Institute of Experimental Mineralogy Russian Academy of Sciences ------------------------------------------------- 142432, Chernogolovka, Moscow district A.V. Chichagov +7(496)52-22320 *** *** W W W - X R A Y P O L *** *********************** CHENITE 1 Pb(4)CU(OH)(6)[SO(4)](2) Triclinic P 1(-) Z = 1 R =0.094 NR =1735 27 .1 .1995 Ref.Str.: Hess H., Keller P., Riffel H. (1988) * Neues Jb. Miner., Mh., H.6, 259-264 Reserv: N.A.D. Initial data from BDM-file Lattice parameters (cub. angs.,degr.): a = 5.791 alpha = 112.02 b = 7.94 beta = 97.73 c = 7.976 gamma = 100.45 Unit cell volume (cub. angs.) = 326.0 Molar volume ( cub.cm/mol.) = 196.36 Co-ordinates, thermal parameters, occupation for atomic positions: NoP x/a y/b z/c B(j) atom / occupation 1 0.3715 0.2541 0.4865 0.03 Pb = 1.00 2 0.5602 0.2717 0.0472 0.03 Pb = 1.00 3 0.0 0.0 0.0 0.02 Cu = 1.00 4 0.0601 0.739 0.276 0.02 S = 1.00 5 0.212 0.236 0.187 0.02 O = 1.00 6 0.277 0.95 0.873 0.03 O = 1.00 7 0.32 0.559 0.596 0.03 O = 1.00 8 0.198 0.316 0.814 0.03 O = 1.00 9 0.162 0.588 0.22 0.03 O = 1.00 10 0.089 0.818 0.481 0.03 O = 1.00 11 0.185 0.887 0.225 0.03 O = 1.00 Co-ordinates for all atomic positions : No NoP x/a y/b z/c 1 1 0.3715 0.2541 0.4865 2 2 0.5602 0.2717 0.0472 3 3 0.0 0.0 0.0 4 4 0.0601 0.739 0.276 5 5 0.212 0.236 0.187 6 6 0.277 0.95 0.873 7 7 0.32 0.559 0.596 8 8 0.198 0.316 0.814 9 9 0.162 0.588 0.22 10 10 0.089 0.818 0.481 11 11 0.185 0.887 0.225 12 1 0.6285 0.7459 0.5135 13 2 0.4398 0.7283 0.9528 14 4 0.9399 0.261 0.724 15 5 0.788 0.764 0.813 16 6 0.723 0.05 0.127 17 7 0.68 0.441 0.404 18 8 0.802 0.684 0.186 19 9 0.838 0.412 0.78 20 10 0.911 0.182 0.519 21 11 0.815 0.113 0.775 X-ray density (g/cm cub.) = 6.01 MU (1/cm) = 1038.44 Mass attenuation coefficient (cm**2/g) = 172.758 Selected interatomic distances (cation-anion,anion-anion): NoP Atom Rad.sph. C.N. Distance NoP N. (angs.) (angs.) 1 Pb 3.144 7 2.3835 5 2.3365 7 2.8279 8 2.776 11 2.4318 7 3.0363 9 2.6926 10 2 Pb 3.144 7 2.4544 5 2.5201 6 2.7734 8 2.3819 6 2.5786 7 3.0176 8 2.822 11 3 Cu 2.808 6 1.9545 5 2.0306 6 2.4924 11 1.9545 5 2.0306 6 2.4924 11 4 S 1.98 4 1.3825 9 1.488 10 1.4828 11 1.4763 8 5 O 3.264 7 2.8053 6 3.1947 7 3.2606 8 2.7797 9 2.8776 11 2.8315 6 2.8312 7 6 O 3.264 7 2.8053 5 3.1411 7 3.2134 8 2.8762 10 3.1265 11 2.8315 5 2.8369 6 7 O 3.264 8 3.1947 5 3.1411 6 3.0979 8 3.1209 9 2.9903 10 2.8312 5 2.8391 7 3.2566 10 8 O 3.264 7 3.2606 5 3.2134 6 3.0979 7 3.2085 9 2.3622 9 2.4207 10 2.3991 11 9 O 3.264 6 2.7797 5 3.1209 7 3.2085 8 2.3481 10 2.3385 11 2.3622 8 10 O 3.264 7 2.8762 6 2.9903 7 2.3481 9 2.4108 11 3.2566 7 2.4207 8 3.1647 10 11 O 3.264 5 2.8776 5 3.1265 6 2.3385 9 2.4108 10 2.3991 8 X-ray diffraction powder data (II), X-Ray W.L. = 1.54056(angs.): No H K L Theta 2*Theta S LPG MF F I int. ( degree ) *100 1 0 0 1 6.133 12.267 0.069 172.23 2 15.3 75.8 2 0 1 0 6.208 12.417 0.07 168.04 2 0.3 0.0 3 0 -1 1 6.707 13.414 0.076 143.65 2 38.2 393.7 4 1 0 0 7.974 15.948 0.09 100.98 2 159.5 4832.9 5 -1 1 0 8.793 17.586 0.099 82.65 2 86.2 1155.9 6 -1 0 1 8.926 17.852 0.101 80.14 2 1.4 0.3 7 1 -1 1 10.288 20.577 0.116 59.79 2 196.7 4355.3 8 0 1 1 10.399 20.798 0.117 58.48 2 7.4 6.0 9 -1 -1 1 10.605 21.211 0.119 56.14 2 85.2 766.2 10 1 0 1 11.127 22.254 0.125 50.8 2 22.5 48.2 11 -1 1 1 11.191 22.383 0.126 50.2 2 20.2 38.5 12 0 -1 2 11.303 22.607 0.127 49.17 2 72.9 491.2 13 1 1 0 11.317 22.635 0.127 49.04 2 12.3 14.0 14 0 -2 1 11.428 22.856 0.129 48.05 2 42.3 161.4 15 0 0 2 12.338 24.677 0.139 40.93 2 226.4 3947.6 16 0 2 0 12.491 24.983 0.14 39.88 2 277.0 5759.6 17 1 -2 1 12.914 25.827 0.145 37.19 2 100.3 704.6 18 -1 2 0 13.037 26.073 0.146 36.45 2 200.7 2763.0 19 -1 0 2 13.147 26.295 0.148 35.8 2 250.4 4223.3 20 -1 -1 2 13.19 26.379 0.148 35.56 2 63.5 269.9 21 0 -2 2 13.509 27.017 0.152 33.81 2 187.4 2234.4 22 1 -1 2 14.567 29.134 0.163 28.79 2 72.5 284.7 23 1 1 1 14.884 29.768 0.167 27.5 2 229.5 2725.0 24 -1 -2 1 15.008 30.017 0.168 27.01 2 54.0 148.1 25 1 -2 2 15.546 31.093 0.174 25.05 2 210.4 2086.2 26 -2 1 0 15.733 31.467 0.176 24.41 2 54.1 134.4 27 -1 2 1 15.856 31.713 0.177 24.0 2 35.9 58.4 28 -1 1 2 15.872 31.745 0.178 23.95 2 133.5 803.8 29 -2 0 1 15.918 31.837 0.178 23.8 2 161.1 1161.8 30 -1 -2 2 15.979 31.958 0.179 23.61 2 278.2 3438.0 31 0 1 2 16.035 32.069 0.179 23.43 2 45.8 92.6 32 2 0 0 16.108 32.216 0.18 23.2 2 84.3 310.3 33 0 2 1 16.125 32.25 0.18 23.15 2 37.8 62.2 34 1 0 2 16.226 32.451 0.181 22.84 2 154.3 1022.7 35 1 2 0 16.553 33.106 0.185 21.87 2 200.0 1645.9 36 -2 1 1 16.561 33.122 0.185 21.85 2 209.7 1808.3 37 0 -1 3 17.056 34.111 0.19 20.49 2 172.9 1152.6 38 0 -3 1 17.283 34.567 0.193 19.91 2 46.2 79.9 39 2 -1 1 17.321 34.643 0.193 19.82 2 241.7 2179.2 40 1 -3 1 17.595 35.191 0.196 19.15 2 185.3 1236.7 41 -2 -1 1 17.715 35.43 0.198 18.87 2 222.1 1750.8 42 0 -2 3 17.726 35.453 0.198 18.84 2 35.8 45.5 43 -1 -1 3 17.764 35.528 0.198 18.75 2 72.7 186.6 44 -2 2 0 17.802 35.604 0.198 18.66 2 112.8 446.9 45 0 -3 2 17.864 35.728 0.199 18.52 2 6.9 1.7 46 -2 0 2 18.079 36.157 0.201 18.04 2 172.1 1005.7 