.238 12.3 4 104.5 37.6 68 4 0 -4 21.511 43.022 0.238 12.27 2 166.1 47.4 69 2 2 -4 21.55 43.101 0.238 12.22 4 2.3 0.0 70 3 1 4 21.914 43.828 0.242 11.77 4 110.9 40.5 71 2 4 0 22.012 44.024 0.243 11.65 4 81.5 21.7 72 6 0 2 22.156 44.312 0.245 11.48 2 91.8 13.5 73 6 2 0 22.177 44.354 0.245 11.45 4 127.2 52.0 74 4 2 3 22.209 44.418 0.245 11.42 4 56.7 10.3 75 6 2 -1 22.346 44.693 0.247 11.26 4 65.9 13.7 76 2 4 -1 22.395 44.791 0.247 11.2 4 221.9 154.6 77 2 2 4 22.413 44.826 0.247 11.18 4 32.0 3.2 78 3 3 -3 22.605 45.21 0.25 10.97 4 10.1 0.3 79 2 4 1 22.607 45.214 0.25 10.97 4 91.9 26.0 80 5 1 3 22.658 45.316 0.25 10.91 4 166.2 84.5 81 5 3 0 22.691 45.381 0.25 10.88 4 50.9 7.9 82 5 3 -1 22.909 45.818 0.253 10.64 4 50.8 7.7 83 0 4 2 22.959 45.919 0.253 10.59 4 153.7 70.2 84 6 2 1 22.978 45.956 0.253 10.57 4 126.9 47.7 85 4 0 4 23.213 46.427 0.256 10.33 2 171.7 42.7 86 1 1 -5 23.386 46.771 0.258 10.16 4 153.3 66.9 87 5 3 1 23.426 46.853 0.258 10.12 4 41.0 4.8 88 7 1 0 23.447 46.894 0.258 10.1 4 8.2 0.2 89 6 2 -2 23.469 46.938 0.259 10.08 4 182.5 94.1 90 3 3 3 23.539 47.079 0.259 10.01 4 70.8 14.1 91 7 1 -1 23.558 47.116 0.259 9.99 4 99.5 27.7 92 2 4 -2 23.72 47.44 0.261 9.84 4 164.4 74.5 93 1 1 5 23.895 47.79 0.263 9.68 4 20.5 1.1 94 5 3 -2 24.061 48.123 0.265 9.52 4 144.8 56.0 95 4 2 -4 24.083 48.165 0.265 9.5 4 0.6 0.0 96 2 4 2 24.124 48.248 0.265 9.47 4 51.0 6.9 97 5 1 -4 24.156 48.312 0.266 9.44 4 59.5 9.4 98 1 3 -4 24.228 48.455 0.266 9.38 4 155.6 63.6 99 7 1 1 24.265 48.53 0.267 9.34 4 94.0 23.2 100 7 1 -2 24.589 49.177 0.27 9.07 4 205.6 107.4 101 1 3 4 24.625 49.25 0.27 9.04 4 13.6 0.5 102 6 2 2 24.675 49.35 0.271 8.99 4 106.9 28.8 103 3 1 -5 24.771 49.542 0.272 8.92 4 129.9 42.1 104 4 4 0 24.901 49.802 0.273 8.81 4 44.5 4.9 105 5 3 2 25.051 50.103 0.275 8.69 4 41.6 4.2 106 4 4 -1 25.154 50.307 0.276 8.61 4 128.3 39.7 107 0 2 5 25.237 50.473 0.277 8.55 4 46.6 5.2 108 0 4 3 25.261 50.522 0.277 8.53 4 36.7 3.2 109 6 2 -3 25.448 50.895 0.279 8.38 4 125.1 36.8 110 4 4 1 25.54 51.081 0.28 8.32 4 30.8 2.2 111 4 2 4 25.652 51.305 0.281 8.23 4 26.3 1.6 112 2 2 -5 25.66 51.321 0.281 8.23 4 69.1 11.0 113 3 3 -4 25.674 51.349 0.281 8.22 4 41.2 3.9 114 2 4 -3 25.875 51.751 0.283 8.07 4 53.0 6.4 115 6 0 -4 25.885 51.769 0.283 8.07 2 77.1 6.7 116 7 1 2 25.946 51.892 0.284 8.02 4 39.7 3.5 117 5 3 -3 26.054 52.108 0.285 7.95 4 124.5 34.5 118 5 1 4 26.103 52.207 0.286 7.91 4 188.4 78.7 119 3 1 5 26.216 52.432 0.287 7.84 4 5.8 0.1 120 4 4 -2 26.279 52.558 0.287 7.79 4 110.7 26.7 121 8 0 0 26.301 52.602 0.288 7.78 2 129.7 18.3 122 2 4 3 26.443 52.886 0.289 7.68 4 33.9 2.5 123 7 1 -3 26.458 52.917 0.289 7.67 4 13.9 0.4 124 2 2 5 26.607 53.213 0.291 7.58 4 38.2 3.1 125 1 5 0 26.807 53.614 0.293 7.45 4 16.8 0.6 126 3 3 4 26.807 53.614 0.293 7.45 4 123.7 32.0 127 4 4 2 27.026 54.051 0.295 7.31 4 123.7 31.4 128 6 2 3 27.144 54.288 0.296 7.24 4 69.5 9.8 129 1 5 -1 27.185 54.37 0.297 7.21 4 11.4 0.3 130 8 0 -2 27.263 54.526 0.297 7.17 2 218.5 47.9 131 1 5 1 27.277 54.554 0.297 7.16 4 37.6 2.8 132 5 3 3 27.451 54.901 0.299 7.06 4 158.9 50.0 133 0 0 6 27.667 55.335 0.301 6.93 2 80.6 6.3 134 4 2 -5 27.82 55.639 0.303 6.85 4 6.2 0.1 135 5 1 -5 27.841 55.681 0.303 6.83 4 139.9 37.5 136 2 0 -6 27.975 55.95 0.304 6.76 2 203.7 39.3 137 1 3 -5 28.086 56.172 0.306 6.7 4 122.0 28.0 138 6 0 4 28.106 56.212 0.306 6.69 2 58.5 3.2 139 7 3 0 28.14 56.279 0.306 6.67 4 47.2 4.2 140 6 2 -4 28.154 56.308 0.306 6.66 4 3.9 0.0 141 1 1 -6 28.163 56.327 0.306 6.66 4 5.3 0.1 142 4 4 -3 28.203 56.406 0.307 6.64 4 24.5 1.1 143 7 3 -1 28.237 56.474 0.307 6.62 4 27.4 1.4 144 0 4 4 28.25 56.5 0.307 6.61 4 50.0 4.6 145 7 1 3 28.381 56.763 0.309 6.54 4 76.1 10.6 146 1 5 -2 28.388 56.775 0.309 6.54 4 16.2 0.5 147 3 5 0 28.517 57.034 0.31 6.47 4 130.9 31.1 148 1 3 5 28.534 57.068 0.31 6.46 4 127.3 29.4 149 8 2 0 28.548 57.095 0.31 6.46 4 26.6 1.3 150 1 5 2 28.566 57.133 0.31 6.45 4 91.7 15.2 151 8 2 -1 28.6 57.2 0.311 6.43 4 63.5 7.3 152 1 1 6 28.7 57.399 0.312 6.38 4 67.8 8.2 153 8 0 2 28.708 57.416 0.312 6.37 2 187.0 31.2 154 2 4 -4 28.731 57.463 0.312 6.36 4 51.4 4.7 155 5 3 -4 28.765 57.53 0.312 6.35 4 114.0 23.1 156 3 5 -1 28.791 57.583 0.313 6.33 4 67.6 8.1 157 7 3 1 28.861 57.723 0.313 6.3 4 25.3 1.1 158 2 0 6 29.046 58.092 0.315 6.21 2 210.1 38.4 159 7 1 -4 29.056 58.111 0.315 6.2 4 14.4 0.4 160 3 5 1 29.057 58.113 0.315 6.2 4 33.8 2.0 161 7 3 -2 29.148 58.297 0.316 6.16 4 66.5 7.6 162 6 4 0 29.243 58.485 0.317 6.11 4 125.9 27.2 163 4 4 3 29.269 58.537 0.317 6.1 4 75.4 9.7 164 3 1 -6 29.299 58.597 0.318 6.09 4 66.1 7.5 165 8 2 1 29.307 58.613 0.318 6.08 4 92.2 14.5 166 3 3 -5 29.311 58.621 0.318 6.08 4 41.4 2.9 167 6 4 -1 29.381 58.763 0.318 6.05 4 100.3 17.1 168 2 4 4 29.436 58.872 0.319 6.02 4 33.8 1.9 169 8 2 -2 29.46 58.92 0.319 6.01 4 42.4 3.0 170 4 2 5 29.596 59.193 0.321 5.95 4 105.3 18.5 171 0 2 6 29.845 59.69 0.323 5.84 4 35.9 2.1 172 3 5 -2 29.865 59.731 0.323 5.83 4 15.4 0.4 173 6 4 1 29.904 59.808 0.324 5.82 4 81.6 10.9 174 4 0 -6 29.935 59.869 0.324 5.8 2 57.8 2.7 175 5 1 5 30.05 60.101 0.325 5.75 4 32.6 1.7 176 2 2 -6 30.138 60.276 0.326 5.71 4 10.6 0.2 177 6 2 4 30.263 60.526 0.327 5.66 4 31.0 1.5 178 6 4 -2 30.314 60.628 0.328 5.64 4 40.4 2.6 179 1 5 -3 30.351 60.703 0.328 5.63 4 34.5 1.9 180 7 3 2 30.365 60.729 0.328 5.62 4 75.8 9.1 181 3 5 2 30.383 60.765 0.328 5.61 4 78.5 9.7 182 9 1 0 30.428 60.855 0.329 5.59 4 62.1 6.1 183 9 1 -1 30.435 60.87 0.329 5.59 4 72.3 8.2 184 5 3 4 30.507 61.013 0.33 5.56 4 5.1 0.0 185 1 5 3 30.608 61.217 0.331 5.52 4 110.1 18.8 186 3 3 5 30.608 61.217 0.331 5.52 4 203.0 63.8 187 7 3 -3 30.828 61.655 0.333 5.43 4 179.3 49.0 188 4 4 -4 30.831 61.662 0.333 5.43 4 21.7 0.7 189 8 2 2 30.839 61.678 0.333 5.43 4 3.0 0.0 190 3 1 6 30.852 61.704 0.333 5.42 4 103.9 16.4 191 8 2 -3 31.087 62.174 0.335 5.33 4 112.0 18.7 192 2 2 6 31.162 62.325 0.336 5.31 4 70.1 7.3 193 9 1 1 31.2 62.401 0.336 5.29 4 41.2 2.5 194 9 1 -2 31.222 62.444 0.336 5.28 4 5.0 0.0 195 6 4 2 31.334 62.669 0.338 5.24 4 77.6 8.8 196 8 0 -4 31.387 62.774 0.338 5.22 2 12.7 0.1 197 7 1 4 31.464 62.928 0.339 5.19 4 77.4 8.7 198 6 2 -5 31.475 62.95 0.339 5.19 4 85.7 10.7 199 3 5 -3 31.689 63.378 0.341 5.11 4 29.2 1.2 200 5 5 0 31.757 63.514 0.342 5.09 4 62.0 5.5 201 0 4 5 31.816 63.632 0.342 5.07 4 77.1 8.5 202 5 5 -1 31.931 63.862 0.343 5.03 4 105.5 15.7 203 4 0 6 31.972 63.943 0.344 5.02 2 120.1 10.1 204 5 1 -6 31.994 63.987 0.344 5.01 4 50.1 3.5 205 6 4 -3 31.998 63.996 0.344 5.01 4 55.3 4.3 206 4 2 -6 32.016 64.032 0.344 5.0 4 47.0 3.1 207 5 3 -5 32.089 64.177 0.345 4.98 4 75.1 7.9 208 4 4 4 32.175 64.35 0.346 4.95 4 92.1 11.8 209 2 4 -5 32.182 64.364 0.346 4.94 4 19.5 0.5 210 7 1 -5 32.278 64.557 0.347 4.91 4 110.3 16.7 211 5 5 1 32.347 64.693 0.347 4.89 4 86.9 10.3 212 1 3 -6 32.385 64.77 0.348 4.88 4 133.9 24.5 213 3 5 3 32.438 64.876 0.348 4.86 4 91.3 11.4 214 0 6 0 32.486 64.971 0.349 4.85 2 127.9 11.1 215 7 3 3 32.586 65.172 0.35 4.81 4 70.3 6.7 216 9 1 2 32.722 65.443 0.351 4.77 4 83.9 9.4 217 9 1 -3 32.756 65.513 0.351 4.76 4 69.9 6.5 218 5 5 -2 32.862 65.724 0.352 4.73 4 91.7 11.1 219 0 6 1 32.863 65.726 0.352 4.73 4 40.0 2.1 220 1 3 6 32.879 65.759 0.352 4.72 4 97.9 12.7 221 1 5 -4 32.998 65.996 0.354 4.69 4 68.0 6.1 222 2 4 5 33.007 66.013 0.354 4.68 4 18.7 0.5 223 8 2 3 33.083 66.166 0.354 4.66 4 11.6 0.2 224 7 3 -4 33.209 66.418 0.356 4.62 4 81.1 8.5 225 1 1 -7 33.209 66.419 0.356 4.62 4 37.7 1.8 226 2 6 0 33.257 66.513 0.356 4.61 4 112.3 16.3 227 1 5 4 33.325 66.65 0.357 4.59 4 98.3 12.4 228 6 0 -6 33.369 66.738 0.357 4.58 2 134.9 11.7 229 8 2 -4 33.417 66.834 0.357 4.56 4 40.5 2.1 230 3 3 -6 33.434 66.868 0.358 4.56 4 14.9 0.3 231 6 4 3 33.479 66.958 0.358 4.54 4 71.1 6.4 232 2 6 -1 33.549 67.097 0.359 4.52 4 59.2 4.4 233 10 0 0 33.632 67.265 0.36 4.5 2 32.1 0.6 234 5 5 2 33.678 67.356 0.36 4.49 4 135.5 23.1 235 2 6 1 33.711 67.422 0.36 4.48 4 7.5 0.1 236 1 1 7 33.779 67.557 0.361 4.46 4 74.5 6.9 237 6 2 5 33.945 67.89 0.362 4.41 4 7.3 0.1 238 0 6 2 33.983 67.966 0.363 4.4 4 56.9 4.0 239 4 2 6 33.983 67.966 0.363 4.4 4 58.9 4.3 240 8 0 4 34.022 68.045 0.363 4.39 2 111.5 7.7 241 4 4 -5 34.078 68.155 0.364 4.38 4 9.9 0.1 242 5 3 5 34.134 68.268 0.364 4.36 4 36.3 1.6 243 3 1 -7 34.165 68.33 0.365 4.35 4 10.1 0.1 244 3 5 -4 34.199 68.397 0.365 4.35 4 106.9 13.9 245 10 0 -2 34.306 68.611 0.366 4.32 2 33.2 0.7 246 6 4 -4 34.375 68.751 0.366 4.3 4 48.2 2.8 247 5 1 6 34.444 68.889 0.367 4.28 4 21.5 0.6 248 9 3 0 34.486 68.973 0.368 4.27 4 40.7 2.0 249 9 3 -1 34.493 68.986 0.368 4.27 4 24.7 0.7 250 5 5 -3 34.518 69.037 0.368 4.26 4 45.7 2.5 251 2 6 -2 34.577 69.155 0.368 4.25 4 27.2 0.9 252 8 4 0 34.728 69.456 0.37 4.21 4 26.5 0.8 253 8 4 -1 34.774 69.549 0.37 4.2 4 110.8 14.5 254 0 2 7 34.788 69.576 0.37 4.2 4 72.1 6.1 255 3 3 6 34.884 69.768 0.371 4.17 4 36.8 1.6 256 2 6 2 34.897 69.794 0.371 4.17 4 26.5 0.8 257 9 1 3 34.941 69.883 0.372 4.16 4 35.2 1.4 258 2 2 -7 34.979 69.958 0.372 4.15 4 46.8 2.5 259 9 1 -4 34.988 69.977 0.372 4.15 4 2.1 0.0 260 7 1 5 35.117 70.235 0.373 4.12 4 85.6 8.5 261 3 5 4 35.159 70.317 0.374 4.11 4 9.2 0.1 262 9 3 1 35.211 70.423 0.374 4.09 4 60.4 4.2 263 9 3 -2 35.231 70.463 0.374 4.09 4 103.6 12.3 264 6 2 -6 35.34 70.68 0.375 4.07 4 15.1 0.3 265 8 4 1 35.411 70.822 0.376 4.05 4 17.9 0.4 266 7 3 4 35.459 70.919 0.377 4.04 4 132.6 19.9 267 4 6 0 35.52 71.04 0.377 4.02 4 26.5 0.8 268 8 4 -2 35.55 71.1 0.377 4.02 4 9.3 0.1 269 10 2 -1 35.564 71.128 0.378 4.01 4 31.8 1.1 270 10 2 0 35.597 71.194 0.378 4.01 4 86.9 8.5 271 4 4 5 35.673 71.347 0.379 3.99 4 13.8 0.2 272 5 5 3 35.712 71.423 0.379 3.98 4 46.1 2.4 273 4 6 -1 35.724 71.448 0.379 3.98 4 186.0 38.6 274 0 6 3 35.811 71.623 0.38 3.96 4 44.9 2.2 275 3 1 7 35.838 71.676 0.38 3.95 4 62.1 4.3 276 10 0 2 35.897 71.794 0.381 3.94 2 110.8 6.8 277 0 4 6 35.899 71.798 0.381 3.94 4 55.7 3.4 278 5 3 -6 35.959 71.919 0.381 3.93 4 91.2 9.2 279 8 2 4 35.977 71.954 0.381 3.92 4 8.8 0.1 280 4 6 1 36.039 72.079 0.382 3.91 4 52.0 3.0 281 7 1 -6 36.061 72.122 0.382 3.91 4 9.7 0.1 282 2 2 7 36.087 72.174 0.382 3.9 4 47.6 2.5 283 2 4 -6 36.166 72.332 0.383 3.88 4 40.7 1.8 284 7 3 -5 36.229 72.458 0.384 3.87 4 3.1 0.0 285 6 0 6 36.245 72.489 0.384 3.87 2 84.4 3.9 286 10 2 -2 36.254 72.507 0.384 3.87 4 51.2 2.8 287 1 5 -5 36.262 72.524 0.384 3.86 4 31.4 1.1 288 6 4 4 36.28 72.56 0.384 3.86 4 32.1 1.1 289 7 5 0 36.309 72.619 0.384 3.86 4 62.4 4.2 290 2 6 -3 36.314 72.628 0.384 3.85 4 8.0 0.1 291 10 2 1 36.351 72.703 0.385 3.85 4 21.0 0.5 292 8 2 -5 36.39 72.78 0.385 3.84 4 12.6 0.2 293 7 5 -1 36.394 72.789 0.385 3.84 4 21.1 0.5 294 5 1 -7 36.59 73.179 0.387 3.8 4 51.7 2.8 295 4 6 -2 36.647 73.295 0.387 3.79 