47 2 -2 1 18.35 36.701 0.204 17.46 2 68.6 154.8 48 2 0 1 18.583 37.167 0.207 16.98 2 44.6 63.5 49 -1 3 0 18.605 37.21 0.207 16.94 2 122.6 479.6 50 -1 0 3 18.647 37.294 0.208 16.86 2 28.8 26.4 51 0 0 3 18.695 37.39 0.208 16.76 2 57.0 102.4 52 1 -3 2 18.795 37.59 0.209 16.57 2 3.4 0.4 53 2 1 0 18.796 37.592 0.209 16.56 2 69.4 150.1 54 -2 -1 2 18.832 37.664 0.21 16.49 2 126.2 494.0 55 0 3 0 18.932 37.863 0.211 16.3 2 82.0 206.3 56 -1 -2 3 19.124 38.249 0.213 15.94 2 3.2 0.3 57 -2 2 1 19.43 38.86 0.216 15.39 2 82.3 196.3 58 -2 1 2 19.533 39.066 0.217 15.21 2 81.3 189.1 59 1 1 2 19.938 39.876 0.221 14.54 2 52.0 73.9 60 1 -2 3 19.962 39.925 0.222 14.5 2 56.8 88.1 61 1 -1 3 20.042 40.084 0.222 14.37 2 195.4 1032.0 62 1 2 1 20.101 40.201 0.223 14.28 2 39.2 41.3 63 -1 2 2 20.378 40.757 0.226 13.85 2 246.6 1585.1 64 0 -3 3 20.511 41.022 0.227 13.65 2 58.1 86.6 65 -1 -3 2 20.522 41.043 0.228 13.63 2 9.4 2.3 66 -1 -3 1 20.587 41.173 0.228 13.53 2 105.4 282.7 67 2 -1 2 20.842 41.684 0.231 13.17 2 27.5 18.8 68 2 -2 2 20.928 41.857 0.232 13.05 2 28.9 20.5 69 0 2 2 21.162 42.324 0.234 12.73 2 178.8 765.9 70 2 -3 1 21.387 42.774 0.237 12.43 2 160.2 600.2 71 -2 -2 1 21.418 42.836 0.237 12.39 2 69.0 111.1 72 -1 1 3 21.537 43.074 0.238 12.23 2 3.8 0.3 73 -1 3 1 21.559 43.119 0.239 12.21 2 45.8 48.1 74 -2 -2 2 21.598 43.195 0.239 12.16 2 108.7 270.3 75 -2 3 0 21.708 43.416 0.24 12.02 2 101.5 232.9 76 2 1 1 21.796 43.592 0.241 11.91 2 221.3 1097.9 77 -2 -1 3 21.86 43.72 0.242 11.83 2 89.1 176.7 78 1 -3 3 21.895 43.789 0.242 11.79 2 243.8 1318.6 79 -2 0 3 21.99 43.98 0.243 11.67 2 134.2 395.6 80 1 0 3 22.116 44.232 0.244 11.53 2 72.8 114.9 81 0 1 3 22.207 44.413 0.245 11.42 2 149.6 480.7 82 -1 -3 3 22.38 44.761 0.247 11.22 2 45.4 43.4 83 0 3 1 22.389 44.779 0.247 11.21 2 112.9 269.1 84 1 3 0 22.562 45.125 0.249 11.02 2 49.4 50.7 85 2 0 2 22.704 45.408 0.251 10.86 2 38.8 30.7 86 -2 2 2 22.841 45.681 0.252 10.72 2 93.7 177.2 87 2 -3 2 22.946 45.891 0.253 10.61 2 44.5 39.6 88 0 -2 4 23.08 46.159 0.254 10.47 2 193.0 734.1 89 2 2 0 23.109 46.218 0.255 10.44 2 49.2 47.6 90 1 -4 1 23.28 46.561 0.257 10.26 2 52.8 53.9 91 0 -1 4 23.301 46.601 0.257 10.24 2 78.9 120.0 92 -1 -1 4 23.338 46.676 0.257 10.21 2 104.5 209.8 93 0 -4 2 23.345 46.691 0.257 10.2 2 256.6 1264.1 94 1 -4 2 23.512 47.025 0.259 10.04 2 159.8 482.4 95 -2 -2 3 23.614 47.228 0.26 9.94 2 72.6 98.6 96 0 -4 1 23.63 47.26 0.26 9.92 2 10.2 2.0 97 -1 -2 4 23.712 47.424 0.261 9.85 2 223.7 927.1 98 -3 1 0 23.748 47.496 0.261 9.81 2 36.8 25.1 99 -3 1 1 23.836 47.671 0.262 9.73 2 127.0 295.6 100 -2 3 1 23.848 47.695 0.262 9.72 2 148.4 403.0 101 -3 0 1 23.955 47.911 0.264 9.62 2 131.6 313.8 102 -2 1 3 23.98 47.959 0.264 9.6 2 102.2 188.6 103 3 0 0 24.593 49.186 0.27 9.06 2 50.1 42.9 104 0 -3 4 24.674 49.348 0.271 8.99 2 2.5 0.1 105 -3 2 0 24.695 49.39 0.271 8.98 2 18.9 6.0 106 -1 0 4 24.771 49.542 0.272 8.92 2 135.4 307.7 107 -1 4 0 24.811 49.622 0.272 8.88 2 144.1 346.9 108 0 -4 3 24.822 49.644 0.272 8.87 2 35.6 21.2 109 1 2 2 24.946 49.891 0.274 8.77 2 138.7 317.6 110 2 -2 3 25.022 50.044 0.275 8.71 2 61.2 61.4 111 -3 0 2 25.056 50.111 0.275 8.69 2 10.8 1.9 112 0 0 4 25.301 50.602 0.277 8.5 2 196.9 619.6 113 3 -1 1 25.392 50.784 0.278 8.43 2 131.5 274.4 114 1 -2 4 25.409 50.818 0.279 8.41 2 78.3 97.1 115 1 -4 3 25.471 50.941 0.279 8.37 2 3.7 0.2 116 -3 2 1 25.486 50.972 0.279 8.36 2 214.7 725.1 117 3 -2 1 25.606 51.212 0.281 8.27 2 182.5 518.1 118 0 4 0 25.632 51.263 0.281 8.25 2 251.7 983.6 119 -3 1 2 25.642 51.284 0.281 8.24 2 74.9 87.1 120 2 -1 3 25.649 51.298 0.281 8.24 2 252.5 987.9 121 1 1 3 25.799 51.598 0.283 8.13 2 227.7 793.0 122 -3 -1 1 25.827 51.654 0.283 8.11 2 210.3 674.5 123 -1 -3 4 25.834 51.668 0.283 8.1 2 128.4 251.3 124 -2 -3 2 25.854 51.708 0.283 8.09 2 42.4 27.3 125 2 -4 1 25.859 51.719 0.283 8.08 2 143.0 311.0 126 -1 2 3 25.892 51.784 0.283 8.06 2 15.3 3.6 127 -1 3 2 25.922 51.845 0.284 8.04 2 127.7 246.7 128 -1 -4 2 26.089 52.178 0.285 7.92 2 211.6 667.4 129 1 3 1 26.106 52.212 0.286 7.91 2 145.4 314.6 130 2 -3 3 26.12 52.24 0.286 7.9 2 197.3 578.6 131 1 -1 4 26.167 52.334 0.286 7.87 2 6.8 0.7 132 2 1 2 26.187 52.375 0.286 7.85 2 1.4 0.0 133 -3 -1 2 26.192 52.384 0.287 7.85 2 7.7 0.9 134 -2 -1 4 26.271 52.541 0.287 7.8 2 186.8 512.1 135 1 -3 4 26.359 52.719 0.288 7.74 2 26.5 10.2 136 -2 -3 1 26.386 52.771 0.288 7.72 2 245.1 872.7 137 2 2 1 26.39 52.781 0.289 7.72 2 9.2 1.2 138 2 -4 2 26.549 53.098 0.29 7.61 2 48.7 33.9 139 -2 4 0 26.817 53.635 0.293 7.44 2 135.8 258.3 140 -1 -4 1 26.823 53.645 0.293 7.44 2 29.7 12.3 141 3 0 1 26.876 53.753 0.293 7.4 2 119.9 200.4 142 -2 -3 3 26.969 53.938 0.294 7.35 2 126.4 220.8 143 -1 -4 3 26.993 53.986 0.295 7.33 2 31.4 13.6 144 0 2 3 27.016 54.033 0.295 7.32 2 99.3 135.7 145 -2 0 4 27.059 54.119 0.295 7.29 2 169.8 395.5 146 3 1 0 27.106 54.212 0.296 7.26 2 82.3 92.5 147 0 3 2 27.116 54.231 0.296 7.26 2 109.3 163.0 148 -2 -2 4 27.152 54.304 0.296 7.23 2 140.5 268.6 149 -3 3 0 27.297 54.593 0.298 7.15 2 63.9 55.0 150 -2 3 2 27.482 54.963 0.3 7.04 2 165.3 