4 87.3 8.1 296 9 3 2 36.649 73.299 0.387 3.79 4 15.8 0.3 297 4 2 -7 36.65 73.299 0.387 3.79 4 162.9 28.2 298 1 5 5 36.654 73.308 0.388 3.79 4 100.2 10.7 299 9 3 -3 36.682 73.364 0.388 3.78 4 167.5 29.7 300 2 6 3 36.784 73.567 0.389 3.76 4 48.3 2.5 301 8 4 2 36.807 73.613 0.389 3.76 4 29.3 0.9 302 5 5 -4 36.856 73.713 0.389 3.75 4 71.9 5.4 303 7 5 1 36.941 73.882 0.39 3.73 4 24.7 0.6 304 8 4 -3 37.034 74.069 0.391 3.71 4 36.6 1.4 305 2 4 6 37.104 74.208 0.392 3.7 4 55.2 3.2 306 1 3 -7 37.113 74.226 0.392 3.7 4 35.0 1.3 307 7 5 -2 37.194 74.389 0.392 3.68 4 19.5 0.4 308 4 6 2 37.271 74.541 0.393 3.67 4 19.7 0.4 309 3 5 -5 37.338 74.676 0.394 3.66 4 45.1 2.1 310 6 4 -5 37.392 74.784 0.394 3.65 4 5.3 0.0 311 10 2 -3 37.65 75.3 0.397 3.6 4 33.8 1.2 312 1 3 7 37.656 75.312 0.397 3.6 4 13.9 0.2 313 9 1 4 37.81 75.621 0.398 3.58 4 94.1 8.9 314 10 2 2 37.811 75.621 0.398 3.58 4 40.5 1.6 315 10 0 -4 37.848 75.695 0.398 3.57 2 72.7 2.6 316 9 1 -5 37.869 75.738 0.398 3.57 4 114.3 13.1 317 4 4 -6 37.892 75.785 0.399 3.56 4 7.8 0.1 318 11 1 -1 37.939 75.877 0.399 3.55 4 28.9 0.8 319 11 1 0 38.009 76.018 0.4 3.54 4 36.5 1.3 320 3 3 -7 38.026 76.051 0.4 3.54 4 15.8 0.2 321 8 0 -6 38.091 76.182 0.4 3.53 2 7.0 0.0 322 6 2 6 38.152 76.303 0.401 3.52 4 62.4 3.8 323 0 0 8 38.252 76.503 0.402 3.5 2 15.2 0.1 324 4 6 -3 38.269 76.539 0.402 3.5 4 21.9 0.5 325 7 5 2 38.277 76.554 0.402 3.5 4 127.8 16.0 326 5 3 6 38.293 76.587 0.402 3.5 4 63.9 4.0 327 0 6 4 38.31 76.619 0.402 3.49 4 16.8 0.3 328 2 0 -8 38.359 76.718 0.403 3.49 2 109.6 5.9 329 5 5 4 38.405 76.809 0.403 3.48 4 38.6 1.5 330 3 5 5 38.496 76.992 0.404 3.46 4 52.9 2.7 331 11 1 -2 38.574 77.148 0.405 3.45 4 42.9 1.8 332 1 1 -8 38.596 77.192 0.405 3.45 4 13.4 0.2 333 7 5 -3 38.694 77.387 0.406 3.43 4 114.3 12.6 334 2 6 -4 38.724 77.447 0.406 3.43 4 95.8 8.8 335 9 3 3 38.771 77.541 0.406 3.42 4 109.1 11.4 336 11 1 1 38.785 77.569 0.407 3.42 4 166.9 26.7 337 4 2 7 38.815 77.63 0.407 3.42 4 5.0 0.0 338 9 3 -4 38.816 77.632 0.407 3.42 4 46.2 2.0 339 8 4 3 38.887 77.774 0.408 3.41 4 56.1 3.0 340 7 3 5 38.94 77.88 0.408 3.4 4 66.7 4.2 341 1 7 0 38.98 77.959 0.408 3.39 4 6.8 0.0 342 6 6 0 39.167 78.334 0.41 3.37 4 143.0 19.3 343 4 6 3 39.19 78.379 0.41 3.36 4 26.6 0.7 344 8 4 -4 39.2 78.399 0.41 3.36 4 26.1 0.6 345 1 1 8 39.209 78.418 0.41 3.36 4 15.4 0.2 346 6 6 -1 39.288 78.576 0.411 3.35 4 56.0 2.9 347 1 7 -1 39.292 78.584 0.411 3.35 4 9.5 0.1 348 5 1 7 39.292 78.584 0.411 3.35 4 6.4 0.0 349 7 1 6 39.312 78.623 0.411 3.35 4 29.6 0.8 350 2 6 4 39.336 78.672 0.411 3.34 4 134.8 17.0 351 1 7 1 39.368 78.736 0.412 3.34 4 29.0 0.8 352 3 1 -8 39.421 78.843 0.412 3.33 4 63.5 3.8 353 8 2 5 39.479 78.958 0.413 3.32 4 12.2 0.1 354 2 0 8 39.584 79.167 0.414 3.31 2 164.6 12.6 355 3 3 7 39.635 79.27 0.414 3.3 4 2.1 0.0 356 6 4 5 39.697 79.393 0.415 3.29 4 35.9 1.2 357 10 2 -4 39.728 79.457 0.415 3.29 4 75.4 5.2 358 6 2 -7 39.729 79.458 0.415 3.29 4 3.8 0.0 359 4 4 6 39.732 79.464 0.415 3.29 4 35.9 1.2 360 6 6 1 39.745 79.491 0.415 3.29 4 33.6 1.0 361 5 5 -5 39.839 79.678 0.416 3.28 4 41.1 1.6 362 7 3 -6 39.85 79.701 0.416 3.27 4 4.3 0.0 363 4 0 -8 39.902 79.803 0.416 3.27 2 7.2 0.0 364 11 1 -3 39.905 79.81 0.416 3.27 4 18.2 0.3 365 10 2 3 39.95 79.899 0.417 3.26 4 35.7 1.2 366 8 2 -6 39.968 79.937 0.417 3.26 4 86.1 6.8 367 6 6 -2 40.107 80.214 0.418 3.24 4 68.3 4.2 368 1 5 -6 40.111 80.221 0.418 3.24 4 6.5 0.0 369 0 2 8 40.127 80.254 0.418 3.24 4 94.3 8.1 370 2 2 -8 40.233 80.465 0.419 3.23 4 49.4 2.2 371 11 1 2 40.253 80.505 0.419 3.22 4 7.6 0.1 372 7 5 3 40.295 