362.0 151 3 -3 1 27.49 54.98 0.3 7.03 2 200.1 530.1 152 -2 2 3 27.522 55.044 0.3 7.01 2 55.3 40.3 153 -3 0 3 27.741 55.483 0.302 6.89 2 132.8 228.6 154 -1 1 4 27.803 55.606 0.303 6.85 2 149.7 289.3 155 0 -4 4 27.851 55.703 0.303 6.83 2 220.2 623.2 156 -3 2 2 27.874 55.748 0.303 6.81 2 59.1 44.8 157 -1 4 1 27.889 55.778 0.304 6.81 2 14.5 2.7 158 2 0 3 27.918 55.837 0.304 6.79 2 82.1 86.1 159 3 -2 2 28.099 56.198 0.306 6.69 2 82.1 84.8 160 -3 -1 3 28.157 56.313 0.306 6.66 2 154.3 298.5 161 2 3 0 28.499 56.998 0.31 6.48 2 2.4 0.1 162 1 0 4 28.537 57.075 0.31 6.46 2 4.6 0.3 163 3 -1 2 28.55 57.099 0.31 6.45 2 26.5 8.5 164 -3 3 1 28.684 57.369 0.312 6.39 2 125.4 189.0 165 2 -4 3 28.804 57.607 0.313 6.33 2 113.2 152.6 166 0 1 4 28.809 57.618 0.313 6.32 2 48.8 28.3 167 1 -4 4 28.9 57.799 0.314 6.28 2 68.7 55.8 168 -3 -2 2 28.908 57.816 0.314 6.28 2 66.8 52.7 169 -3 1 3 28.934 57.868 0.314 6.26 2 78.1 71.9 170 0 4 1 29.093 58.187 0.316 6.19 2 7.9 0.7 171 1 4 0 29.109 58.218 0.316 6.18 2 130.7 198.7 172 0 -2 5 29.164 58.328 0.316 6.15 2 80.8 75.6 173 1 -5 2 29.193 58.387 0.317 6.14 2 100.8 117.4 174 -3 -2 1 29.208 58.416 0.317 6.13 2 118.6 162.4 175 3 -3 2 29.244 58.488 0.317 6.11 2 47.8 26.3 176 -1 -2 5 29.262 58.525 0.317 6.11 2 2.8 0.1 177 -2 4 1 29.311 58.622 0.318 6.08 2 141.9 230.4 178 -2 1 4 29.426 58.853 0.319 6.03 2 158.6 285.2 179 -1 -4 4 29.431 58.862 0.319 6.03 2 190.7 412.6 180 0 -5 2 29.558 59.116 0.32 5.97 2 6.3 0.4 181 -1 -1 5 29.576 59.153 0.32 5.96 2 56.7 36.0 182 -2 -3 4 29.601 59.202 0.321 5.95 2 63.4 45.0 183 1 -5 1 29.63 59.26 0.321 5.94 2 98.1 107.5 184 3 1 1 29.884 59.767 0.323 5.82 2 198.7 432.6 185 0 -3 5 29.907 59.814 0.324 5.81 2 127.8 178.8 186 0 -1 5 29.982 59.965 0.324 5.78 2 135.0 198.3 187 -3 -2 3 30.136 60.273 0.326 5.72 2 175.6 331.7 188 2 -2 4 30.201 60.401 0.327 5.69 2 85.5 78.2 189 0 -5 3 30.203 60.407 0.327 5.69 2 102.6 112.6 190 1 -5 3 30.278 60.557 0.327 5.66 2 141.9 214.4 191 0 -5 1 30.425 60.851 0.329 5.59 2 2.7 0.1 192 -1 -3 5 30.503 61.005 0.329 5.56 2 100.7 106.3 193 3 0 2 30.55 61.101 0.33 5.54 2 150.2 235.2 194 2 -3 4 30.559 61.118 0.33 5.54 2 1.9 0.0 195 1 2 3 30.689 61.377 0.331 5.49 2 37.9 14.8 196 3 -4 1 30.837 61.674 0.333 5.43 2 158.7 257.3 197 1 3 2 30.844 61.689 0.333 5.43 2 0.6 0.0 198 2 2 2 30.913 61.826 0.333 5.4 2 59.9 36.4 199 3 2 0 31.009 62.018 0.334 5.36 2 38.8 15.2 200 -2 -4 2 31.193 62.386 0.336 5.29 2 101.3 102.2 201 -3 4 0 31.272 62.544 0.337 5.26 2 40.5 16.3 202 -1 3 3 31.307 62.613 0.337 5.25 2 38.1 14.4 203 2 -5 1 31.364 62.727 0.338 5.23 2 128.2 161.7 204 2 -5 2 31.368 62.736 0.338 5.23 2 4.9 0.2 205 2 -1 4 31.369 62.738 0.338 5.23 2 2.4 0.1 206 -1 0 5 31.417 62.833 0.338 5.21 2 80.8 64.0 207 -3 3 2 31.518 63.036 0.339 5.17 2 56.0 30.5 208 -3 -1 4 31.523 63.045 0.339 5.17 2 56.0 30.5 209 -1 5 0 31.55 63.099 0.34 5.16 2 123.3 147.8 210 -2 -4 3 31.581 63.162 0.34 5.15 2 110.0 117.3 211 2 1 3 31.594 63.188 0.34 5.15 2 185.1 331.8 212 1 -2 5 31.596 63.191 0.34 5.15 2 2.8 0.1 213 -3 2 3 31.618 63.237 0.34 5.14 2 200.5 388.7 214 -2 -1 5 31.693 63.385 0.341 5.11 2 34.8 11.6 215 -3 0 4 31.745 63.491 0.342 5.09 2 41.7 16.6 216 1 -3 5 31.824 63.647 0.342 5.07 2 215.9 444.4 217 3 -4 2 31.876 63.753 0.343 5.05 2 93.5 83.0 218 -2 -2 5 31.877 63.754 0.343 5.05 2 11.8 1.3 219 3 -2 3 31.931 63.862 0.343 5.03 2 69.3 45.5 220 2 3 1 31.99 63.98 0.344 5.01 2 228.8 493.6 221 -1 2 4 32.136 64.272 0.345 4.96 2 150.1 210.3 222 0 -4 5 32.147 64.293 0.345 4.96 2 23.9 5.3 223 -4 1 1 32.194 64.388 0.346 4.94 2 112.7 118.0 224 -1 4 2 32.224 64.448 0.346 4.93 2 143.3 190.6 225 -2 -4 1 32.269 64.538 0.347 4.92 2 63.3 37.1 226 -2 3 3 32.283 64.566 0.347 4.91 2 16.3 2.4 227 1 1 4 32.29 64.58 0.347 4.91 2 50.7 23.7 228 0 0 5 32.291 64.581 0.347 4.91 2 60.9 34.2 229 0 -5 4 32.307 64.614 0.347 4.9 2 4.4 0.2 230 3 -3 3 32.398 64.797 0.348 4.87 2 158.8 231.4 231 -1 -5 2 32.411 64.822 0.348 4.87 2 38.0 13.3 232 2 -4 4 32.415 64.829 0.348 4.87 2 10.0 0.9 233 -4 1 0 32.539 65.079 0.349 4.83 2 113.0 116.1 234 -1 -5 3 32.61 65.219 0.35 4.81 2 87.1 68.6 235 0 5 0 32.733 65.467 0.351 4.77 2 62.2 34.7 236 1 4 1 32.743 65.485 0.351 4.76 2 69.0 42.7 237 -4 0 1 32.771 65.541 0.351 4.76 2 172.4 265.9 238 0 3 3 32.786 65.572 0.351 4.75 2 133.1 158.3 239 -3 -2 4 32.789 65.579 0.352 4.75 2 62.1 34.5 240 1 -5 4 32.795 65.589 0.352 4.75 2 48.9 21.4 241 -2 5 0 32.813 65.626 0.352 4.74 2 76.1 51.7 242 2 -5 3 32.825 65.651 0.352 4.74 2 188.7 317.6 243 -4 2 0 32.842 65.684 0.352 4.73 2 94.5 79.5 244 1 -1 5 32.855 65.711 0.352 4.73 2 194.5 336.6 245 3 -1 3 32.946 65.891 0.353 4.7 2 132.3 154.9 246 -3 -3 2 32.956 65.912 0.353 4.7 2 46.6 19.2 247 -2 0 5 32.993 65.986 0.353 4.69 2 49.4 21.5 248 -4 2 1 33.094 66.188 0.354 4.66 2 176.9 274.1 249 -2 4 2 33.124 66.249 0.355 4.65 2 108.9 103.7 250 -3 4 1 33.149 66.298 0.355 4.64 2 151.1 199.4 251 -2 2 4 33.161 66.322 0.355 4.64 2 108.7 103.0 252 -1 -4 5 33.194 66.387 0.355 4.63 2 3.4 0.1 253 -4 0 2 33.266 66.533 0.356 4.61 2 35.6 11.0 254 -4 1 2 33.288 66.576 0.356 4.6 2 79.4 54.6 255 -2 -4 4 33.406 66.812 0.357 4.56 2 170.9 250.8 256 -3 1 4 33.441 66.882 0.358 4.55 2 125.8 135.7 257 -3 -3 3 33.513 67.026 0.358 4.53 2 148.1 187.0 258 1 -4 5 33.523 67.045 0.358 4.53 2 26.8 6.1 259 -2 -3 5 33.532 67.065 0.359 4.53 2 115.4 113.5 260 0 2 4 33.534 67.069 0.359 4.53 2 117.1 116.9 261 -1 -5 1 33.645 67.291 0.36 4.5 2 136.9 158.6 262 4 0 0 33.703 67.406 0.36 4.48 2 77.2 50.3 263 0 4 2 33.743 67.487 0.361 4.47 2 150.0 189.3 264 -3 -3 1 33.824 67.648 0.361 4.45 2 123.0 126.6 265 3 1 2 33.939 67.878 0.362 4.42 2 35.9 10.7 266 2 0 4 33.975 67.951 0.363 4.41 2 36.2 10.9 267 4 -2 1 34.014 68.029 0.363 4.39 2 61.0 30.7 268 3 2 1 34.174 68.348 0.365 4.35 2 91.5 68.6 269 -1 -5 4 34.229 68.457 0.365 4.34 2 57.2 26.7 270 4 -1 1 34.302 68.604 0.366 4.32 2 120.8 118.6 271 3 -4 3 34.316 68.633 0.366 4.32 2 88.8 64.1 272 -4 3 0 34.591 69.183 0.369 4.24 2 55.4 24.5 273 -1 1 5 34.645 69.29 0.369 4.23 2 109.6 95.6 274 -4 -1 2 34.691 69.382 0.369 4.22 2 83.8 55.8 275 2 4 0 34.736 69.473 0.37 4.21 2 56.9 25.6 276 -4 2 2 34.755 69.51 0.37 4.2 2 44.6 15.7 277 -4 -1 1 34.786 69.573 0.37 4.2 2 84.2 55.9 278 -1 5 1 34.815 69.63 0.371 4.19 2 15.6 1.9 279 -4 0 3 35.161 70.321 0.374 4.11 2 189.8 278.5 280 4 -3 1 35.162 70.324 0.374 4.11 2 64.3 32.0 281 3 0 3 35.377 70.755 0.376 4.06 2 5.8 0.3 282 -4 3 1 35.414 70.827 0.376 4.05 2 38.3 11.2 283 3 -5 1 35.416 70.832 0.376 4.05 2 100.8 77.3 284 -3 -3 4 35.462 70.924 0.377 4.04 2 61.9 29.1 285 1 0 5 35.52 71.041 0.377 4.02 2 54.5 22.5 286 -1 -2 6 35.607 71.214 0.378 4.0 2 189.9 271.7 287 -3 3 3 35.609 71.218 0.378 4.0 2 83.0 51.9 288 -2 5 1 35.623 71.246 0.378 4.0 2 123.6 114.9 289 2 -5 4 35.643 71.286 0.378 4.0 2 31.1 7.3 290 1 -6 2 35.671 71.343 0.379 3.99 2 188.1 265.7 291 -2 1 5 35.694 71.388 0.379 3.99 2 63.8 30.5 292 0 -5 5 35.731 71.461 0.379 3.98 2 129.5 125.6 293 -4 1 3 35.756 71.512 0.379 3.97 2 88.4 58.4 294 3 -5 2 35.819 71.637 0.38 3.96 2 8.9 0.6 295 0 -2 6 35.916 71.832 0.381 3.94 2 82.3 50.2 296 0 1 5 35.936 71.872 0.381 3.93 2 116.3 100.1 297 -4 -1 3 35.982 71.965 0.381 3.92 2 71.3 37.5 298 4 0 1 36.01 72.02 0.382 3.92 2 104.6 80.7 299 0 -3 6 36.016 72.032 0.382 3.92 2 54.0 21.5 300 2 -3 5 36.03 72.06 0.382 3.91 2 164.8 200.1 301 3 3 0 36.067 72.133 0.382 3.91 2 40.1 11.8 302 -3 -1 5 36.083 72.166 0.382 3.9 2 73.6 39.7 303 1 -6 3 36.084 72.169 0.382 3.9 2 44.7 14.7 304 -1 -3 6 36.164 72.327 0.383 3.89 2 100.1 73.2 305 1 5 0 36.241 72.481 0.384 3.87 2 54.5 21.7 306 4 1 0 36.264 72.528 0.384 3.86 2 53.8 21.1 307 2 -2 5 36.272 72.543 0.384 3.86 2 36.8 9.9 308 0 5 1 36.34 72.681 0.385 3.85 2 69.4 34.9 309 -3 4 2 36.354 72.708 0.385 3.85 2 33.1 7.9 310 -3 5 0 36.392 72.784 0.385 3.84 2 24.5 4.3 311 0 -6 2 36.455 72.91 0.386 3.83 2 133.9 129.0 312 2 2 3 36.458 72.915 0.386 3.82 2 6.6 0.3 313 -1 -1 6 36.46 72.919 0.386 3.82 2 98.8 70.3 314 0 -6 3 36.47 72.941 0.386 3.82 2 10.8 0.8 315 -3 2 4 36.508 73.015 0.386 3.82 2 25.1 4.5 316 4 -2 2 36.545 73.091 0.387 3.81 2 136.1 132.7 317 -2 -4 5 36.56 73.12 0.387 3.8 2 68.1 33.2 318 1 3 3 36.567 73.135 0.387 3.8 2 169.6 205.8 319 1 -5 5 36.591 73.183 0.387 3.8 2 176.0 221.4 320 1 -6 1 36.633 73.266 0.387 3.79 2 86.8 53.7 321 2 3 2 36.66 73.32 0.388 3.78 2 10.1 0.7 322 -3 -2 5 36.71 73.42 0.388 3.78 2 150.8 161.7 323 3 -3 4 36.771 73.541 0.389 3.76 2 88.0 54.8 324 -3 0 5 36.859 73.717 0.389 3.75 2 127.7 114.9 325 3 -2 4 36.897 73.794 0.39 3.74 2 122.1 104.9 326 4 -3 2 37.098 74.196 0.392 3.7 2 138.6 133.9 327 -1 -5 5 37.18 74.36 0.392 3.69 2 15.1 1.6 328 2 -4 5 37.19 74.38 0.392 3.68 2 50.2 17.5 329 2 -6 2 37.199 74.398 0.392 3.68 2 47.4 15.5 330 0 -1 6 37.217 74.435 0.393 3.68 2 84.5 49.5 331 1 2 4 37.222 74.444 0.393 3.68 2 28.5 5.6 332 -2 -5 3 37.243 74.486 0.393 3.68 2 116.7 94.2 333 4 -1 2 37.388 74.777 0.394 3.65 2 161.7 179.5 334 -2 -5 2 37.447 74.895 0.395 3.64 2 27.6 5.2 335 -4 -2 2 37.486 74.973 0.395 3.63 2 105.0 75.3 336 0 -4 6 37.513 75.026 0.395 3.63 2 121.1 100.1 337 1 4 2 37.539 75.078 0.396 3.62 2 58.9 23.7 338 -1 3 4 37.568 75.136 0.396 3.62 2 129.2 113.6 339 3 -5 3 37.582 75.163 0.396 3.61 2 115.7 91.0 340 -4 3 2 37.59 75.18 0.396 3.61 2 60.2 24.6 341 -2 -2 6 37.604 75.208 0.396 3.61 2 70.7 34.0 342 -1 4 3 37.626 75.251 0.396 3.61 2 45.4 14.0 343 4 -4 1 37.688 75.376 0.397 3.6 2 113.0 86.5 344 -4 4 0 37.696 75.391 0.397 3.6 2 18.2 2.3 345 -4 2 3 37.741 75.482 0.397 3.59 2 168.6 192.0 346 2 -6 1 37.757 75.514 0.397 3.58 2 82.5 45.9 347 0 -6 1 37.799 75.598 0.398 3.58 2 44.3 13.2 348 0 -6 4 37.845 75.689 0.398 3.57 2 173.2 201.5 349 1 -6 4 37.854 75.708 0.398 3.57 2 105.8 75.1 350 2 1 4 37.881 75.761 0.399 3.56 2 52.5 18.5 351 2 -1 5 37.904 75.808 0.399 3.56 2 212.0 301.1 352 -2 -1 6 37.994 75.988 0.4 3.54 2 184.9 228.1 353 2 -6 3 37.995 75.989 0.4 3.54 2 117.9 92.8 354 3 -4 4 38.034 76.068 0.4 3.54 2 131.0 114.2 355 -2 4 3 38.081 76.161 0.4 3.53 2 74.7 37.1 356 -2 3 4 38.081 76.163 0.4 3.53 2 200.4 266.7 357 -1 -4 6 38.106 76.211 0.401 3.53 2 153.9 157.2 358 -3 -4 3 38.117 76.234 0.401 3.52 2 101.0 67.7 359 -4 -2 1 38.139 76.278 0.401 3.52 2 111.7 