80.59 0.42 3.22 4 13.9 0.2 373 1 7 -2 40.301 80.601 0.42 3.22 4 68.0 4.2 374 5 3 -7 40.362 80.725 0.42 3.21 4 111.1 11.1 375 7 1 -7 40.384 80.768 0.421 3.21 4 40.9 1.5 376 3 7 0 40.41 80.821 0.421 3.2 4 0.3 0.0 377 1 7 2 40.452 80.904 0.421 3.2 4 60.8 3.3 378 0 4 7 40.494 80.987 0.422 3.19 4 106.8 10.2 379 1 5 6 40.566 81.132 0.422 3.19 4 52.7 2.5 380 4 6 -4 40.566 81.132 0.422 3.19 4 11.7 0.1 381 3 7 -1 40.644 81.288 0.423 3.18 4 46.1 1.9 382 2 4 -7 40.675 81.35 0.423 3.17 4 61.7 3.4 383 7 5 -4 40.87 81.74 0.425 3.15 4 85.2 6.4 384 3 7 1 40.871 81.742 0.425 3.15 4 0.9 0.0 385 10 0 4 40.902 81.804 0.425 3.15 2 148.7 9.8 386 6 6 2 41.016 82.032 0.426 3.14 4 62.5 3.4 387 6 4 -6 41.019 82.037 0.426 3.14 4 51.3 2.3 388 3 5 -6 41.079 82.158 0.427 3.13 4 26.6 0.6 389 10 4 -1 41.232 82.464 0.428 3.11 4 7.0 0.0 390 3 1 8 41.242 82.485 0.428 3.11 4 8.1 0.1 391 10 4 0 41.263 82.527 0.428 3.11 4 35.5 1.1 392 9 1 5 41.301 82.601 0.428 3.11 4 41.3 1.5 393 9 1 -6 41.371 82.741 0.429 3.1 4 12.7 0.1 394 2 2 8 41.443 82.886 0.43 3.09 4 45.9 1.8 395 0 6 5 41.449 82.899 0.43 3.09 4 49.5 2.1 396 9 3 4 41.55 83.1 0.431 3.08 4 43.3 1.6 397 3 7 -2 41.57 83.14 0.431 3.08 4 83.6 6.0 398 9 3 -5 41.607 83.215 0.431 3.08 4 21.1 0.4 399 6 6 -3 41.614 83.228 0.431 3.07 4 10.6 0.1 400 8 4 4 41.627 83.254 0.431 3.07 4 93.0 7.5 401 12 0 0 41.654 83.308 0.431 3.07 2 118.6 6.1 402 5 1 -8 41.662 83.325 0.431 3.07 4 76.7 5.1 403 11 3 -1 41.675 83.35 0.432 3.07 4 20.4 0.4 404 5 5 5 41.731 83.462 0.432 3.06 4 101.2 8.8 405 2 4 7 41.732 83.464 0.432 3.06 4 124.8 13.4 406 8 0 6 41.744 83.488 0.432 3.06 2 1.2 0.0 407 11 3 0 41.744 83.488 0.432 3.06 4 117.9 11.9 408 4 2 -8 41.758 83.516 0.432 3.06 4 87.9 6.6 409 4 6 4 41.774 83.549 0.432 3.06 4 41.2 1.5 410 2 6 -5 41.781 83.561 0.432 3.06 4 71.2 4.3 411 10 4 -2 41.892 83.784 0.433 3.05 4 7.4 0.0 412 11 1 -4 41.916 83.832 0.434 3.05 4 45.9 1.8 413 10 4 1 41.986 83.972 0.434 3.04 4 74.9 4.8 414 1 7 -3 41.994 83.989 0.434 3.04 4 95.0 7.7 415 3 7 2 42.022 84.043 0.435 3.04 4 37.7 1.2 416 8 4 -5 42.023 84.046 0.435 3.04 4 56.0 2.7 417 9 5 0 42.061 84.122 0.435 3.03 4 3.0 0.0 418 9 5 -1 42.068 84.135 0.435 3.03 4 59.7 3.0 419 12 0 -2 42.131 84.263 0.435 3.03 2 78.8 2.6 420 1 7 3 42.22 84.44 0.436 3.02 4 22.3 0.4 421 4 4 -7 42.272 84.545 0.437 3.01 4 118.0 11.8 422 11 3 -2 42.296 84.593 0.437 3.01 4 34.5 1.0 423 1 3 -8 42.318 84.636 0.437 3.01 4 48.5 2.0 424 4 0 8 42.32 84.64 0.437 3.01 2 19.8 0.2 425 11 1 3 42.398 84.797 0.438 3.0 4 51.5 2.2 426 3 5 6 42.435 84.87 0.438 3.0 4 71.8 4.3 427 10 2 -5 42.469 84.938 0.438 3.0 4 43.3 1.6 428 11 3 1 42.503 85.006 0.439 2.99 4 20.2 0.3 429 2 6 5 42.533 85.066 0.439 2.99 4 11.0 0.1 430 9 5 1 42.744 85.488 0.441 2.97 4 60.6 3.1 431 10 2 4 42.75 85.5 0.441 2.97 4 1.0 0.0 432 9 5 -2 42.763 85.526 0.441 2.97 4 28.2 0.7 433 6 0 -8 42.843 85.686 0.441 2.97 2 202.8 17.1 434 6 2 7 42.9 85.801 0.442 2.96 4 44.2 1.6 435 1 3 8 42.919 85.838 0.442 2.96 4 14.7 0.2 436 6 6 3 42.968 85.935 0.442 2.96 4 58.5 2.8 437 7 5 4 42.979 85.957 0.443 2.96 4 67.1 3.7 438 5 3 7 43.001 86.002 0.443 2.95 4 14.6 0.2 439 7 3 6 43.02 86.04 0.443 2.95 4 57.7 2.8 440 3 3 -8 43.128 86.256 0.444 2.94 4 60.8 3.1 441 3 7 -3 43.18 86.36 0.444 2.94 4 7.1 0.0 442 10 4 -3 43.238 86.477 0.445 2.94 4 52.7 2.3 443 5 7 0 43.241 86.482 0.445 2.94 4 4.5 0.0 444 12 2 -1 43.391 86.783 0.446 2.93 4 54.8 2.5 445 10 4 2 43.394 86.788 0.446 2.92 4 24.4 0.5 446 5 7 -1 43.397 86.795 0.446 2.92 4 70.3 4.1 447 5 5 -6 43.454 86.907 0.446 2.92 4 28.5 0.7 448 12 2 0 43.498 86.995 0.447 2.92 4 