82.7 360 -3 -4 2 38.15 76.299 0.401 3.52 2 11.6 0.9 361 1 -3 6 38.163 76.325 0.401 3.52 2 3.3 0.1 362 -4 -2 3 38.184 76.368 0.401 3.51 2 131.0 113.5 363 -4 0 4 38.363 76.726 0.403 3.49 2 24.4 3.9 364 -2 -5 4 38.39 76.78 0.403 3.48 2 87.7 50.4 365 3 -1 4 38.408 76.816 0.403 3.48 2 58.1 22.1 366 2 4 1 38.477 76.955 0.404 3.47 2 5.5 0.2 367 1 -2 6 38.511 77.022 0.404 3.46 2 1.5 0.0 368 3 2 2 38.555 77.109 0.405 3.46 2 100.1 65.1 369 -2 -3 6 38.595 77.191 0.405 3.45 2 129.8 109.4 370 -4 -1 4 38.604 77.209 0.405 3.45 2 2.9 0.1 371 -1 0 6 38.686 77.372 0.406 3.44 2 90.3 52.7 372 -3 5 1 38.706 77.411 0.406 3.43 2 57.9 21.6 373 -3 -3 5 38.714 77.428 0.406 3.43 2 75.3 36.6 374 -1 6 0 38.93 77.861 0.408 3.4 2 155.1 153.9 375 -2 -5 1 38.996 77.992 0.408 3.39 2 187.0 223.2 376 -3 1 5 39.006 78.012 0.409 3.39 2 23.4 3.5 377 4 -4 2 39.025 78.05 0.409 3.39 2 55.1 19.3 378 -4 4 1 39.047 78.094 0.409 3.38 2 202.1 259.9 379 4 1 1 39.062 78.124 0.409 3.38 2 60.9 23.6 380 3 1 3 39.115 78.231 0.41 3.37 2 128.1 104.1 381 -1 2 5 39.117 78.234 0.41 3.37 2 35.8 8.1 382 -1 -6 3 39.129 78.257 0.41 3.37 2 18.8 2.2 383 1 -4 6 39.189 78.378 0.41 3.36 2 9.8 0.6 384 -1 5 2 39.288 78.576 0.411 3.35 2 175.1 193.2 385 0 3 4 39.322 78.644 0.411 3.34 2 68.6 29.6 386 -3 -4 4 39.424 78.848 0.412 3.33 2 6.5 0.3 387 0 4 3 39.436 78.873 0.412 3.33 2 63.7 25.4 388 1 1 5 39.475 78.95 0.413 3.32 2 198.2 245.7 389 -4 1 4 39.494 78.987 0.413 3.32 2 4.2 0.1 390 -1 -6 2 39.498 78.997 0.413 3.32 2 200.7 251.8 391 -3 -4 1 39.521 79.043 0.413 3.32 2 48.5 14.7 392 3 3 1 39.592 79.184 0.414 3.31 2 171.8 183.7 393 4 0 2 39.596 79.192 0.414 3.31 2 124.2 96.0 394 -2 6 0 39.65 79.299 0.414 3.3 2 58.1 20.9 395 -2 5 2 39.68 79.359 0.414 3.3 2 105.1 68.6 396 -2 2 5 39.682 79.364 0.414 3.3 2 4.4 0.1 397 2 -5 5 39.707 79.413 0.415 3.29 2 208.2 268.7 398 -2 0 6 39.752 79.504 0.415 3.29 2 102.3 64.8 399 0 0 6 39.871 79.742 0.416 3.27 2 76.2 35.7 400 -1 -6 4 40.091 80.182 0.418 3.24 2 198.3 239.9 401 1 5 1 40.097 80.193 0.418 3.24 2 186.9 213.2 402 2 -6 4 40.118 80.236 0.418 3.24 2 28.8 5.1 403 4 2 0 40.121 80.242 0.418 3.24 2 128.8 101.1 404 -4 -2 4 40.21 80.42 0.419 3.23 2 22.1 3.0 405 1 -1 6 40.223 80.446 0.419 3.23 2 42.0 10.7 406 4 -3 3 40.329 80.657 0.42 3.21 2 33.8 6.9 407 4 -2 3 40.341 80.683 0.42 3.21 2 21.9 2.9 408 0 -5 6 40.353 80.706 0.42 3.21 2 63.1 24.0 409 0 6 0 40.457 80.914 0.421 3.2 2 168.2 170.3 410 0 -6 5 40.532 81.064 0.422 3.19 2 18.5 2.1 411 3 -5 4 40.645 81.289 0.423 3.18 2 72.9 31.8 412 -3 4 3 40.778 81.557 0.424 3.16 2 154.9 142.8 413 0 2 5 40.795 81.589 0.424 3.16 2 142.1 120.2 414 -3 3 4 40.836 81.672 0.424 3.16 2 85.5 43.4 415 -2 -5 5 40.853 81.706 0.425 3.15 2 71.1 30.0 416 2 0 5 40.872 81.745 0.425 3.15 2 38.7 8.9 417 1 -6 5 40.922 81.844 0.425 3.15 2 70.6 29.5 418 -2 -4 6 40.938 81.876 0.425 3.14 2 130.8 101.3 419 3 -6 2 40.946 81.892 0.425 3.14 2 27.9 4.6 420 -4 3 3 41.049 82.098 0.426 3.13 2 26.5 4.1 421 3 -6 1 41.109 82.218 0.427 3.13 2 194.4 222.3 422 0 5 2 41.135 82.27 0.427 3.12 2 68.8 27.8 423 -1 -6 1 41.191 82.383 0.427 3.12 2 9.8 0.6 424 3 0 4 41.257 82.514 0.428 3.11 2 155.2 141.1 425 -1 -5 6 41.372 82.743 0.429 3.1 2 50.7 15.0 426 4 -5 1 41.512 83.023 0.43 3.08 2 96.4 53.9 427 1 -5 6 41.562 83.125 0.431 3.08 2 38.7 8.7 428 -4 -3 2 41.565 83.129 0.431 3.08 2 130.9 99.3 429 4 -4 3 41.67 83.339 0.432 3.07 2 100.1 57.9 430 -4 -3 3 41.699 83.398 0.432 3.07 2 110.9 71.0 431 -4 4 2 41.706 83.412 0.432 3.07 2 13.4 1.0 432 4 -1 3 41.707 83.414 0.432 3.07 2 50.6 14.8 433 -5 1 1 41.721 83.442 0.432 3.06 2 9.6 0.5 434 -3 -1 6 41.74 83.479 0.432 3.06 2 109.5 69.1 435 -3 -2 6 41.796 83.593 0.433 3.06 2 94.1 51.0 436 2 5 0 41.847 83.694 0.433 3.05 2 19.0 2.1 437 -4 2 4 41.967 83.934 0.434 3.04 2 9.5 0.5 438 -3 -4 5 42.038 84.077 0.435 3.03 2 98.7 55.6 439 -4 5 0 42.065 84.13 0.435 3.03 2 78.8 35.4 440 3 -6 3 42.101 84.202 0.435 3.03 2 130.4 97.0 441 -5 2 1 42.107 84.215 0.435 3.03 2 75.4 32.4 442 3 4 0 42.198 84.397 0.436 3.02 2 101.3 58.3 443 -1 1 6 42.225 84.449 0.436 3.02 2 151.3 130.1 444 -5 2 0 42.255 84.51 0.436 3.02 2 53.6 16.3 445 3 -3 5 42.27 84.539 0.437 3.01 2 113.3 72.9 446 4 -5 2 42.275 84.549 0.437 3.01 2 174.4 172.6 447 -3 5 2 42.295 84.591 0.437 3.01 2 116.5 76.9 448 -5 1 2 42.343 84.686 0.437 3.01 2 124.4 87.6 449 -1 -6 5 42.365 84.731 0.437 3.01 2 11.7 0.8 450 -5 1 0 42.415 84.829 0.438 3.0 2 163.6 151.2 451 2 3 3 42.426 84.852 0.438 3.0 2 214.2 259.1 452 -3 2 5 42.468 84.936 0.438 3.0 2 133.8 101.0 453 -4 -1 5 42.489 84.978 0.438 3.0 2 36.0 7.3 454 2 -3 6 42.494 84.988 0.438 2.99 2 3.5 0.1 455 -1 6 1 42.505 85.01 0.439 2.99 2 7.4 0.3 456 -3 6 0 42.588 85.176 0.439 2.99 2 27.9 4.4 457 -5 0 1 42.682 85.364 0.44 2.98 2 25.1 3.5 458 -4 -3 1 42.745 85.49 0.441 2.97 2 129.3 93.5 459 -5 0 2 42.758 85.516 0.441 2.97 2 33.9 6.4 460 -4 0 5 42.798 85.595 0.441 2.97 2 208.6 243.1 461 -1 -3 7 42.799 85.597 0.441 2.97 2 82.4 38.0 462 -1 -2 7 42.812 85.625 0.441 2.97 2 76.4 32.6 463 -2 6 1 42.834 85.667 0.441 2.97 2 92.8 48.1 464 -2 1 6 42.837 85.675 0.441 2.97 2 166.2 154.2 465 1 -7 3 42.875 85.751 0.442 2.96 2 130.5 95.0 466 3 -2 5 42.936 85.872 0.442 2.96 2 72.1 28.9 467 3 -4 5 42.948 85.897 0.442 2.96 2 56.9 18.0 468 2 2 4 43.0 86.0 0.443 2.95 2 104.7 61.0 469 1 -7 2 43.026 86.053 0.443 2.95 2 102.2 58.1 470 -3 0 6 43.029 86.058 0.443 2.95 2 57.2 18.2 471 0 -3 7 43.036 86.072 0.443 2.95 2 138.9 107.1 472 2 -4 6 43.064 86.127 0.443 2.95 2 57.8 18.6 473 4 1 2 43.117 86.234 0.444 2.95 2 86.4 41.3 474 -4 -3 4 43.147 86.293 0.444 2.94 2 20.2 2.3 475 -3 -3 6 43.198 86.396 0.444 2.94 2 138.2 105.6 476 1 0 6 43.263 86.527 0.445 2.93 2 37.7 7.8 477 2 -2 6 43.269 86.538 0.445 2.93 2 131.0 94.8 478 1 3 4 43.271 86.542 0.445 2.93 2 17.0 1.6 479 -5 2 2 43.272 86.544 0.445 2.93 2 1.1 0.0 480 4 2 1 43.392 86.784 0.446 2.93 2 10.9 0.7 481 2 4 2 43.42 86.84 0.446 2.92 2 30.6 5.1 482 -5 3 0 43.44 86.88 0.446 2.92 2 213.1 249.7 483 1 4 3 43.44 86.88 0.446 2.92 2 100.4 55.4 484 0 -2 7 43.484 86.969 0.447 2.92 2 110.3 66.8 485 -4 -2 5 43.524 87.048 0.447 2.92 2 192.6 203.5 486 2 -6 5 43.527 87.053 0.447 2.92 2 32.5 5.8 487 0 -7 3 43.679 87.358 0.448 2.91 2 22.5 2.8 488 5 -2 1 43.714 87.428 0.449 2.9 2 48.8 13.0 489 0 1 6 43.823 87.647 0.449 2.9 2 32.7 5.8 490 -5 3 1 43.836 87.672 0.45 2.89 2 36.9 7.4 491 -3 -5 3 43.887 87.775 0.45 2.89 2 202.4 223.0 492 5 0 0 43.917 87.833 0.45 2.89 2 103.5 58.3 493 -4 5 1 43.928 87.856 0.45 2.89 2 40.0 8.7 494 0 -4 7 43.93 87.86 0.45 2.89 2 29.6 4.8 495 -2 -6 3 43.948 87.896 0.45 2.89 2 20.5 2.3 496 1 -7 4 44.035 88.069 0.451 2.88 2 6.1 0.2 497 2 -7 2 44.053 88.107 0.451 2.88 2 46.6 11.8 498 -1 4 4 44.078 88.156 0.452 2.88 2 61.8 20.7 499 3 2 3 44.096 88.192 0.452 2.88 2 15.7 1.3 500 -1 -4 7 44.127 88.254 0.452 2.88 2 103.1 57.5 501 -2 4 4 44.142 88.283 0.452 2.88 2 123.7 82.8 502 -5 0 3 44.144 88.289 0.452 2.88 2 122.8 81.6 503 -1 -1 7 44.168 88.337 0.452 2.87 2 49.7 13.3 504 1 6 0 44.181 88.362 0.452 2.87 2 111.0 66.7 505 0 -7 2 44.207 88.415 0.453 2.87 2 66.8 24.1 506 -5 1 3 44.273 88.546 0.453 2.87 2 2.1 0.0 507 2 -7 3 44.28 88.56 0.453 2.87 2 129.2 90.1 508 4 -5 3 44.345 88.69 0.454 2.86 2 58.2 18.3 509 3 3 2 44.346 88.692 0.454 2.86 2 0.0 0.0 510 -2 -2 7 44.349 88.698 0.454 2.86 2 4.1 0.1 511 5 -3 1 44.353 88.707 0.454 2.86 2 5.6 0.2 512 0 6 1 44.385 88.771 0.454 2.86 2 50.3 13.6 513 4 0 3 44.407 88.815 0.454 2.86 2 44.9 10.9 514 5 -1 1 44.416 88.832 0.454 2.86 2 14.3 1.1 515 -4 1 5 44.447 88.895 0.455 2.86 2 48.7 12.8 516 0 -7 4 44.46 88.92 0.455 2.86 2 62.9 21.2 517 -3 -5 2 44.462 88.924 0.455 2.86 2 2.0 0.0 518 1 -7 1 44.486 88.973 0.455 2.86 2 86.2 39.9 519 0 -6 6 44.489 88.978 0.455 2.86 2 95.5 49.1 520 -5 -1 2 44.514 89.029 0.455 2.85 2 156.2 131.1 521 -2 -6 4 44.517 89.033 0.455 2.85 2 109.1 63.9 522 3 -6 4 44.561 89.122 0.455 2.85 2 41.5 9.2 523 -2 -5 6 44.595 89.189 0.456 2.85 2 136.3 99.6 524 -3 -5 4 44.621 89.243 0.456 2.85 2 7.8 0.3 525 1 2 5 44.666 89.333 0.456 2.85 2 60.7 19.7 526 -2 -6 2 44.688 89.376 0.456 2.84 2 57.0 17.4 527 -2 -3 7 44.769 89.538 0.457 2.84 2 3.8 0.1 528 -1 3 5 44.788 89.576 0.457 2.84 2 55.1 16.2 529 4 -3 4 44.809 89.618 0.457 2.84 2 65.5 22.9 530 -2 3 5 44.908 89.816 0.458 2.83 2 15.1 1.2 531 -1 5 3 44.932 89.864 0.458 2.83 2 25.4 3.4 532 -2 5 3 44.939 89.877 0.459 2.83 2 25.7 3.5 533 3 -1 5 44.942 89.883 0.459 2.83 2 57.7 17.7 534 3 -5 5 44.967 89.934 0.459 2.83 2 83.7 37.3 535 2 -5 6 44.973 89.946 0.459 2.83 2 44.9 10.7 536 -5 -1 1 44.981 89.962 0.459 2.83 2 31.7 5.3 X-ray diffraction powder data (I)...X-Ray wave length = 1.54056 (angs.): No H K L Theta 2*Theta d I int I int.n. I p.h.n. H(Si) ( degree ) (angstrem) *100 *100 1 0 0 1 6.133 12.267 7.20945 75.8 1.3 1.3 5.6 2 0 -1 1 6.707 13.414 6.59513 393.7 6.8 6.9 5.6 3 1 0 0 7.974 15.948 5.55267 4832.9 83.9 84.4 5.6 4 -1 1 0 8.793 17.586 5.03892 1155.9 20.1 20.2 5.6 5 1 -1 1 10.288 20.577 4.31286 4355.3 75.6 75.9 5.6 6 -1 -1 1 10.605 21.211 4.18532 766.2 13.3 13.3 5.6 7 0 -1 2 11.303 22.607 3.92992 505.2 8.8 8.8 5.6 8 0 -2 1 11.428 22.856 3.88763 161.4 2.8 2.8 5.6 9 0 0 2 12.338 24.677 3.60473 3947.6 68.5 68.6 5.6 10 0 2 0 12.491 24.983 3.5613 5759.6 100.0 100.0 5.6 11 1 -2 1 12.914 25.827 3.44674 704.6 12.2 12.2 5.6 12 -1 2 0 13.037 26.073 3.41476 2763.0 48.0 47.9 5.6 13 -1 0 2 13.147 26.295 3.38649 4223.3 73.3 73.3 5.6 14 -1 -1 2 13.19 26.379 3.37583 269.9 4.7 4.7 5.6 15 0 -2 2 13.509 27.017 3.29756 2234.4 38.8 38.7 5.6 16 1 -1 2 14.567 29.134 3.06257 284.7 4.9 4.9 5.6 17 1 1 1 14.884 29.768 2.99875 2725.0 47.3 47.1 5.6 18 -1 -2 1 15.008 30.017 2.97452 148.1 2.6 2.6 5.6 19 1 -2 2 15.546 31.093 2.87396 2086.2 36.2 36.0 5.6 20 -2 1 0 15.733 31.467 2.84067 134.4 2.3 2.3 5.6 21 -1 1 2 15.872 31.745 2.81641 862.1 15.0 14.9 5.6 22 -2 0 1 15.918 31.837 2.80851 1161.8 20.2 20.1 5.6 23 -1 -2 2 15.979 31.958 2.79811 3438.0 59.7 59.4 5.6 24 0 1 2 16.035 32.069 2.78866 92.6 1.6 1.6 5.6 25 2 0 0 16.108 32.216 2.77634 372.6 6.5 6.4 5.6 26 1 0 2 16.226 32.451 2.75672 1022.7 17.8 17.7 5.6 27 -2 1 1 16.561 33.122 2.70241 3454.2 60.0 59.6 5.6 28 0 -1 3 17.056 34.111 2.62625 1152.6 20.0 19.9 5.7 29 0 -3 1 17.283 