62.0 3.1 449 4 6 -5 43.522 87.043 0.447 2.92 4 11.2 0.1 450 8 2 6 43.587 87.173 0.448 2.91 4 34.0 0.9 451 11 3 -3 43.604 87.208 0.448 2.91 4 97.8 7.8 452 7 5 -5 43.71 87.421 0.449 2.9 4 125.6 12.8 453 6 4 6 43.726 87.451 0.449 2.9 4 42.1 1.4 454 5 7 1 43.772 87.544 0.449 2.9 4 37.3 1.1 455 6 6 -4 43.799 87.598 0.449 2.9 4 43.0 1.5 456 3 7 3 43.855 87.71 0.45 2.89 4 19.3 0.3 457 12 0 2 43.932 87.865 0.45 2.89 2 211.9 18.2 458 11 3 2 43.947 87.894 0.45 2.89 4 57.7 2.7 459 12 2 -2 43.972 87.945 0.451 2.89 4 85.1 5.9 460 10 0 -6 44.036 88.072 0.451 2.88 2 116.0 5.4 461 7 1 7 44.072 88.143 0.451 2.88 4 95.4 7.3 462 7 3 -7 44.077 88.154 0.452 2.88 4 86.9 6.1 463 9 5 2 44.112 88.225 0.452 2.88 4 147.7 17.6 464 8 6 0 44.128 88.257 0.452 2.88 4 25.5 0.5 465 9 5 -3 44.144 88.288 0.452 2.88 4 74.4 4.5 466 8 2 -7 44.156 88.312 0.452 2.87 4 29.2 0.7 467 4 2 8 44.16 88.32 0.452 2.87 4 87.6 6.2 468 8 6 -1 44.172 88.344 0.452 2.87 4 35.2 1.0 469 5 7 -2 44.24 88.481 0.453 2.87 4 29.9 0.7 470 12 2 1 44.29 88.581 0.453 2.87 4 1.7 0.0 471 1 7 -4 44.364 88.729 0.454 2.86 4 52.0 2.2 472 4 4 7 44.372 88.745 0.454 2.86 4 52.9 2.2 473 1 1 -9 44.445 88.891 0.455 2.86 4 4.7 0.0 474 1 5 -7 44.558 89.116 0.455 2.85 4 57.2 2.6 475 11 1 -5 44.599 89.198 0.456 2.85 4 74.4 4.4 476 1 7 4 44.664 89.328 0.456 2.85 4 125.5 12.6 477 5 1 8 44.664 89.328 0.456 2.85 4 80.0 5.1 478 6 2 -8 44.681 89.363 0.456 2.84 4 11.2 0.1 479 8 6 1 44.771 89.542 0.457 2.84 4 65.3 3.4 480 8 6 -2 44.902 89.805 0.458 2.83 4 31.0 0.8 481 3 3 8 44.926 89.852 0.458 2.83 4 90.8 6.5 482 9 3 5 44.984 89.967 0.459 2.83 4 40.7 1.3 483 5 7 2 44.989 89.978 0.459 2.83 4 14.0 0.2 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 1 1 0 6.042 12.085 7.31762 309.9 52.4 52.9 5.6 2 2 0 0 6.36 12.72 6.95373 394.8 66.7 67.3 5.6 3 1 1 -1 7.361 14.723 6.01187 13.0 2.2 2.2 5.6 4 1 1 1 7.65 15.301 5.78605 190.6 32.2 32.4 5.6 5 0 0 2 8.904 17.808 4.97664 96.2 16.3 16.3 5.6 6 0 2 0 10.313 20.626 4.30255 24.7 4.2 4.2 5.6 7 2 0 -2 10.564 21.129 4.20133 81.3 13.7 13.8 5.6 8 3 1 0 10.879 21.758 4.08125 123.5 20.9 20.9 5.6 9 0 2 1 11.247 22.494 3.94935 214.4 36.2 36.3 5.6 10 2 0 2 11.366 22.732 3.90849 253.6 42.9 42.9 5.6 11 3 1 -1 11.486 22.972 3.86831 63.8 10.8 10.8 5.6 12 3 1 1 12.048 24.096 3.69023 19.0 3.2 3.2 5.6 13 2 2 0 12.153 24.307 3.65881 112.3 19.0 19.0 5.6 14 4 0 0 12.8 25.6 3.47686 591.6 100.0 100.0 5.6 15 3 1 -2 13.646 27.292 3.26499 151.7 25.6 25.6 5.6 16 0 2 2 13.689 27.379 3.2548 69.7 11.8 11.8 5.6 17 1 1 -3 14.539 29.079 3.06831 231.1 39.1 38.9 5.6 18 3 1 2 14.595 29.19 3.05683 7.4 1.3 1.2 5.6 19 2 2 -2 14.848 29.696 3.00594 62.0 10.5 10.5 5.6 20 1 1 3 14.995 29.99 2.97713 37.8 6.4 6.4 5.6 21 4 0 -2 15.094 30.189 2.95796 16.2 2.7 2.7 5.6 22 2 2 2 15.441 30.883 2.89303 76.2 12.9 12.8 5.6 23 1 3 0 15.914 31.828 2.80924 56.4 9.5 9.5 5.6 24 4 0 2 16.246 32.491 2.75338 149.6 25.3 25.1 5.6 25 1 3 -1 16.485 32.969 2.71456 107.3 18.1 18.0 5.6 26 1 3 1 16.622 33.243 2.6928 85.7 14.5 14.4 5.6 27 3 1 -3 16.811 33.622 2.66335 7.7 1.3 1.3 5.7 28 4 2 -1 16.9 33.8 2.64969 10.0 1.7 1.7 5.7 29 0 2 3 17.048 34.097 2.62734 37.6 6.4 6.3 5.7 30 5 1 -1 17.198 34.397 2.60512 120.4 20.4 20.2 5.7 31 4 2 1 17.431 34.862 2.57138 15.1 2.5 2.5 5.7 32 5 1 1 17.85 35.7 2.51293 41.3 7.0 6.9 5.7 33 2 2 -3 17.884 35.768 2.50831 8.6 1.5 1.4 5.7 34 3 1 3 17.991 35.983 2.49384 79.1 13.4 13.3 5.7 35 0 0 4 18.033 36.065 2.48832 13.1 2.2 2.2 5.7 36 3 3 0 18.409 36.817 2.43921 68.1 11.5 11.4 5.7 37 1 3 2 18.477 36.955 2.43043 51.7 8.7 8.7 5.7 38 5 1 -2 18.637 37.274 2.41033 26.8 4.5 4.5 