34.567 2.5927 79.9 1.4 1.4 5.7 30 2 -1 1 17.321 34.643 2.58718 2179.2 37.8 37.5 5.7 31 1 -3 1 17.595 35.191 2.54814 1236.7 21.5 21.3 5.7 32 -2 -1 1 17.715 35.43 2.53143 1796.3 31.2 30.9 5.7 33 -1 -1 3 17.764 35.528 2.52467 186.6 3.2 3.2 5.7 34 -2 2 0 17.802 35.604 2.51946 446.9 7.8 7.7 5.7 35 -2 0 2 18.079 36.157 2.4822 1005.7 17.5 17.3 5.7 36 2 -2 1 18.35 36.701 2.44666 154.8 2.7 2.7 5.7 37 -1 3 0 18.605 37.21 2.41433 543.0 9.4 9.3 5.7 38 0 0 3 18.695 37.39 2.40315 102.4 1.8 1.8 5.7 39 2 1 0 18.796 37.592 2.39068 150.1 2.6 2.6 5.7 40 -2 -1 2 18.832 37.664 2.38627 494.0 8.6 8.5 5.7 41 0 3 0 18.932 37.863 2.3742 206.3 3.6 3.5 5.7 42 -2 2 1 19.43 38.86 2.31556 196.3 3.4 3.4 5.7 43 -2 1 2 19.533 39.066 2.3038 189.1 3.3 3.2 5.7 44 1 -2 3 19.962 39.925 2.25621 162.0 2.8 2.8 5.7 45 1 -1 3 20.042 40.084 2.2476 1032.0 17.9 17.7 5.7 46 -1 2 2 20.378 40.757 2.21207 1585.1 27.5 27.1 5.7 47 0 -3 3 20.511 41.022 2.19838 88.9 1.5 1.5 5.7 48 -1 -3 1 20.587 41.173 2.19064 282.7 4.9 4.8 5.7 49 0 2 2 21.162 42.324 2.13372 765.9 13.3 13.1 5.7 50 2 -3 1 21.387 42.774 2.11228 600.2 10.4 10.3 5.7 51 -2 -2 1 21.418 42.836 2.10937 111.1 1.9 1.9 5.7 52 -2 -2 2 21.598 43.195 2.09266 270.3 4.7 4.6 5.7 53 -2 3 0 21.708 43.416 2.08254 232.9 4.0 4.0 5.7 54 2 1 1 21.796 43.592 2.07451 1097.9 19.1 18.7 5.7 55 -2 -1 3 21.86 43.72 2.06876 176.7 3.1 3.0 5.7 56 1 -3 3 21.895 43.789 2.06565 1318.6 22.9 22.5 5.7 57 -2 0 3 21.99 43.98 2.05714 395.6 6.9 6.8 5.7 58 1 0 3 22.116 44.232 2.04601 114.9 2.0 2.0 5.7 59 0 1 3 22.207 44.413 2.03806 480.7 8.3 8.2 5.7 60 0 3 1 22.389 44.779 2.02226 312.6 5.4 5.3 5.7 61 -2 2 2 22.841 45.681 1.98439 177.2 3.1 3.0 5.7 62 0 -2 4 23.08 46.159 1.96496 734.1 12.7 12.5 5.7 63 0 -1 4 23.301 46.601 1.94734 173.9 3.0 3.0 5.7 64 0 -4 2 23.345 46.691 1.94381 1473.9 25.6 25.1 5.7 65 1 -4 2 23.512 47.025 1.93078 482.4 8.4 8.2 5.7 66 -2 -2 3 23.614 47.228 1.92296 100.6 1.7 1.7 5.7 67 -1 -2 4 23.712 47.424 1.91544 927.1 16.1 15.8 5.7 68 -2 3 1 23.848 47.695 1.90519 698.5 12.1 11.9 5.7 69 -3 0 1 23.955 47.911 1.89712 502.4 8.7 8.5 5.7 70 -1 0 4 24.771 49.542 1.83842 307.7 5.3 5.2 5.7 71 -1 4 0 24.811 49.622 1.83563 368.1 6.4 6.2 5.7 72 1 2 2 24.946 49.891 1.82636 317.6 5.5 5.4 5.7 73 2 -2 3 25.022 50.044 1.82114 61.4 1.1 1.0 5.7 74 0 0 4 25.301 50.602 1.80236 619.6 10.8 10.5 5.8 75 3 -1 1 25.392 50.784 1.79633 371.5 6.4 6.3 5.8 76 -3 2 1 25.486 50.972 1.79014 725.1 12.6 12.3 5.8 77 0 4 0 25.632 51.263 1.78065 2576.8 44.7 43.6 5.8 78 1 1 3 25.799 51.598 1.76988 1467.5 25.5 24.8 5.8 79 2 -4 1 25.859 51.719 1.76603 589.7 10.2 10.0 5.8 80 -1 3 2 25.922 51.845 1.76204 246.7 4.3 4.2 5.8 81 -1 -4 2 26.089 52.178 1.75158 981.9 17.0 16.6 5.8 82 2 -3 3 26.12 52.24 1.74962 578.6 10.0 9.8 5.8 83 -2 -1 4 26.271 52.541 1.74031 512.1 8.9 8.7 5.8 84 -2 -3 1 26.386 52.771 1.73326 884.1 15.3 14.9 5.8 85 -2 4 0 26.817 53.635 1.70738 270.6 4.7 4.6 5.8 86 3 0 1 26.876 53.753 1.70391 200.4 3.5 3.4 5.8 87 -2 -3 3 26.969 53.938 1.6985 234.4 4.1 4.0 5.8 88 0 2 3 27.016 54.033 1.69573 135.7 2.4 2.3 5.8 89 -2 0 4 27.059 54.119 1.69324 395.5 6.9 6.7 5.8 90 0 3 2 27.116 54.231 1.69 255.4 4.4 4.3 5.8 91 -2 -2 4 27.152 54.304 1.68792 268.6 4.7 4.5 5.8 92 3 -3 1 27.49 54.98 1.66873 892.1 15.5 15.0 5.8 93 -3 0 3 27.741 55.483 1.6548 228.6 4.0 3.8 5.8 94 -1 1 4 27.803 55.606 1.65144 289.3 5.0 4.9 5.8 95 0 -4 4 27.851 55.703 1.64878 667.9 11.6 11.2 5.8 96 2 0 3 27.918 55.837 1.64515 86.1 1.5 1.4 5.8 97 3 -2 2 28.099 56.198 1.63542 84.8 1.5 1.4 5.8 98 -3 -1 3 28.157 56.313 1.63236 298.5 5.2 5.0 5.8 99 -3 3 1 28.684 57.369 1.60481 189.0 3.3 3.2 5.8 100 2 -4 3 28.804 57.607 1.59872 180.9 3.1 3.0 5.8 101 1 -4 4 28.9 57.799 1.59387 108.6 1.9 1.8 5.8 102 -3 1 3 28.934 57.868 1.59214 71.9 1.2 1.2 5.8 103 1 4 0 29.109 58.218 1.58339 198.7 3.4 3.3 5.8 104 0 -2 5 29.164 58.328 1.58068 75.6 1.3 1.3 5.8 105 -3 -2 1 29.208 58.416 1.5785 279.8 4.9 4.7 5.8 106 -2 4 1 29.311 58.622 1.57344 230.4 4.0 3.9 5.8 107 -1 -4 4 29.431 58.862 1.5676 697.9 12.1 11.7 5.8 108 1 -5 1 29.63 59.26 1.55802 188.6 3.3 3.2 5.8 109 3 1 1 29.884 59.767 1.546 611.3 10.6 10.2 5.8 110 0 -1 5 29.982 59.965 1.54138 198.3 3.4 3.3 5.8 111 -3 -2 3 30.136 60.273 1.53424 331.7 5.8 5.5 5.8 112 0 -5 3 30.203 60.407 1.53116 190.8 3.3 3.2 5.8 113 1 -5 3 30.278 60.557 1.52772 214.4 3.7 3.6 5.8 114 -1 -3 5 30.503 61.005 1.51757 106.3 1.8 1.8 5.8 115 3 0 2 30.55 61.101 1.51542 235.3 4.1 3.9 5.8 116 3 -4 1 30.837 61.674 1.5027 257.3 4.5 4.3 5.8 117 -2 -4 2 31.193 62.386 1.48726 102.2 1.8 1.7 5.8 118 2 -5 1 31.364 62.727 1.47998 162.0 2.8 2.7 5.8 119 -1 0 5 31.417 62.833 1.47774 64.0 1.1 1.1 5.9 120 -3 3 2 31.518 63.036 1.47346 61.0 1.1 1.0 5.9 121 -1 5 0 31.55 63.099 1.47215 147.8 2.6 2.5 5.9 122 2 1 3 31.594 63.188 1.47028 837.9 14.5 13.9 5.9 123 1 -3 5 31.824 63.647 1.46079 444.4 7.7 7.4 5.9 124 3 -4 2 31.876 63.753 1.45862 84.4 1.5 1.4 5.9 125 2 3 1 31.99 63.98 1.45399 493.6 8.6 8.2 5.9 126 -1 2 4 32.136 64.272 1.44808 215.6 3.7 3.6 5.9 127 -4 1 1 32.194 64.388 1.44576 118.0 2.0 2.0 5.9 128 -1 4 2 32.224 64.448 1.44454 190.6 3.3 3.2 5.9 129 -2 -4 1 32.269 64.538 1.44276 97.5 1.7 1.6 5.9 130 3 -3 3 32.398 64.797 1.43762 245.6 4.3 4.1 5.9 131 -4 1 0 32.539 65.079 1.43207 116.1 2.0 1.9 5.9 132 -1 -5 3 32.61 65.219 1.42932 68.6 1.2 1.1 5.9 133 -4 0 1 32.771 65.541 1.42308 557.5 9.7 9.2 5.9 134 -4 2 0 32.842 65.684 1.42034 785.4 13.6 13.0 5.9 135 3 -1 3 32.946 65.891 1.41636 174.1 3.0 2.9 5.9 136 -4 2 1 33.094 66.188 1.41073 274.1 4.8 4.5 5.9 137 -3 4 1 33.149 66.298 1.40866 406.1 7.1 6.7 5.9 138 -4 1 2 33.288 66.576 1.40344 65.5 1.1 1.1 5.9 139 -2 -4 4 33.406 66.812 1.39906 250.8 4.4 4.2 5.9 140 -3 1 4 33.441 66.882 1.39777 135.7 2.4 2.2 5.9 141 -3 -3 3 33.513 67.026 1.39511 423.6 7.4 7.0 5.9 142 -1 -5 1 33.645 67.291 1.39027 158.6 2.8 2.6 5.9 143 0 4 2 33.743 67.487 1.38671 189.3 3.3 3.1 5.9 144 -3 -3 1 33.824 67.648 1.3838 126.6 2.2 2.1 5.9 145 3 2 1 34.174 68.348 1.37132 68.6 1.2 1.1 5.9 146 4 -1 1 34.302 68.604 1.36682 182.7 3.2 3.0 5.9 147 -1 1 5 34.645 69.29 1.35496 95.6 1.7 1.6 5.9 148 -4 -1 1 34.786 69.573 1.35014 57.9 1.0 1.0 5.9 149 -4 0 3 35.161 70.321 1.33759 310.5 5.4 5.1 5.9 150 3 -5 1 35.416 70.832 1.32919 88.5 1.5 1.5 5.9 151 -1 -2 6 35.607 71.214 1.32301 438.5 7.6 7.2 5.9 152 1 -6 2 35.671 71.343 1.32093 303.4 5.3 5.0 5.9 153 0 -5 5 35.731 71.461 1.31903 184.0 3.2 3.0 5.9 154 0 1 5 35.936 71.872 1.31249 150.3 2.6 2.5 5.9 155 2 -3 5 36.03 72.06 1.30953 339.8 5.9 5.6 5.9 156 1 -6 3 36.084 72.169 1.30783 66.2 1.2 1.1 5.9 157 -1 -3 6 36.164 72.327 1.30535 73.2 1.3 1.2 5.9 158 0 -6 2 36.455 72.91 1.29635 200.5 3.5 3.3 6.0 159 1 3 3 36.567 73.135 1.29292 593.1 10.3 9.7 6.0 160 -3 -2 5 36.71 73.42 1.2886 161.7 2.8 2.6 6.0 161 -3 0 5 36.859 73.717 1.28413 114.9 2.0 1.9 6.0 162 3 -2 4 36.897 73.794 1.28299 104.9 1.8 1.7 6.0 163 4 -3 2 37.098 74.196 1.27703 133.9 2.3 2.2 6.0 164 -2 -5 3 37.243 74.486 1.27278 149.3 2.6 2.4 6.0 165 4 -1 2 37.388 74.777 1.26854 179.5 3.1 2.9 6.0 166 0 -4 6 37.513 75.026 1.26495 175.4 3.0 2.9 6.0 167 3 -5 3 37.582 75.163 1.26298 286.8 5.0 4.7 6.0 168 4 -4 1 37.688 75.376 1.25994 88.7 1.5 1.4 6.0 169 -4 2 3 37.741 75.482 1.25844 237.8 4.1 3.9 6.0 170 0 -6 4 37.845 75.689 1.2555 276.6 4.8 4.5 6.0 171 2 -1 5 37.904 75.808 1.25384 319.6 5.5 5.2 6.0 172 -2 -1 6 37.994 75.988 1.25131 320.9 5.6 5.2 6.0 173 3 -4 4 38.034 76.068 1.2502 114.2 2.0 1.9 6.0 174 -1 -4 6 38.106 76.211 1.2482 461.0 8.0 7.5 6.0 175 -4 -2 1 38.139 76.278 1.24728 150.4 2.6 2.4 6.0 176 -4 -2 3 38.184 76.368 1.24602 113.5 2.0 1.8 6.0 177 -2 -5 4 38.39 76.78 1.24037 76.4 1.3 1.2 6.0 178 3 2 2 38.555 77.109 1.23589 65.1 1.1 1.1 6.0 179 -2 -3 6 38.595 77.191 1.23478 109.4 1.9 1.8 6.0 180 -1 0 6 38.686 77.372 1.23234 110.9 1.9 1.8 6.0 181 -1 6 0 38.93 77.861 1.22583 153.9 2.7 2.5 6.0 182 -2 -5 1 38.996 77.992 1.22409 246.0 4.3 4.0 6.0 183 -4 4 1 39.047 78.094 1.22275 283.6 4.9 4.6 6.0 184 3 1 3 39.115 78.231 1.22095 114.5 2.0 1.9 6.0 185 -1 5 2 39.288 78.576 1.21645 193.2 3.4 3.1 6.0 186 -1 -6 2 39.498 78.997 1.21103 512.3 8.9 8.3 6.0 187 3 3 1 39.592 79.184 1.20862 279.7 4.9 4.5 6.0 188 2 -5 5 39.707 79.413 1.20572 358.2 6.2 5.8 6.0 189 -2 0 6 39.752 79.504 1.20457 64.8 1.1 1.0 6.0 190 -1 -6 4 40.091 80.182 1.19607 559.3 9.7 9.0 6.0 191 0 6 0 40.457 80.914 1.1871 170.3 3.0 2.7 6.1 192 -3 4 3 40.778 81.557 1.17936 263.0 4.6 4.2 6.1 193 -3 3 4 40.836 81.672 1.17798 73.4 1.3 1.2 6.1 194 -2 -4 6 40.938 81.876 1.17557 135.4 2.4 2.2 6.1 195 3 -6 1 41.109 82.218 1.17154 250.2 4.3 4.0 6.1 196 3 0 4 41.257 82.514 1.16809 141.1 2.4 2.3 6.1 197 -4 -3 2 41.565 83.129 1.161 107.9 1.9 1.7 6.1 198 -4 -3 3 41.699 83.398 1.15794 145.2 2.5 2.3 6.1 199 -3 -1 6 41.74 83.479 1.15702 69.1 1.2 1.1 6.1 200 -3 -4 5 42.038 84.077 1.15031 91.0 1.6 1.5 6.1 201 3 -6 3 42.101 84.202 1.14891 129.4 2.2 2.1 6.1 202 -1 1 6 42.225 84.449 1.14618 188.4 3.3 3.0 6.1 203 4 -5 2 42.275 84.549 1.14508 338.6 5.9 5.4 6.1 204 -5 1 2 42.343 84.686 1.14358 88.3 1.5 1.4 6.1 205 2 3 3 42.426 84.852 1.14176 410.3 7.1 6.5 6.1 206 -3 2 5 42.468 84.936 1.14085 108.4 1.9 1.7 6.1 207 -4 -3 1 42.745 85.49 1.13487 100.0 1.7 1.6 6.1 208 -4 0 5 42.798 85.595 1.13375 313.7 5.4 5.0 6.1 209 -2 1 6 42.837 85.675 1.1329 202.3 3.5 3.2 6.1 210 1 -7 3 42.875 85.751 1.13209 95.0 1.6 1.5 6.1 211 2 2 4 43.0 86.0 1.12944 137.2 2.4 2.2 6.1 212 0 -3 7 43.036 86.072 1.12868 125.7 2.2 2.0 6.1 213 -3 -3 6 43.198 86.396 1.12528 105.6 1.8 1.7 6.1 214 2 -2 6 43.269 86.538 1.1238 104.3 1.8 1.7 6.1 215 1 4 3 43.44 86.88 1.12025 310.3 5.4 4.9 6.1 216 0 -2 7 43.484 86.969 1.11934 66.8 1.2 1.1 6.1 217 -4 -2 5 43.524 87.048 1.11852 209.3 3.6 3.3 6.1 218 -3 -5 3 43.887 87.775 1.11113 281.3 4.9 4.4 6.2 219 -5 0 3 44.144 88.289 1.10598 222.0 3.9 3.5 6.2 220 1 6 0 44.181 88.362 1.10525 104.1 1.8 1.6 6.2 221 2 -7 3 44.28 88.56 1.10329 90.1 1.6 1.4 6.2 222 -2 -6 4 44.517 89.033 1.09865 284.0 4.9 4.5 6.2 223 -2 -5 6 44.595 89.189 1.09713 99.9 1.7 1.6 6.2 224 3 -5 5 44.967 89.934 1.08997 79.2 1.4 1.2 6.2 Reference: Chichagov A.V. et al. Information-Calculating System on Crystal Structure Data of Minerals (MINCRYST) - Kristallographiya, v.35, n.3, 1990, p.610-616 (in Russian) |