5.7 39 2 0 -4 18.707 37.415 2.40161 26.6 4.5 4.5 5.7 40 3 3 1 19.156 38.311 2.34745 52.0 8.8 8.7 5.7 41 1 1 4 19.326 38.651 2.32757 53.5 9.1 8.9 5.7 42 6 0 0 19.409 38.819 2.31791 57.3 9.7 9.6 5.7 43 2 0 4 19.672 39.344 2.28818 100.6 17.0 16.8 5.7 44 3 3 -2 20.247 40.494 2.22582 11.5 1.9 1.9 5.7 45 3 1 -4 20.584 41.168 2.1909 121.2 20.5 20.2 5.7 46 6 0 -2 20.839 41.678 2.16528 12.1 2.0 2.0 5.7 47 1 3 -3 20.888 41.777 2.16039 285.8 48.3 47.6 5.7 48 3 3 2 20.929 41.858 2.15637 101.0 17.1 16.8 5.7 49 5 1 -3 21.033 42.065 2.14624 9.2 1.6 1.5 5.7 50 1 3 3 21.223 42.446 2.12784 10.4 1.8 1.7 5.7 51 4 0 -4 21.511 43.022 2.10067 85.1 14.4 14.2 5.7 52 3 1 4 21.914 43.828 2.06393 40.5 6.9 6.7 5.7 53 2 4 0 22.012 44.024 2.05517 21.7 3.7 3.6 5.7 54 6 2 0 22.177 44.354 2.04062 65.5 11.1 10.9 5.7 55 4 2 3 22.209 44.418 2.03785 10.3 1.7 1.7 5.7 56 6 2 -1 22.346 44.693 2.02596 13.7 2.3 2.3 5.7 57 2 4 -1 22.395 44.791 2.02175 157.8 26.7 26.2 5.7 58 2 4 1 22.607 45.214 2.0038 26.0 4.4 4.3 5.7 59 5 1 3 22.658 45.316 1.99952 84.5 14.3 14.0 5.7 60 5 3 0 22.691 45.381 1.99682 7.9 1.3 1.3 5.7 61 5 3 -1 22.909 45.818 1.97879 7.7 1.3 1.3 5.7 62 0 4 2 22.959 45.919 1.97468 117.9 19.9 19.6 5.7 63 4 0 4 23.213 46.427 1.95425 42.7 7.2 7.1 5.7 64 1 1 -5 23.386 46.771 1.94066 66.9 11.3 11.1 5.7 65 6 2 -2 23.469 46.938 1.93416 94.1 15.9 15.6 5.7 66 7 1 -1 23.558 47.116 1.92725 41.8 7.1 6.9 5.7 67 2 4 -2 23.72 47.44 1.91484 74.5 12.6 12.3 5.7 68 5 3 -2 24.061 48.123 1.88927 56.0 9.5 9.3 5.7 69 2 4 2 24.124 48.248 1.88465 6.9 1.2 1.1 5.7 70 5 1 -4 24.156 48.312 1.88229 9.4 1.6 1.6 5.7 71 1 3 -4 24.228 48.455 1.87708 63.6 10.8 10.5 5.7 72 7 1 1 24.265 48.53 1.87434 23.2 3.9 3.8 5.7 73 7 1 -2 24.589 49.177 1.8512 107.4 18.2 17.7 5.7 74 6 2 2 24.675 49.35 1.84512 28.8 4.9 4.8 5.7 75 3 1 -5 24.771 49.542 1.83842 42.1 7.1 7.0 5.7 76 4 4 -1 25.154 50.307 1.81223 39.7 6.7 6.6 5.8 77 0 2 5 25.237 50.473 1.80666 8.4 1.4 1.4 5.8 78 6 2 -3 25.448 50.895 1.79266 36.8 6.2 6.1 5.8 79 3 3 -4 25.674 51.349 1.77788 16.5 2.8 2.7 5.8 80 6 0 -4 25.885 51.769 1.76443 13.1 2.2 2.2 5.8 81 5 3 -3 26.054 52.108 1.75376 34.5 5.8 5.7 5.8 82 5 1 4 26.103 52.207 1.75066 78.7 13.3 13.0 5.8 83 4 4 -2 26.279 52.558 1.73981 45.1 7.6 7.4 5.8 84 3 3 4 26.807 53.614 1.70799 32.0 5.4 5.3 5.8 85 4 4 2 27.026 54.051 1.6952 31.4 5.3 5.2 5.8 86 6 2 3 27.144 54.288 1.68836 9.8 1.7 1.6 5.8 87 8 0 -2 27.263 54.526 1.68156 50.8 8.6 8.3 5.8 88 5 3 3 27.451 54.901 1.67095 50.0 8.4 8.2 5.8 89 0 0 6 27.667 55.335 1.65888 6.3 1.1 1.0 5.8 90 5 1 -5 27.841 55.681 1.64937 37.5 6.3 6.1 5.8 91 2 0 -6 27.975 55.95 1.64209 39.3 6.6 6.4 5.8 92 1 3 -5 28.086 56.172 1.63613 31.2 5.3 5.1 5.8 93 0 4 4 28.25 56.5 1.6274 6.0 1.0 1.0 5.8 94 7 1 3 28.381 56.763 1.62049 11.1 1.9 1.8 5.8 95 3 5 0 28.517 57.034 1.61342 60.4 10.2 9.9 5.8 96 1 5 2 28.566 57.133 1.61088 16.5 2.8 2.7 5.8 97 8 2 -1 28.6 57.2 1.60915 7.3 1.2 1.2 5.8 98 8 0 2 28.708 57.416 1.60358 44.2 7.5 7.2 5.8 99 5 3 -4 28.765 57.53 1.6007 31.2 5.3 5.1 5.8 100 2 0 6 29.046 58.092 1.58654 40.7 6.9 6.7 5.8 101 7 3 -2 29.148 58.297 1.58145 7.6 1.3 1.2 5.8 102 6 4 0 29.243 58.485 1.5768 36.9 6.2 6.0 5.8 103 8 2 1 29.307 58.613 1.57366 24.9 4.2 4.1 5.8 104 6 4 -1 29.381 58.763 1.57001 17.1 2.9 2.8 5.8 105 4 2 5 29.596 59.193 1.55962 18.5 3.1 3.0 5.8 106 6 4 1 29.904 59.808 1.54505 10.9 1.8 1.8 5.8 107 7 3 2 30.365 60.729 1.5238 20.6 3.5 3.4 5.8 108 9 1 -1 30.435 60.87 1.52062 14.3 2.4 2.3 5.8 109 3 3 5 30.608 61.217 1.51282 82.5 13.9 13.4 5.8 110 7 3 -3 30.828 61.655 1.50311 66.1 11.2 10.7 5.8 111 8 2 -3 31.087 62.174 1.49181 18.7 3.2 3.0 5.8 112 2 2 6 31.162 62.325 1.48857 7.3 1.2 1.2 5.8 113 6 4 2 31.334 62.669 1.48121 8.8 1.5 1.4 5.8 114 6 2 -5 31.475 62.95 1.47527 19.4 3.3 3.1 5.9 115 0 4 5 31.816 63.632 1.46109 8.5 1.4 1.4 5.9 116 5 5 -1 31.931 63.862 1.45638 15.7 2.7 2.5 5.9 117 4 0 6 31.972 63.943 1.45474 18.0 3.0 2.9 5.9 118 5 3 -5 32.089 64.177 1.45 7.9 1.3 1.3 5.9 119 4 4 4 32.175 64.35 1.44651 12.3 2.1 2.0 5.9 120 7 1 -5 32.278 64.557 1.44238 16.7 2.8 2.7 5.9 121 5 5 1 32.347 64.693 1.43967 10.3 1.7 1.7 5.9 122 1 3 -6 32.385 64.77 1.43815 24.5 4.1 4.0 5.9 123 3 5 3 32.438 64.876 1.43605 11.4 1.9 1.8 5.9 124 0 6 0 32.486 64.971 1.43418 11.1 1.9 1.8 5.9 125 7 3 3 32.586 65.172 1.43025 6.7 1.1 1.1 5.9 126 9 1 2 32.722 65.443 1.42497 9.4 1.6 1.5 5.9 127 9 1 -3 32.756 65.513 1.42363 6.5 1.1 1.1 5.9 128 1 3 6 32.879 65.759 1.41889 25.9 4.4 4.2 5.9 129 1 5 -4 32.998 65.996 1.41437 6.5 1.1 1.1 5.9 130 7 3 -4 33.209 66.418 1.40641 10.4 1.8 1.7 5.9 131 2 6 0 33.257 66.513 1.40462 16.3 2.8 2.6 5.9 132 1 5 4 33.325 66.65 1.40207 12.4 2.1 2.0 5.9 133 6 0 -6 33.369 66.738 1.40044 11.7 2.0 1.9 5.9 134 6 4 3 33.479 66.958 1.39636 6.4 1.1 1.0 5.9 135 5 5 2 33.678 67.356 1.38908 23.1 3.9 3.7 5.9 136 1 1 7 33.779 67.557 1.38543 6.9 1.2 1.1 5.9 137 4 2 6 33.983 67.966 1.3781 8.3 1.4 1.3 5.9 138 8 0 4 34.022 68.045 1.37669 7.7 1.3 1.2 5.9 139 3 5 -4 34.199 68.397 1.37045 13.9 2.4 2.2 5.9 140 8 4 -1 34.774 69.549 1.35054 20.6 3.5 3.3 5.9 141 7 1 5 35.117 70.235 1.33903 8.5 1.4 1.4 5.9 142 9 3 -2 35.231 70.463 1.33525 16.5 2.8 2.6 5.9 143 7 3 4 35.459 70.919 1.32778 19.9 3.4 3.2 5.9 144 10 2 0 35.597 71.194 1.32333 8.5 1.4 1.4 5.9 145 4 6 -1 35.724 71.448 1.31924 41.0 6.9 6.5 5.9 146 3 1 7 35.838 71.676 1.3156 6.5 1.1 1.0 5.9 147 10 0 2 35.897 71.794 1.31373 10.2 1.7 1.6 5.9 148 5 3 -6 35.959 71.919 1.31176 9.2 1.6 1.5 5.9 149 6 0 6 36.245 72.489 1.30283 7.8 1.3 1.2 5.9 150 1 5 5 36.654 73.308 1.2903 76.9 13.0 12.2 6.0 151 9 1 4 37.81 75.621 1.25647 10.5 1.8 1.7 6.0 152 9 1 -5 37.869 75.738 1.25481 15.7 2.7 2.5 6.0 153 7 5 2 38.277 76.554 1.24346 20.0 3.4 3.2 6.0 154 7 5 -3 38.694 77.387 1.23214 12.6 2.1 2.0 6.0 155 2 6 -4 38.724 77.447 1.23133 8.8 1.5 1.4 6.0 156 11 1 1 38.785 77.569 1.2297 38.1 6.4 6.0 6.0 157 6 6 0 39.167 78.334 1.2196 19.9 3.4 3.1 6.0 158 2 6 4 39.336 78.672 1.21521 17.0 2.9 2.7 6.0 159 2 0 8 39.584 79.167 1.20885 12.6 2.1 2.0 6.0 160 10 2 -4 39.728 79.457 1.20516 7.5 1.3 1.2 6.0 161 8 2 -6 39.968 79.937 1.19913 7.9 1.3 1.2 6.0 162 0 2 8 40.127 80.254 1.19519 12.3 2.1 1.9 6.0 163 5 3 -7 40.362 80.725 1.1894 12.6 2.1 2.0 6.1 164 0 4 7 40.494 80.987 1.18621 10.2 1.7 1.6 6.1 165 7 5 -4 40.87 81.74 1.17717 6.4 1.1 1.0 6.1 166 10 0 4 40.902 81.804 1.17642 9.8 1.6 1.5 6.1 167 3 7 -2 41.57 83.14 1.16088 7.7 1.3 1.2 6.1 168 8 4 4 41.627 83.254 1.15958 13.5 2.3 2.1 6.1 169 11 3 0 41.744 83.488 1.15691 40.7 6.9 6.3 6.1 170 1 7 -3 41.994 83.989 1.15129 16.3 2.8 2.5 6.1 171 4 4 -7 42.272 84.545 1.14513 12.8 2.2 2.0 6.1 172 6 0 -8 42.843 85.686 1.13278 17.1 2.9 2.6 6.1 173 7 5 4 42.979 85.957 1.1299 6.6 1.1 1.0 6.1 174 5 7 -1 43.397 86.795 1.12114 7.0 1.2 1.1 6.1 175 11 3 -3 43.604 87.208 1.11688 7.8 1.3 1.2 6.2 176 7 5 -5 43.71 87.421 1.11471 14.3 2.4 2.2 6.2 177 12 0 2 43.932 87.865 1.11022 20.9 3.5 3.2 6.2 178 7 1 7 44.072 88.143 1.10743 13.4 2.3 2.1 6.2 179 9 5 2 44.112 88.225 1.10661 18.1 3.1 2.8 6.2 180 4 2 8 44.16 88.32 1.10567 12.3 2.1 1.9 6.2 181 1 7 4 44.664 89.328 1.09579 17.8 3.0 2.7 6.2 182 3 3 8 44.926 89.852 1.09075 6.5 1.1 1.0 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |